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61.
《Magnetic resonance in chemistry : MRC》2018,56(8):775-781
Recently, it has been reported that large nJCC correlations can sometimes be observed in 1,1‐ADEQUATE spectra with significant intensity, which opens the possibility of structural misassignment. In this work, we have focused on pyrimidine‐based compounds, which exhibit multiple bond correlations in the 1,1‐ADEQUATE experiment as a consequence of 3JCC coupling constants greater than 10 Hz. Results are supported by both the experimental measurement of 3JCC coupling constants in question using J‐modulated‐ADEQUATE and density functional theory calculations. 相似文献
63.
64.
We study stable blow-up dynamics in the generalized Hartree equation with radial symmetry, which is a Schrödinger-type equation with a nonlocal, convolution-type nonlinearity: First, we consider the -critical case in dimensions and obtain that a generic blow-up has a self-similar structure and exhibits not only the square root blowup rate , but also the log-log correction (via asymptotic analysis and functional fitting), thus, behaving similarly to the stable blow-up regime in the -critical nonlinear Schrödinger equation. In this setting, we also study blow-up profiles and show that generic blow-up solutions converge to the rescaled , a ground state solution of the elliptic equation . We also consider the -supercritical case in dimensions . We derive the profile equation for the self-similar blow-up and establish the existence and local uniqueness of its solutions. As in the NLS -supercritical regime, the profile equation exhibits branches of nonoscillating, polynomially decaying (multi-bump) solutions. A numerical scheme of putting constraints into solving the corresponding ordinary differential equation is applied during the process of finding the multi-bump solutions. Direct numerical simulation of solutions to the generalized Hartree equation by the dynamic rescaling method indicates that the is the profile for the stable blow-up. In this supercritical case, we obtain the blow-up rate without any correction. This blow-up happens at the focusing level , and thus, numerically observable (unlike the -critical case). In summary, we find that the results are similar to the behavior of stable self-similar blowup solutions in the corresponding settings for the nonlinear Schrödinger equation. Consequently, one may expect that the form of the nonlinearity in the Schrödinger-type equations is not essential in the stable formation of singularities. 相似文献
65.
In our previous two works, we studied the blow-up and lifespan estimates for damped wave equations with a power nonlinearity of the solution or its derivative, with scattering damping independently. In this work, we are devoted to establishing a similar result for a combined nonlinearity. Comparing to the result of wave equation without damping, one can say that the scattering damping has no influence. 相似文献
66.
Lintao Yang Author VitaeHao JiangAuthor Vitae Sai Wang Author VitaeLin Wang Author Vitae Yuan Fang Author Vitae 《Ad hoc Networks》2012,10(3):524-535
We use a counting process representation of the pairwise contact process to analyze pairwise contact patterns. Studying two real-world traces, we find that the pairwise contact patterns have three characteristics. First, human contact patterns are influenced by daily and weekly cycles of activity. Second short time intervals with intensive contact event (bursts) are separated by long periods with few contact events. Third, the pairwise contact process exhibits long range dependence. We introduce a Markov modulated Poisson process (MMPP) as a flexible model for pairwise contact process exhibiting both regular structure and irregular bursts of activity. Using standard statistical techniques, we demonstrate that the proposed model is consistent with the empirical data. Our work has significant implication for mobility modeling and performance analysis in human contact networks. 相似文献
67.
Single crystals of a new silicate carbonate, K2Ca[Si2O5](CO3), have been synthesized in a multi-components hydrothermal solution with a pH value close to neutral and a high concentration of a carbonate mineralizer. The new compound has an axial structure (s.g. P6322) with unit cell parameters a = 5.04789 (15), c = 17.8668 (6) Å. Pseudosymmetry of the structure corresponds to s.g. P63/mmc which is broken only by one oxygen position. The structure consists of two layered fragments: one of the type of the mineral kalsilite (KAlSiO4) and the other of the high-temperature soda-like α-Na2CO3, Ca substituting for Na. The electro-neutral layer K2[Si2O5] (denoted K) as well as the layer Ca(CO3) (denoted S) may separately correspond to individual structures. In K2Ca[Si2O5](CO3) the S-K layers are connected together via Ca-O interactions between Ca atoms from the carbonate layer and apical O atoms from the silicate one, and also via K-O interlayer interactions. A hypothetical acentric structure, sp.gr. P-62c, is predicted on the basis of the order-disorder theory. It presents another symmetrical option for the arrangement of K-layers relative to S-layers. The K,Ca-silicate-carbonate powder produces a moderate SHG signal that is two times larger that of the α-quartz powder standard and close to other silicates with acentric structures and low electronic polarizability. 相似文献
68.
We study optical analogues of higher-order Dirac solitons (HODSs) in binary waveguide arrays. Like higher-order solitons obtained from the well-known nonlinear Schrödinger equation governing the pulse propagation in an optical fiber, these HODSs have amplitude profiles which are numerically shown to be periodic over large propagation distances. At the same time, HODSs possess some unique features. Firstly, the period of a HODS depends on its order parameter. Secondly, the discrete nature in binary waveguide arrays imposes the upper limit on the order parameter of HODSs. Thirdly, the order parameter of HODSs can vary continuously in a certain range. 相似文献
69.
针对变极距电容位移传感器提出了一种双频激励方法。同时采用低频、高频正弦电压源激励平板发射电极,通过电容耦合效应将极距变化转换为双频调幅信号,并通过高阻抗缓冲、带通滤波、精密整流电路获得双路位移调制电压信号。采用数字信号处理器(DSP)同步采集双路位移调制电压信号以及参考位移信号,对高、低频激励方式下的位移检测分辨率、纹波、动态响应速度等性能进行了对比分析。实验结果表明:双频激励时,通道间耦合作用较小,低频激励方式在位移分辨率、测量范围、线性度、抗干扰等指标上显著优于高频激励;高频激励在动态响应速度上具有明显优势。 相似文献
70.
为减小压电陶瓷的迟滞非线性对系统跟踪精度的影响,该文采用经典的存在逆解析的PI迟滞模型对压电陶瓷的迟滞特性进行建模,将PI模型的逆模型用于压电陶瓷的前馈控制算法中,然后设计了神经元比例、积分、微分(PID)反馈控制算法,将前馈控制算法与神经元PID反馈控制算法结合得到了压电陶瓷的复合控制算法。将仅含前馈的控制算法和复合控制算法在压电陶瓷的控制器上执行,实验结果表明,仅含前馈的控制算法的跟踪误差为1.256μm,而复合控制算法的跟踪误差仅为0.092μm,该复合控制算法使跟踪精度提高了1.164μm。 相似文献