锁网终端分析模型的研究与应用

随着3G和4G网络建设的完善,为了降低2G网络的数据业务压力,提高3G/4G网络的使用,如何引导客户充分使用3G/4G网络成为市场经营的一个重点课题,而终端锁网用户的解锁工作就是其中一个重要组成部分。基于大数据分析理论,充分利用网络侧的CS域与PS域多个接口的信令数据,并联合规划、话单等话单数据,开展锁网终端模型的分析研究。另外本文还介绍了中山地市业务部门应用该模型在2013年精确定位3G/4G锁网用户用于实际解锁营销和终端更换营销中,所取得的良好营销效果。     

利用串联双滤波技术改善声光滤波器光谱分辨率的实验研究

考虑旋光性设计 制作了两个非共线型声光可调滤波器(AOTF),通过前后放置对信号光进行两次的级联滤 波。 调节前后两个AOTF所加的超声频率值, 保证前后两个AOTF存在透射光谱的叠加区,从而实现光谱分辨率的提升及调控。实 验结果表明,双滤波技术还可以有效抑制AOTF透射光谱的旁瓣效应,改善透射光 谱的纯度。     

顺序扫描阵列配置方法研究

对于超宽带稀疏阵列,均匀无冗余阵列具有低栅瓣水平和高方位向分辨率。阵列配置的目的是设计双程阵列,使其单程等效阵列是均匀无冗余的。文中主要配置顺序扫描阵列,证明了若阵元总数大于4,没有均匀无冗余阵列的配置方法。然后给出了一种非均匀阵列配置方法,分析了其方位向分辨率和栅瓣水平。理论与仿真表明,文中提出的方法比与其阵元总数相同的端发多收阵列的栅瓣低。最后,根据所需要的方位向分辨率和栅瓣水平配置了一种实际顺序扫描阵列。     

The first stereoselective synthesis of dendrodolide A

The first stereoselective total synthesis of natural product, dendrodolide A (1) is described from readily available (R)-propylene oxide and 3-buten-1-ol as starting materials. The synthesis was achieved in 10 steps with an overall yield of 19.1%. The key steps involved in the synthesis are Jacobsen hydrolytic kinetic resolution, epoxide ring opening with 2-allyl-1, 3-dithiane, Yamaguchi esterification, and ring-closing metathesis (RCM).     

Analysis of hair components by nanoparticle-assisted laser desorption/ionization mass spectrometry imaging

Using a vertical hair-slice section, we compared the components of normal and damaged hair regions using two ionization methods, matrix-assisted laser desorption/ionization and nanoparticle-assisted laser desorption/ionization (Nano-PALDI) mass spectrometry. Nano-PALDI is useful for small-molecule and high spatial resolution (5 μm) analyses due to the lack of noise. Thus, clear images were obtained from thin hair samples. In Nano-PALDI mass spectrometry imaging, cystine and 18-methyleicosanoic acid as endogenous hair components localized in the cuticle and cortex and cuticle of normal hair, respectively. In contrast, both components were absent in damaged hair.     

Screening,isolation and selection of a potent lipase producing microorganism and its use in the kinetic resolution of drug intermediates

Lipases are ubiquitous enzymes that belong to family of serine hydolases with a wide variety of industrial applications. This study reports isolation, screening and identification of enantioselctive lipase producing microorganism for kinetic resolution of racemic alcohols. For this, we collected soil samples from different oil rich environments and we performed primary screening that was by carried out by using MSM-tributryin clear zone assay. The selected samples from first screen were subjected to secondary screening to distinguish lipase producing strains from esterase producing strains using p-nitrophenyl palmitate lipase assay. In tertiary screening, 16 lipase producing strains that were identified in secondary screening were employed for resolution of 5 different (RS)-alcohols. Out of all 16 lipase producing strains, only one strain selectively converted 3 racemic alcohols. Based on morphological, biochemical and physiological characteristics, and 16S rRNA gene sequencing, the strain was identified as Pseudomonas beteli. The strain was found to be S-selective and there been no reports on use of Pseudomonas beteli lipase for kinetic resolution of alcohols. The lipase activity was further increased by media optimization and by improving growth conditions, and production of lipase in shake flask study as well as in laboratory scale fermenter. The optimum time for enzyme production by Pseudomonas beteli was 96 ​h whereas cell mass growth was highest at 72 ​h. Optimum temperature and pH were 30 ​°C and 6, respectively. Beef extract (5 ​g/L), peptone (5 ​g/L), sodium chloride (5 ​g/L), yeast extract (1 ​g/L) and glucose (5 ​g/L) were found as optimum nutrition sources for the cell mass growth and lipase production by Pseudomonas sp. Overall, 3.4 times higher enzyme activity and 2.75 times higher cell mass growth were achieved in bioreactor in comparison to the shake flask study. Lipase having high titer was employed successfully for the kinetic resolution of several drug intermediates.     

