Dynamic Visualization of Free Radicals at Single Oxygen Bubbles using Chemiluminescence

The generation of free radicals is a key process in the formation and the collapse of the bubbles in water, however, the direct and dynamic observation of the radicals in this process at single bubbles has never been achieved. Here, the hydroxyl (OH^.) and oxygen (O₂^.−) radicals at single oxygen bubbles are continuously traced using chemiluminescence (CL), in which these radicals at the bubble react with the surrounding luminol in the solution emitting the light. Varied increase trends of luminescence are observed in the generation of a bubble, floating, short parking at the water/air interface and the final explosion, revealing the complexity in the distribution of radicals at the bubble unprecedentedly. Despite more radicals are observed at the bubble generated at a deep position under the water for the stabilization, almost the same amount of radicals are included in the bubbles that is independent on the water pressure during the production of the bubble. This rich information collected from the dynamic study of bubbles illustrates the complicated generation and distribution process of radicals at the bubbles, and will facilitate the understanding of the function about the bubbles.     

光学观测中太阳夹角的分析与计算

对影响光学观测效果的太阳夹角计算方法进行了研究。首先给出了太阳夹角的定义及计算公式。然后重点研究了太阳视位置的计算方法,比较了几种赤纬角计算方法,给出了一种改进的时角计算方法,实现了高精度的太阳视位置计算,并对其计算精度进行了分析。最后提出了在实际光学观测应用中的太阳夹角计算算法。实验表明,太阳视位置计算精度比传统数值近似方法高一个数量级,能够满足光学观测中太阳光照分析的需要。     

One-dimensional migration of interstitial clusters in SUS316L and its model alloys at elevated temperatures

For self-interstitial atom (SIA) clusters in various concentrated alloys, one-dimensional (1D) migration is induced by electron irradiation around 300 K. But at elevated temperatures, the 1D migration frequency decreases to less than one-tenth of that around 300 K in iron-based bcc alloys. In this study, we examined mechanisms of 1D migration at elevated temperatures using in situ observation of SUS316L and its model alloys with high-voltage electron microscopy. First, for elevated temperatures, we examined the effects of annealing and short-term electron irradiation of SIA clusters on their subsequent 1D migration. In annealed SUS316L, 1D migration was suppressed and then recovered by prolonged irradiation at 300 K. In high-purity model alloy Fe-18Cr-13Ni, annealing or irradiation had no effect. Addition of carbon or oxygen to the model alloy suppressed 1D migration after annealing. Manganese and silicon did not suppress 1D migration after annealing but after short-term electron irradiation. The suppression was attributable to the pinning of SIA clusters by segregated solute elements, and the recovery was to the dissolution of the segregation by interatomic mixing under electron irradiation. Next, we examined 1D migration of SIA clusters in SUS316L under continuous electron irradiation at elevated temperatures. The 1D migration frequency at 673 K was proportional to the irradiation intensity. It was as high as half of that at 300 K. We proposed that 1D migration is controlled by the competition of two effects: induction of 1D migration by interatomic mixing and suppression by solute segregation.     

QUANTIFICATION OF SHEAR DAMAGE EVOLUTION IN ALUMINIUM ALLOY 2024T3

Shear damage may occur in the process of metal machining such as blanking and cutting, where localized shear deformation is developed. Experimental findings indicate that microscopic shear damage evolution in aluminium alloy 2024T3 (A1 2024T3) is a multi-stage mechanism, including particle cracking, micro-shear banding, matrix microcracking and coalescence of microcracks. This study is an attempt to use a set of equations to describe the multi-stage shear damage evolution in Al 2024T3. The shear damage variables in terms of multi-couple parameters of a power-law hardening material have been defined. An evolution curve of shearing damage has been calculated from experimental data. The values of the shear damage variable at different stages of damage have also been calculated. By making use of the findings, the relation between the microscopic shear damage evolution and the macroscopic shear response of the material has been discussed.     

