Antisolvent crystallization of aqueous ammonium dihydrogen phosphate solutions by addition of acetone at different rates

Results of an investigation of in situ measurements of laser‐beam intensity I_s and I_m transmitted through aqueous ammonium dihydrogen phosphate (ADP) solutions saturated at 30 °C and water, respectively, and temperature T_s of solution and T_m of water during feeding of antisolvent acetone at different rates R_A, using an indigenously designed experimental setup, are presented and discussed. It was found that: (1) for the measurement of MSZW, defined as the maximum volume fraction of acetone content Δx_max in the solution, obtained from temperature measurements are more reliable than transmitted laser‐beam intensity measurements for solutions, (2) two minima ΔT_min1 and ΔT_min2 associated with endothermic reactions, separated by a maximum ΔT_max due to exothermic reactions appear in the plots of temperature difference ΔT = T_s−T_m against acetone feeding time t, and (3) in the ΔT(t) plots there are time intervals Δt of constant rates R_T of increase in ΔT of aqueous ADP solutions, and these values of R_T increase linearly with acetone feeding time rate R_A. The experimental data on the observed dependence of MSZW on antisolvent feeding rate R_A, the appearance of minima ΔT_min1 and ΔT_min2 and maximum ΔT_max and their dependence on R_A, and the relationship between R_T and R_A are discussed from consideration of processes of nucleation and growth of crystallites.     

自动动态补偿功能改善酸蚀蚀刻不均匀性问题

在酸蚀制程中,由于其蚀铜量较大,蚀刻线生产时蚀刻速度较慢,导致蚀刻不均匀性对线路制作存在很大影响,为改善蚀刻不均匀性的问题,采用奥宝公司专门开发的可制造性设计功能----自动动态补偿(Dynamic Etch Compensation),根据不同的间距设置不同的线宽补偿量,来确保蚀刻后线宽的一致性。     

三相电压型PWM整流器控制新技术的研究

根据电压型PWM整流器在同步旋转dq坐标系中建立的整流器电流控制数学模型,基于电流前馈解耦,解决了有功电流和无功电流互为耦合问题。为克服直流电压响应较慢、抗扰性较差的不足,提出了采用电流内环、基于滑模控制的电压外环电压型PWM整流器的新控制策略。由于采用滑模控制的电压外环,提高了整流器直流电压跟踪和电流跟踪能力,使系统具有响应快、稳定性好、抗负载扰动能力强的优点。文中给出了系统控制器的设计方法。通过正常负载及负载扰动情况下的计算机仿真,证明了新控制策略的可行性。     

一种便携式发电箱的设计

在外旅游或者没有电源的情况下,便携式光伏发电箱可以实现手机、手电筒、剃须刀等能量补给及夜晚照明。文章主要介绍了光伏发电箱的太阳能发电系统,该系统由光伏电池、蓄电池、控制器、逆变器、数据采集板、上位机等几部分组成;文中对该系统各部分的功能和相互联系进行了分析;重点叙述逆变器的设计,包括电路结构、DSP软件的设计、PWM波形的产生原理;通过数据采集板和上位机可实时监测系统的运行状况,具有一定的市场潜力。     

基于模糊度和噪声水平的图像质量评价方法

针对图像质量评价的重要性,提出了一种新的无参考图像质量客观评价方式。算法考虑了模糊度与噪声水平两方面,用平均边缘宽度衡量图像的模糊度,通过比较去噪前后的图像预测图像受噪声污染的程度,最后通过两者的综合作为无参考图像质量评价指标。实验结果表明:将模糊度和噪声评价相结合,具有很强的抗噪性和广泛的适用范围;与峰值信噪比(PSNR)和结构类似性(SSIM)等算法比较,本文算法可以很好地区分各种失真类型图像的质量好坏,其结果接近人眼的主观感受。     

Cs原子磁力仪共振谱线宽度的研究

介绍了Cs原子无自旋交换弛豫磁力仪(Cs-SERFM)的工作原理;分析了Cs泡温度105℃条件下,缓冲气体He的压强对Cs原子横向弛豫及线宽的影响,给出了惰性气体He的最佳压强为350×133.3 Pa;讨论了共振谱线的宽度与温度之间的关系,在105℃时Cs-SERFM谱线宽度仅为3.7 Hz。     

Fabrication of Sub‐10 nm Metallic Lines of Low Line‐Width Roughness by Hydrogen Reduction of Patterned Metal–Organic Materials

The fabrication of very narrow metal lines by the lift‐off technique, especially below sub‐10 nm, is challenging due to thinner resist requirements in order to achieve the lithographic resolution. At such small length scales, when the grain size becomes comparable with the line‐width, the built‐in stress in the metal film can cause a break to occur at a grain boundary. Moreover, the line‐width roughness (LWR) from the patterned resist can result in deposited metal lines with a very high LWR, leading to an adverse change in device characteristics. Here a new approach that is not based on the lift‐off technique but rather on low temperature hydrogen reduction of electron‐beam patterned metal naphthenates is demonstrated. This not only enables the fabrication of sub‐10 nm metal lines of good integrity, but also of low LWR, below the limit of 3.2 nm discussed in the International Technology Roadmap for Semiconductors. Using this method, sub‐10 nm nickel wires are obtained by reducing patterned nickel naphthenate lines in a hydrogen‐rich atmosphere at 500 °C for 1 h. The LWR (i.e., 3 σ_LWR) of these nickel nanolines was found to be 2.9 nm. The technique is general and is likely to be suitable for fabrication of nanostructures of most commonly used metals (and their alloys), such as iron, cobalt, nickel, copper, tungsten, molybdenum, and so on, from their respective metal–organic compounds.     

DSP在交流异步电动机变频调速中的应用

以三相交流异步电动机为控制对象,以TMS320LF2407A处理器为控制部件,通过SVPWM控制方法对交流电机实现恒压频比控制。试验表明,该系统控制性能和精度良好。     

层状磁电复合基板微带天线设计及应用

 本文提出一种新的小型化、宽频带微带天线.采用以层状磁电复合材料为基板的微带天线形式,推导了设计公式并给出计算结果.与介质基板矩形微带天线相比,该磁电复合基板天线的尺寸缩小了40%多,而带宽约为6%,是介质基板天线4倍.     

A novel optical polarimeter based on the signal width measurement of the waveform

For the optical polarimeter based on the structure of polarizer–Faraday modulator–analyzer, a novel method of optical rotation measurement was proposed by the waveform analysis of optical intensity signals. The calculation method of the optical rotation was provided by measuring the signal width of the waveform. Furthermore, the optical rotations of sugar solutions with different concentrations were measured by this method, and the fitting degree of obtained fitting curve is 0.9996. This showed that this method was effective.