一种加载铁氧体磁环的高功率宽带巴伦

针对高功率天线的差分馈电和阻抗匹配问题,文中提出了一种基于同轴线结构加载铁氧体磁环的宽 带巴伦模型。双同轴线具有阻抗变换功能和较好的功率承载能力,铁氧体磁环改善了巴伦在低频时的输入匹配和 两个输出端口不平衡度。仿真和实测表明,此巴伦在0. 05~1. 24 GHz 内回波损耗低于-10 dB,去除3. 0 dB 系统插损 后单端插入损耗在1. 5 dB 以内,两端输出的相位不平衡度在5°以内,幅度不平衡度在2%以内。通过分析巴伦的电 磁热损耗场、温度场和应力形变场,验证了巴伦在高功率馈电下的工作性能,结果表明此巴伦在工作频带内能够承 受500 W 的功率。     

等离子体限幅器对雷电防护效果的试验分析北大核心CSCD

雷电对于各类装备及民用系统的电子设备有着极大的破坏作用,引起射频系统损坏的主要为感应雷,而现有的设备无法满足射频系统的防雷需求。文章对微波防护用等离子体限幅器的雷电防护特性进行了研究并开展了相关试验,结果表明,等离子体限幅器可以起到雷电防护的作用,对于感应雷电波形的幅值及波形均有着一定的限制,在等离子限幅器后接入PIN限幅器所形成的级联防护器件对后方的电路起到了有效的防护作用。     

硅基片上集成二维光控多波束形成的研究

传统雷达系统在当今日益复杂的电磁环境中面临严重挑战,而集成微波光子学技术可突破传统雷达的技术瓶颈,具有大带宽、高分辨率、高复用度、高集成化等技术优势。本文基于集成微波光子技术,研制了一款硅基集成二维光控多波束形成系统样机,提出了一种基于二氧化硅平面光波导的片上集成二维光控多波束形成系统架构,结合流片加工平台完成了关键光芯片的设计流片和封装测试,最终完成系统样机整机联调测试,并对实验结果进行理论计算处理,验证了硅基集成波束形成系统的关键性能指标。系统具有大瞬时带宽、二维同时多波束、各波束多波位独立扫描的能力,与此同时兼具硅基光子集成技术的小型化、轻量化、低成本等优势,试验结果验证了集成微波光子技术应用于雷达系统的先进性和应用潜力。     

一种Ku波段综合馈电多功能板的研制

基于多层微波数字复合基板层叠互联技术,研制的Ku波段综合馈电多功能板集成了射频收发网络、电源分配网络、阵面波控及波控分配网络,主要负责16个片式T/R组件的功率分配与合成,同时为各T/R组件提供电源及控制信号。文中对多功能板的架构设计、工作原理进行了说明,重点介绍了各微波垂直互联电路和射频收发网络的设计,最后加工并测试了验证样件,测试结果良好。收发网络总口驻波＜1.9,分口驻波＜1.3,插损＜16 dB,相邻端口的隔离度＞20 dB,且幅度一致性≤0.602 dB,相位一致性≤6.429°。工程应用可行性和实用性得到了验证。     

白藜芦醇分子的转动惯量和电偶极矩

通过分子轨道理论和杂化轨道理论推断出较稳定的白藜芦醇分子是平面型分子,然后根据白藜芦醇分子结构特点计算了该化合物的一种稳定异构体的转动惯量,用矢量合成法计算了其电偶极矩,为微波辅助白藜芦醇萃取理论研究提供转动惯量和电偶极矩的数据.     

Solid-supported Hantzsch—Biginelli reaction for syntheses of pyrimidine derivatives

The microwave-assisted dry media technology was utilized for the synthesis of some novel derivatives in the Hantzsch—Biginelli reaction. In this eco-friendly approach, the usage of organic solvents and hazardous reagents resulting in corrossion of materials was minimized, giving high yields of products within a short reaction time.     

Micro construction of poly(epsilon-caprolactone)/poly(L-lactic acid) blend film by solution casting under microwave irradiation

The micro construction of poly(epsilon-caprolactone) (PCL) and poly(L-lactic acid) (PLLA) blend films fabricated by solution casting under microwave irradiation was investigated by selective enzymatic degradation and scanning electron microscopy (SEM). The results were totally different from the blends obtained by conventional methods. The blend was more homogeneous and the PCL continuous phase more compact as no spherulites and tiny zone separation were observed from the film surface and no PCL network was observed inside the film, and the degradation of a PCL plank by Pseudomonas lipase was significantly retarded. The distributed PLLA micro spheres were enlarged and amorphous. The thermal behavior of the blend by microwave heating revealed that PCL and PLLA underwent a melting process, which induced the variations of the PCL phase and PLLA spheres. The weight loss caused by degradation of the PCL/PLLA blend obtained by conventional methods (B50c) is greater than that of the blend obtained by microwave methods (B50m), which reflects the change in morphology from a loose PCL network (B50c) to a dense PCL plank (B50m).     

微波辐射下三组分“一锅法”合成5-芳基-1,5,6,7,8,9-六氢化-2H-吡唑[5,4-b]并喹啉-6-酮

在微波辐射下以芳醛、1,3-环己二酮或达米酮和氨基吡唑为原料, 用乙二醇作能量转移剂, 三组分“一锅法”快速合成了一系列吡唑[5,4-b]并喹啉类化合物. 该方法速度快(30～90 s), 产率高(88%～98%), 环境友好. 产物结构通过红外光谱、核磁共振谱和元素分析证实, 化合物4e的单晶经X射线衍射分析, 进一步确证了产物结构.     

微波消解-氢化物发生原子荧光法测定塑料原料及其制品中的砷、汞

采用微波消解进行样品前处理，以硫脲为预还原剂，用氢化物发生原子荧光法测定塑料原料及其制品中的砷、汞。测定砷和汞的线性范围均为0～8μg／L，砷、汞的检出限分别为0．005、0．076μg／L，测定结果的相对标准偏差分别为4.96％～7．38％、2．94％～7．20％(n=6)，回收率分别为92．0％～103．2％、92．0％～98.0％。     

Microwave assisted low temperature synthesis of sodium zirconium phosphate (NaZr<Subscript>2</Subscript>P<Subscript>3</Subscript>O<Subscript>12</Subscript>)

Sodium zirconium phosphate [NaZr₂P₃O₁₂], a potential ceramic matrix for fixation of high level nuclear waste, was synthesized by heating the mixture of sodium carbonate [Na₂CO₃], zirconyl nitrate hydrate [ZrO(NO₃)₂·5H₂O] and ammonium dihydrogen phosphate [NH₄H₂PO₄] in air, in a resistance heated furnace and a microwave heating system respectively in the temperature range 450 to 650°C. The mixture heated for 1 h in a resistance furnace at 450°C yielded a poorly crystalline NaZr₂P₃O₁₂ [NZP]. Increasing the temperature to 650°C produced a highly crystalline product. The same mixture heated in a microwave oven at 450°C for 1 h however, yielded the most crystalline NZP.In an alternate method, the mixture of sodium dihydrogen phosphate (NaH₂PO₄), zirconium dioxide (ZrO₂) and diammonium hydrogen phosphate [(NH₄)₂HPO₄] heated in resistance furnace at 650°C for the same period did not react in air. It also did not yield the pure product at 450°C when heated in microwave assembly for 1 h.The authors thank the Board of Research in Nuclear Sciences (BRNS) of the Department of Atomic Energy (DAE) for the financial support for this work under the project No. 2000/37/19/BRNS/1959 dtd09-02-02.