红外遥感技术在民用对地观测卫星中的应用现状（下）

利用卫星遥感技术对地球资源、海洋和大气等环境状况进行监测,可以为人类生存环境提供预测信息和安全保障。红外遥感仪器是对地观测卫星的主要探测载荷。随着红外探测器性能和系统集成技术的不断提高,空间红外遥感仪器的探测能力也得到了长足发展。介绍了近五年各国相继发射的各类高性能对地观测卫星,总结了主要红外遥感仪器的应用状况、功能和特性,并对其未来的发展趋势进行了分析。     

二元光学在光学观测轰炸瞄准中的应用研究

光学观测瞄准是大中型轰炸机主要的对地攻击瞄准方式,其光学系统一般采用望远式光学系统,这就要求光学系统能满足可见光和近红外光两个光谱波段。根据国内大中型轰炸机光学观测瞄准系统的主要缺陷,结合光学观测瞄准的实际,探讨了基于二元光学的光学观测系统的组成结构和瞄准原理,分析了可见光波段混合目镜的光学性能、谐衍射物镜的衍射效率以及近红外光波段光学系统的像质,推导了横偏棱镜调平误差引起的瞄准误差的数学表达式,并对设计的合理性进行了验证。     

番荔枝属不同品种叶表面微形态的电镜观察

应用扫描电子显微镜对番荔枝属九个番荔枝品种的叶表面角质、蜡质、表皮毛、气孔等微形态进行了观察比较.结果显示：它们之间的叶表面表皮毛、角质、蜡质和气孔等微形态均有较大的差异.秘鲁番荔枝、AP杂交番荔枝、无核番荔枝上下表面均具有单列丝状毛,气孔只分布于下表面;普通番荔枝、圆滑番荔枝、粗鳞番荔枝叶表面均无表皮毛;秘鲁番荔枝、AP杂交番荔枝、普通番荔枝、粗鳞番荔枝上下表皮角质呈不规则的岛状突起,而圆滑番荔枝、无核番荔枝表面角质较平,角质膜形状不甚清晰;以上所述番荔枝叶表面都覆盖有密厚的针晶状蜡被;除圆滑番荔枝的气孔有副卫细胞外,其它气孔只有保卫细胞而无副卫细胞;刺番荔枝、山刺番荔枝、牛心番荔枝的叶表皮毛为短棍棒状,其表皮角质细胞呈乳突状或波状突起;山刺番荔枝的棒状毛顶端钝圆,而刺番荔枝与牛心番荔枝的棒状毛顶端尖锐;刺番荔枝和山刺番荔枝只有下表皮才具有棒状毛,其气孔形状近似圆形,孔口略内陷于表皮层,牛心番荔枝表面角质呈不规则波状突起,气孔细长稍突.由于这些不同的叶表面微形态是长期受各物种原产地的气候、环境条件影响所形成的,因此研究番荔枝品种的叶表面微形态结构,对正确引种和推广番荔枝果树种植有着重要的意义.     

电离层垂直探测中扰动观测模式研究

电离层高频反射回波的多普勒频移观测是研究电离层扰动的一个重要方法.利用电离层垂直探测中的组合脉冲控制和回波相位测量分析方法,开发并实现了一种电离层扰动观测模式.实验观测表明,新开发的观测模式在电离层高频反射回波为窄带信号的情况下,可实时获得高精度多普勒频高图,并给出电离层扰动速度的时空变化曲线,能够满足电离层扰动观测研究的需要.     

用于测量亚硝酸的长光程吸收光谱仪的研制

This article has been retracted at the request of the authors.     

花岗岩单轴压缩侧向变形及脆性破坏机制实验研究

为研究花岗岩侧向变形及脆性破坏机制,对花岗岩试件进行单轴压缩实验。利用动态应变采集系统、数字散斑相关方法(DSCM)和显微观测手段,记录并分析花岗岩试件在单轴压缩过程中的宏观侧向应变、局部侧向应变以及破裂面形貌,并与水泥砂浆试件的破坏过程对比,讨论了花岗岩脆性破坏机制。实验与分析结果表明:(1)花岗岩试件在加载初期发生侧向收缩变形,产生并发展于压密阶段,消失于线弹性阶段初期,这主要由于试件内部裂纹闭合造成的;此后,宏观侧向应变持续增长,当侧向应变与轴向应变之比接近0.5时试件破坏;(2)在峰值载荷前很长一段时间内,局部侧向应变在一定范围内波动,临近试件破坏时局部侧向应变最大值和最小值均出现较大幅度的波动,二者差值迅速增大,试件不均匀程度增大,最终导致试件破坏;(3)在峰值载荷前有无塑性屈服阶段是峰值载荷后脆性破坏程度的重要影响因素,而宏观裂纹的贯通程度是峰值载荷后应力降大小的决定因素。