Characteristic X-ray detector: In-situ imaging of radioactive contaminant distributions

The characteristic X-ray detector (CXRD), a CsI(Tl) scintillator with a 50-mm diameter, is a directional X-ray sensor that measures characteristic X-rays from radioactive material, such as ¹³⁷Cs, and identifies the direction of radioactive contamination. We evaluated a CXRD and visualized the distribution of radioactivity in the contaminated area near the Fukushima Dai-ichi nuclear power station, where the ambient dose equivalent rate was 2.1 μSv/h at 1 m above ground level. We found a good correlation between the characteristic X-ray fluxes and the distribution of radioactive contaminants with a 0.823 Pearson product–moment correlation coefficient.     

Application of Non‐Stop‐Flow Differential Pulse Voltammetry at a Tubular Detector of Silver Solid Amalgam for Electrochemical Determination of Lomustine (CCNU)

An application of the flow differential pulse voltammetry with tubular detector based on silver solid amalgam for determination of antineoplastic drug lomustine in pharmaceutical preparations is presented. The highest sensitivity was obtained in [0.10 mol dm^?3 MES; 2.00 mol dm^?3 NaCl; pH 6.0]:EtOH (9 : 1) with flow rate 0.50 mL min^?1, and the magnitude of the modulation amplitude ?0.070 V. The calibration dependence was linear in the range 1×10^?6–1 × 10^?4 mol dm^?3 (R²=0.999). The limit of detection was 1.5×10^?7 mol dm^?3. This method was successfully used for determination of lomustine in real samples of chemotherapy drug CeeNU Lomustine 40 mg.     

镍修饰WO3膜光电化学氧化水的研究

在强碱性溶液中低电压低电流条件下在W基底上经阳极氧化得到致密WO3层,而后在酸性条件下在WO3表面经光辅助电化学还原沉积镍,所获得的复合电极具有优异的光电化学氧化水的活性和稳定性.SEM,EDX,XPS和TEM等表征表明复合电极中具有体心立方结构的W基底经阳极氧化形成了具有单斜结构的WO3层,表面修饰的镍物种以Ni(OH)2形式存在.光电化学实验表明WO3层对可见光具有良好的光响应,表面修饰镍后,光电氧化水的起始电位显著降低,电极的稳定性也得以提高.     

微流控芯片简易安培检测器的制作及对烟酰胺片中烟酰胺的测定

搭建了微流控芯片简易安培检测器,并用于市售药品烟酰胺片中烟酰胺含量的测定。由碳纳米管微圆盘电极和钛管组成集成双电极,中间的碳纳米管微圆盘电极作为安培检测的工作电极,外套的钛管既作为安培检测的对极,又充当分离高压电源的地极,使其结构更加简化和微型化。优化了缓冲溶液种类、浓度,分离电压及进样时间等实验条件。结果表明,在10 mmol·L-1磷酸盐缓冲液(pH 7.8)中,进样10 s,在2.0kV电压下分离,烟酰胺在2 min内可实现较好的分离和检测,其线性范围为10~600μmol·L-1,检出限(S/N=3)为5.0μmol·L-1,相对标准偏差(RSD)为3.0%,平均加标回收率为99.1%。该装置实现了微型化和集成化,并具有检测灵敏度较高、选择性好、成本低等特点,可用于药品的质量控制。     

Efficient implementation of 3D filter for moving object extraction

In this paper the design and implementation of Multi-Dimensional (MD) filter, particularly 3-Dimensional (3D) filter, are presented. Digital (discrete domain) filters applied to image and video signal processing using the novel 3D multirate algorithms for efficient implementation of moving object extraction are engineered with an example. The multirate (decimation and/or interpolation) signal processing algorithms can achieve significant savings in computation and memory usage. The proposed algorithm uses the mapping relations of z-transfer functions between non-multirate and multirate mathematical expressions in terms of time-varying coefficient instead of traditional polyphase de- composition counterparts. The mapping properties can be readily used to efficiently analyze and synthesize MD multirate filters.     

线阵CCD参量测试系统

根据CCD光电参量的定义和测试方法,设计一种线阵CCD参量测试系统.硬件上该系统以LED为光源,用CPLD驱动线阵CCD采集光线,由USB接口传输数据;软件上用Veriolog HDL开发CCD驱动程序,keil C开发USB接口固件程序,VC 开发USB上位机驱动程序、界面操作及数据处理程序.该系统能够方便地观察CCD的驱动时序及输出信号,实现主要光电参量的测量,并且结构简单、操作方便,适宜高校实验室应用.     

一种鲁棒的均值漂移与彩色特征点提取相结合的面部跟踪算法

针对复杂背景中的多人脸跟踪问题,提出一种均值漂移与彩色特征点提取相结合的面部跟踪算法.手动选取要跟踪的面部区域,并利用彩色Harris探测器进行特征点提取,然后根据肤色的色度信息,利用均值漂移算法粗略定位人脸的位置,之后对这个区域提取特征点,与其前提取的特征点进行匹配,满足约束条件的区域即为要跟踪的人脸区域.实验表明,该算法可以排除近肤色物体的干扰并可以在多人脸发生重叠的情况下保持稳定跟踪.     

一种高性能的金属探测门信号处理电路的设计

设计了基于正交解调和窄带滤波技术的信号处理电路,它使用模拟开关作为乘法器,实现解调,并使用一种性能优异的窄带滤波电路对解调结果进行滤波和放大.整个电路具有高增益、高灵敏度、强抗干扰能力、低成本等优点,可有效提高金属探测门的性能.     

ACM-02型COD仪分光光度法快速测定废水中COD

水样在165℃下密封消解15 min,用ACM-2型COD仪测定.实验结果表明,本法既快速又节省试剂,加标回收率和相对标准偏差均能满足质量控制要求,具有一定适用性.