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131.
132.
在氢化丁苯共聚物13C-NMR谱脂肪碳部分谱带归属的基础上,根据各谱带的主要来源,推导出六个二单元浓度的计算公式。计算出二单元、一单元的相对含量,各结构单元的数均序列长度、嵌段含量和其它结构参数。加氢前后的1H-和13C-NMR谱的组成计算结果基本一致。初步探讨了作为粘度指数改进剂的氢化丁苯共聚物微观结构与性能的关系,为合成提供了依据。 相似文献
133.
134.
超临界流体色谱流程设计及其应用 总被引:1,自引:1,他引:0
本文设计了多功能超临界流体色谱流程,流程中包括毛细管/微填充柱SFC,GC,计算机控制温度、压力、密度及信号采集、处理,配置有超临界流体萃取池,解决了超临界流体色谱分流口易堵问题。利用该流程,将石腊、DC-200气相色谱固定相、黄油、蜂蜡、救心油、红花油等样品进行超临界流体色谱分离。 相似文献
135.
We discuss an error estimation procedure for the global error of collocation schemes applied to solve singular boundary value problems with a singularity of the first kind. This a posteriori estimate of the global error was proposed by Stetter in 1978 and is based on the idea of Defect Correction, originally due to Zadunaisky. Here, we present a new, carefully designed modification of this error estimate which not only results in less computational work but also appears to perform satisfactorily for singular problems. We give a full analytical justification for the asymptotical correctness of the error estimate when it is applied to a general nonlinear regular problem. For the singular case, we are presently only able to provide computational evidence for the full convergence order, the related analysis is still work in progress. This global estimate is the basis for a grid selection routine in which the grid is modified with the aim to equidistribute the global error. This procedure yields meshes suitable for an efficient numerical solution. Most importantly, we observe that the grid is refined in a way reflecting only the behavior of the solution and remains unaffected by the unsmooth direction field close to the singular point. 相似文献
136.
137.
Ying Tan 《The Journal of VLSI Signal Processing》2002,32(1-2):45-54
In this paper, we propose a new approach for signal detection in wireless digital communications based on the neural network with transient chaos and time-varying gain (NNTCTG), and give a concrete model of the signal detector after appropriate transformations and mappings. It is well known that the problem of the maximum likelihood signal detection can be described as a complex optimization problem that has so many local optima that conventional Hopfield-type neural networks fail to solve. By refraining from the serious local optima problem of Hopfield-type neural networks, the NNTCTG makes use of the time-varying parameters of the recurrent neural network to control the evolving behavior of the network so that the network undergoes the transition from chaotic behavior to gradient convergence. It has richer and more flexible dynamics rather than conventional neural networks only with point attractors, so that it can be expected to have much ability to search for globally optimal or near-optimal solutions. After going through a transiently inverse-bifurcation process, the NNTCTG can approach the global optimum or the neighborhood of global optimum of our problem. Simulation experiments have been performed to show the effectiveness and validation of the proposed neural network based method for the signal detection in digital communications. 相似文献
138.
Lu Chuanrong 《数学年刊B辑(英文版)》1997,18(1):71-78
Let $\{\xi_{\bold t}, {\bold t}
\in {\bold Z}^d\}$ be a nonuniform $\varphi$-mixing strictly stationary
real random field with
$E\xi_{\bold 0}=0, E|\xi_{\bold 0}|^{2+\delta}<\infty$ for some
$0<\delta<1$. A sufficient
condition is given for the sequence of partial sum set-indexed process
$\{Z_n(A),\ A\in \Cal A\}$ to converge to Brownian motion. By a direct
calculation, the author shows
that the result holds for a more general class of set index ${\Cal A}$, where
${\Cal A}$ is assumed only to have the metric entropy exponent $r, 0相似文献
139.
This paper deals mainly with generalizations of results in finitary combinatorics to infinite ordinals. It is well-known that for finite ordinals ∑bT<αβ is the number of 2-element subsets of an α-element set. It is shown here that for any well-ordered set of arbitrary infinite order type α, ∑bT<αβ is the ordinal of the set M of 2-element subsets, where M is ordered in some natural way. The result is then extended to evaluating the ordinal of the set of all n-element subsets for each natural number n ≥ 2. Moreover, series ∑β<αf(β) are investigated and evaluated, where α is a limit ordinal and the function f belongs to a certain class of functions containing polynomials with natural number coefficients. The tools developed for this result can be extended to cover all infinite α, but the case of finite α appears to be quite problematic. 相似文献
140.
M. M. Moustafa 《Journal of Thermal Analysis and Calorimetry》1997,50(3):463-471
The oxime and Schiff's base of N-furoylphenylhydroxylamine form complexes with Co2+, Cu2+, Zn2+ and Fe3+. These complexes were studied by means of the UV — Vis. spectra of nujol mulls, electron spin resonance (ESR) spectra and magnetic susceptibility to determine their stereochemistry. The complexes were characterized via elemental analyses, molar conductivities and thermogravimetric analyses. Organic reagents were used for the gravimetric determination of Co2+, Cu2+ and Fe3+ through the precipitation of their complexes. The compounds were also used for separation of a binary mixture of Cu2+ and Cu2+. Interferences were studied. 相似文献