The DI-SPME Method for Determination of Selected Narcotics and Their Metabolites,and Application to Bone Marrow and Whole Blood Analysis

The present investigation utilised the quick and easy SPME/LC-MS method to determine selected narcotic substances and their metabolites in whole blood. The study included qualitative analysis and validation of the method. Analytes were determined in the linearity range of 25–300 ng/mL. The precision during and between days (in general CV < 13.41%), and the LOD which results in between 0.36 and 11.08 ng/mL, and the LOQ between 1.20 and 36.90 ng/mL were investigated. The validation results obtained, as well as the results of subsequent in-laboratory tests, confirmed the applicability of the method in the analysis of blood samples. An attempt to apply the method to the analysis of bone marrow samples has yielded promising results; however, more detailed studies are needed in this area.     

Review of Fluorescence Spectroscopy in Environmental Quality Applications

Fluorescence spectroscopy is an optical spectroscopic method that has been applied for the assessment of environmental quality extensively during the last 20 years. Most of the earlier works have used conventional light sources in spectrofluorometers to assess quality. Many recent works have used laser sources of light for the same purpose. The improvement of the energy sources and of the higher resolution spectrometers has led to a tremendous increase in applications. The motivation for the present review study is the increasing use of laser sources in environmental applications. The review is divided in two parts. The fundamental principles of fluorescence spectroscopy are described in the first part. The environmental applications are described in the second part.     

大行程位移台干涉测距系统的误差补偿

双频激光干涉仪作为常用的精密光学非接触式测量设备,具有精度高、抗干扰能力强、灵活性好等优点。然而环境温度变化、机械振动等因素可能会影响其测量结果的准确性,并且影响程度会随着测量光程的增加而增大。针对基于双频激光干涉仪的大行程位移台测距系统,首先研究了位移台测距系统的测量原理,然后针对系统存在的各项误差进行了分析和补偿,最后,对系统进行综合误差补偿实验,短时间补偿量达到10^-8 m量级,且时间越长补偿效果越好。该方法较现有的误差补偿方法更为完整,补偿量更大。     

基于DFB激光器的振动传感系统改进PGC解调算法

相位生成载波(Phase Generated Carrier, PGC)解调算法是目前光纤干涉传感领域中重要的解调算法。针对目前PGC解调算法中光强扰动和调制深度影响信号解调准确度的问题,提出了一种改进的PGC解调算法(PGC-Ameliorated),并搭建了基于分布反馈(Distributed Feedback, DFB)激光器的振动传感系统进行实验验证。实验结果表明,当被测振动信号的频率为800 Hz时,该算法信噪比为57 dB,优于微分交叉相乘(Differential and Cross Multiplying, DCM)算法和反正切(Arctan)算法近20 dB。在不同光强下,该算法解调信号幅值波动范围在±0.02 rad;在不同调制深度下,该算法总谐波失真最小为0.61%,信纳比最大为25.9 dB,相比于DCM算法和Arctan算法具有更低的总谐波失真和更高的信纳比。     

低强度激光辐照对蝗虫活性的影响

为研究低强度激光辐照对蝗虫活动能力的影响,以减少农药的使用量和降低农药的浓度,选择大功率连续型近红外半导体二极管激光器,针对3龄至4龄期东亚飞蝗蝻虫头部位置,在距离激光发光面4cm处,进行2s和4s的辐照试验,分别观察比较辐照前后蝗虫的活性和活性降低程度．试验结果表明,辐照前,蝗虫具有较高的活性,辐照后蝗虫的活性降低,并逐渐趋于一致性;辐照时间越长,蝗虫的活性降低程度越高。说明低强度近红外激光辐照蝗虫头部位置能明显抑制其活动能力。     

新型光纤激光雷达的结构理论分析与作用距离计算

为了改善当前激光雷达存在的对振动敏感,体积庞大,对人眼不安全等问题,综合国内外激光雷达研究现状的基础上.给出了一种新型光纤激光雷达的结构.该雷达利用光纤激光器作为光源,光路中大量采用了光纤器件,使得系统体积大大减小.采用相干探测的原理,根据激光雷达作用距离方程,给出了信噪比与光纤激光雷达作用距离的关系.根据所选的器件参数,通过理论计算,在探测概率为0.9,虚警概率小于10-4的情况下,得到了2 km的最大作用距离.所设计的光纤激光雷达体积小,结构紧凑、新颖,具有良好的探测能力.     

用激光冲击波无损评估材料内部的均一性

利用脉冲激光诱导的冲击波对材料的内部组织结构进行无损评估，首次通过测量激光在铝和碳纤维／环氧复合材料中诱导的冲击波获得了材料内部的均一性信息。     

一种新型薄腔法-珀干涉测速系统研究

本文所关注的激光干涉测速技术主要用于测试在冲击波或爆轰波作用下各种材料样品的自由面速度随时间变化的过程,介绍了基于光学谐振腔的选频特性利用薄腔法-珀干涉仪直接测量高速飞片所引起的多普勒频移从而获得其速度信息的设想,并根据此设想构建薄腔法-珀干涉测速系统的技术路线。最后描述了利用该项测试技术实际测量金属箔电爆炸驱动的Kapton膜飞片速度的实验并对实验结果进行了分析。与其它激光测速装置相比,该干涉仪具有体积小、结构简单紧凑和成本低的特点。     

电控宽带连续调谐外腔半导体激光器

介绍了一种电控调谐的外腔半导体激光器，并对其连续调谐特性进行了理论和实验分析。压电陶瓷（ＰＺＴ）（双晶片）的电扫描角度可达１°，采用适当的外腔结构，靠ＰＺＴ可同时改变外腔腔长和光栅衍射角，实现输出波长的调谐。该器件调谐范围最大可达１５ｎｍ，连续调谐范围（无跳模）为５０ＧＨｚ     

非偏振光叠加传播及散射势获取的相关讨论

经典的Stokes理论认为非偏振光叠加仍为非偏振光。以高斯-谢尔模光束为示例,表明光场在自由传播的过程中情况并非总是如此。并以此为例,展示Stokes理论的可叠加性原理在描述光场传播过程中的本地行为和全局行为上是有区别的。作为应用示例,讨论了一个与大气和生物组织相关的散射势获取的问题。