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11.
N. Fazeli F. Afshar Taromi 《Journal of polymer science. Part A, Polymer chemistry》2003,41(1):135-142
The basis of the two‐step in–in method is as follows: star polymers with poly(divinyl benzene) cores, synthesized by the arm‐first method, include many unreacted double bonds in their core, and these double bonds can be attacked by the carbanions of some monomers such as styrene and dienes. In this work, linear polyisoprene chains were used to attack the double bonds existing in the poly(divinyl benzene) cores of polystyrene star polymers, so that a heteroarm star polymer with polystyrene and polyisoprene arms was synthesized. It was later well characterized with size exclusion chromatography, light scattering, viscometry, UV spectroscopy, dynamic mechanical thermal analysis, and 1H NMR. © 2002 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 41: 135–142, 2003 相似文献
12.
给出平凹谐振腔和凹平凹谐振腔失调时光轴确定方法。在二维轴对称折迭-组合腔 激光器小角度失调运行时,对非相干并和和相干并和后的输出光束的近场强度分布做了分析和模拟。结果表明:小角度失调对4cm以内的近场影响不大,光强分布仍具有高斯状分布;对4cm以外的近场影响较大,光强分布发生相应的形变,且随着失调角度变大而变大。 相似文献
13.
激光束偏转法检测金属表面层的缺陷 总被引:3,自引:0,他引:3
本文编程计算了由激光光热应产业的金属表面的温度分布和泵浦光的调制频率、金属层厚度等的关系,预言检测浓度缺陷的能力。用激光光束偏转法检测到表面下不同深处的缺陷,并把面扫描幅值信号以三维象和灰度象显示。 相似文献
14.
15.
介绍了谐振式力传感器的工作原理,并从理论上和实验上对中科院合肥智能所研制的第一代微型硅谐振梁(3×0.4×0.045mm^3)式测力传感器进行了全面的振动分析,所得结构为其进一步优化设计提供了科学根据,文中使用的实验分析方法,为其它微小物体的动态和识别提供了一条有效途径。 相似文献
16.
Cang Li 《Journal of solid state chemistry》2004,177(12):4569-4575
Reaction of an aqueous slurry of an Mg2Al-NO3 layered double hydroxide with a four-fold excess of Na[Eu(EDTA)] gives a material which analyses for Mg0.68Al0.32(OH)2[Eu(EDTA)]0.10(CO3)0.11·0.66H2O. The interlayer spacing of the material is 13.8 Å, corresponding to a gallery height of 9.0 Å, which accords with the maximal dimensions (9-10 Å) of the anion in metal-EDTA complex salts as determined by single crystal X-ray diffraction. Geometrical considerations show that the charge density on the layered double hydroxide layers is too high to be balanced by intercalation of [Eu(EDTA)]− alone, necessitating the co-intercalation of carbonate ions which have a much higher charge density. 相似文献
17.
Powdered samples of cotton, flax and viscose from textile fibres were subjected to electron beam irradiation (20-400 KGy). ESR signals were observed after irradiation. The intensity of the signals depended on the administered dose and exhibited an exponential decay with time. The ESR spectra, whose pattern depended drastically on the crystallinity of the samples, indicated the simultaneous presence of at least three carbon-centred radical species. When the whole irradiated textile fibres were quenched in a solution of glycidyl methacrylate (GMA) a significant increase of the weight was observed, the increase being strongly dependent on the administered dose and on the time interval elapsed between irradiation and quenching. Spectroscopic characterisation evidenced that GMA acted as cellulose radicals scavenger on the unsubstituted carbon of the double bond and was covalently linked to the fibre through a new C-C bond while maintaining unaltered the ester and the epoxide groups, available for further derivatisations. Because irradiation of the whole textile fibres in the range 20-200 KGy does not result in significant degradation of the material, GMA quenching of fibres irradiated in this dose range may represent an attractive route to their functionalisation. 相似文献
18.
《Surface and interface analysis : SIA》2003,35(3):246-250
Among the magnetic metal/semiconductor contacts, the Fe/GaAs system has been widely studied owing to its potential applications in electronic devices. In contrast, there are not many studies concerning the Fe/AlxGa1?xAs contact, and in particular there are no reports concerning the changes induced in the interfacial zone by the presence of Al. In this work, thin polycrystalline iron films were deposited by ion beam sputtering at room temperature on a 300 nm thick Al0.25Ga0.75As layer grown by molecular beam epitaxy onto GaAs(001). X‐ray diffraction analysis showed that the iron films are polycrystalline, and indications of a (002) texture of the film were observed. The fine scale analysis of the interface was achieved by high‐resolution transmission electron microscopy (HRTEM) observations, the results of which are compared with the physicochemical information obtained from electron‐induced x‐ray emission spectroscopy, by analysing the Al 3p valence states at the Fe/AlxGa1?xAs interface. The HRTEM experiments on cross‐section samples indicate that the interfacial zone between iron and AlGaAs is limited to <1.5 nm in thickness. X‐ray emission spectroscopy showed the presence of Al atoms in an FeAl‐like environment at the interface, and the existence of wrong bonds and point defects. The estimated width of the perturbed interface (2.0 ± 0.5 nm) is in agreement with the HRTEM results. Copyright © 2003 John Wiley & Sons, Ltd. 相似文献
19.
David Tzach Robert Buschauer Gregory Benford 《International Journal of Infrared and Millimeter Waves》1981,2(1):71-82
After eliminating reflections from the walls of the plasma container, we observed polarization of the coherent synchrotron radiation from a relativistic electron beam rotating in a plasma. Several features of the polarization agree well with calculations based on the single particle synchrotron radiation theory. A particular polarization ratio (Fig. 3) does not, however. We deduce from this direct diffraction of the radiation by the beam electrons. This is strong evidence for beam-particle bunches of size cm. Also, there must be some absorption of the extraordinary wave to account for the observations. We suggest a way to apply these results to measure the pitch angle of the beam.Work supported by Army Research Office. 相似文献
20.