雷达伺服系统中DAC位数和数字PWM位数的选择

雷达伺服系统是全闭环伺服系统。文中分析了D／A变换器（DAC）的工作特性以及在全闭环伺服系统中的应用特点。由于DAC和齿轮减速比都影响着伺服系统的开环增益,当系统开环增益一定时,DAC位数的实际作用和减速比的选择相互限制,在设计雷达伺服系统中需注意。文中同时指出,数字式PWM的实质也是一种DAC,它的位数选择同样遵循DAC的选择原则。     

谈我校的电工电子实习

为了提高学生对实验课程的认识,结合教学实践和当前电子技术发展的薪形势,井针对学生实践能力和创新能力的培养,我校电工电子实验中心针对“电气技术与自动控制”各专业统一开设了“电工电子实习”这门课程。本文主要介绍了“电工电子实习”课程开设的目的、内容和作用等,几年的实践所获成效表明,“电工电子实习”课程的开设有利于培养学生的动手能力以及提高学生的学习兴趣。     

改进的五阶WENO-Z+格式

WENO-ZWENO-Z$+\!$格式的性能提升依赖于新增项的作用,该项的作用是在WENO-Z格式的基础上进一步增大欠光滑子模板上的权重. 系数$\lambda$被设置用来调控该项的作用, 以避免负耗散. 本文指出了WENO-Z$+\!$格式的缺陷,其所采用$\lambda $的取值方式既不能充分发挥格式的潜力, 也未完全消除负耗散;提出$\lambda $的值应随当地流场数据变化,方能充分发挥新增项在降低数值耗散、提高分辨率上的潜力. 基于此,本文重新设计了$\lambda $的计算公式,该公式能自适应地调控新增项的作用: 只在欠光滑子模板上的权重容易过度增大的地方削弱该项的作用,以避免负耗散; 在其他地方则充分发挥新增项的作用,最大限度增大欠光滑子模板上的权重, 提高格式的分辨率.将使用该系数公式的新格式命名为WENO-Z++, 并对其数值性能进行了系统的研究.理论分析表明, 新格式在间断处具有基本无振荡(essentially non-oscillatory,ENO)特性和更低的数值耗散. 对近似色散关系(approximate dispersion relation,ADR)的研究表明,新格式有效地避免了因过度增大欠光滑子模板上的权重而带来的负耗散,其频谱特性也得到了显著提升.本文还推导了使新格式在极值点处也能保持最优阶的精度的参数设置.一系列求解Euler方程的数值试验表明,新格式的激波捕捉能力和对复杂流场结构的分辨率都显著优于原WENO-Z$+\!$格式.}     

Analysis of Vicinal Water in Soft Contact Lenses Using a Combination of Infrared Absorption Spectroscopy and Multivariate Curve Resolution

In this paper, we propose a new spectroscopic method to explore the behavior of molecules near polymeric molecular networks of water-containing soft materials such as hydrogels. We demonstrate the analysis of hydrogen bonding states of water in the vicinity of hydrogels (soft contact lenses). In this method, we apply force to hydrated contact lenses to deform them and to modulate the ratio between the signals from bulk and vicinal regions. We then collect spectra at different forces. Finally, we extracted the spectra of the vicinal region using the multivariate curve resolution-alternating least square (MCR-ALS) method. We report the hydration states depending on the chemical structures of hydrogels constituting the contact lenses.