Determination of selected trace elements in marine biota samples with the application of fast temperature programs and solid sampling continuous source high resolution atomic absorption spectroscopy: method validation

Analytical procedure for the determination of As, Cd, Cu, Ni, Co and Cr in marine biota samples using solid sampling high-resolution continuum source atomic absorption spectrometry (HR CS AAS) and accelerated fast temperature programmes has been developed. Calibration technique based on the use of solid certified reference materials similar to the nature of the analysed sample and statistics of regression analysis were applied. A validation approach in line with the requirements of ISO 17025 standard and Eurachem guidelines was followed. Accordingly, blanks, selectivity, calibration, linearity, working range, trueness, repeatability and reproducibility, limits of detection and quantification and expanded uncertainty for all investigated elements were assessed. The major contributors to the combined uncertainty of the analyte mass fractions were found to be the homogeneity of the samples and the microbalance precision. Traceability to the SI system of units of the obtained with the proposed analytical procedure results was also demonstrated. The potential of the proposed analytical procedure based on solid sampling HR CS AAS technique was demonstrated by direct analysis of marine reference biota samples. Overall, the use of solid sampling HR CS AAS permits obtaining significant advantages for the determination of selected trace elements in marine biota samples, such as straightforward calibration, a high sample throughput, sufficient precision, a suitable limit of detection and reduced risk of analyte loss and contamination.     

用功的互等定理求解矩形薄板的自然频率

从虚功原理出发，证明了薄板小挠度弯曲问题的功的互等定理，并由此推出了求解矩形薄板自然频率的公式．算例表明，该公式计算简便，精度较高．     

圆柱形弹性贮液容器基频近似计算法

在工业和工程领域中,广泛地应用圆柱形弹性薄壁贮液容器。在冲击或地震地面运动激励下,此种容器的变形,严格地说就遵循薄壳结构动力学规律。考虑到在水平地震作用下短圆柱形容器的变形,剪切效应起主导作用,因而可用剪切梁变形理论来近似地代替。对于盛有液体的贮液容器,因为激励引起的振动是耦联的,即液体中产生的液动压力与结构的变形有关,而结构的变形又受到液动压力的很大影响。欲寻求此种耦联体系的动力响应,必须对其动力特性进行分析。为此,本文根据Fischer“冲击质量”理论,提出了对圆柱形弹性贮液容器基频的近似计算方法。此方法概念清晰,计算简便,很便于工程上应用。     

Vibrations of a Floating Elastic Plate Due to Periodic Displacements of a Bottom Segment

The problem of the behavior of a floating elastic thin plate under periodic vibrations of a bottom segment is solved using a numerical procedure based on the Wiener-Hopf technique. The effects of the vibration frequency, the position of the vibrating bottom segment, and the fluid depth on the vibration frequencies of the fluid and plate are studied numerically.__________Translated from Prikladnaya Mekhanika i Tekhnicheskaya Fizika, Vol. 46, No. 5, pp. 166–179, September–October, 2005.     

相移数字云纹测量系统

介绍了一种相位移数字云纹变形测量系统．测试系统采用ＣＣＤ摄像系统记录光栅图像，控制采样的空间频率大约为光栅线密度的整数倍，对试件栅进行采样后用数字信号处理的方法，实现空间相位移及进行实时数字云纹条纹显示，并对相移误差及光栅信号的高阶谐波的影响进行了校正     

双层旋转壳流固耦合振动有限元分析

本文采用旋转壳体元和流体元分析了双层旋转壳体流固耦合振动特性,基于Novozhilov壳体理论、水弹性理论以及Hamilton变分原理推导出耦合系统运动方程,计算结果与实测值比较表明本分析方法有较好的精度。     

弹性非保守压杆的大幅度动力分析

本文讨论弹性非保守压杆的大幅度动力问题。导出了在一般非保守力作用下杆的非线性运动微分方程,并给出与此相应的拟Hamilton变分表达式,具体地分析了悬臂杆在大挠度下的动力特性,当挠度很小其高次项可以略去时,本文所得结论都能近似地退化为线性理论的结果。     

基于MOS晶体管的低频功率放大器设计与实现

功率放大器是＂电子技术＂课程中一个重要内容。本文结合第九届全国大学生电子设计竞赛,介绍了一种由分立的大功率MOS晶体管实现的低频宽带功率放大器系统设计。该系统由阻抗匹配电路、前置放大电路、低通滤波电路、带阻滤波电路和功率放大电路组成。测试结果表明设计满足指标要求。     

基于DCSBM模型的受访者驱动抽样调查估计量改进

大数据背景下,将受访者驱动抽样(RDS)用于网络抽样调查,解决了传统抽样调查难以获得可用抽样框、难以接触被调查者以及难以获得回答等问题,也使得网络调查可以实现概率抽样,得到一定误差范围内的总体参数估计.然而,在实际抽样过程中,同质性问题(即样本单元在推荐同伴时倾向于推荐那些与自己有相同属性的同伴)会导致RDS估计量的方...     

TD-MBMS与R4/HSDPA共网时隔离带设置分析

本文首先分析了TD-SCDMA网络中TD-MBMS与R4/HSDPA共存时存在的干扰,并从理论上探讨了如何设置隔离带宽度才能有效规避MBMS业务对R4/HSDPA性能的影响。然后,利用系统级仿真平台对各种场景进行模拟分析,并与理论值做了对比验证。本文提出了在保证网络性能前提下的最佳隔离距离的判断方法,并给出在中等负荷网络情况下隔离距离的建议值。