Separation and determination of m-phenoxybenzaldehyde reaction products by capillary gas chromatography

A capillary GC method employing an internal standard has been developed and successfully used for quantitative determination both of the raw materials used for the manufacture of m-phenoxybenzaldehyde and for the components of the reaction mixtures obtained at various stages of the development of the process. A complete analysis can be performed in a single temperature programmed run.     

开发“民间商用电话保密机”的市场评估

给出了民用电话保密产品需求量分析和对民用电话加密装置的六点要求及其市场效益评估。     

基于EWB的D/A数模转换器的仿真研究

阐述了D／A转换器的仿真原理，给出了T形电阻网络D／A转换器仿真模型的构造方法，并采用EWB进行了系统仿真，仿真结果表明该方法是合理、可行的。     

基于XML技术数据库优化接入设计

鉴于用户对目前数据库接入技术要求的提高，一种基于XML技术对数据库接入进行优化的技术出现了。这种技术利用了基于XML传输时的可扩展、高度结构化等特性，在JavaBean，JDBC，Apache，Tomcat等设计组件及Linux体系结构的配合使用下．为用户提供了一个安全、高效、可扩展且访问灵活的数据库接入方式。     

迭加与量化水印嵌入方案的比较及量化参数优化

分别研究了迭加法和量化法的隐蔽性和稳健性，并且提出了量化调制水印方案中的参数优化方法。对两类方法的分析比较表明，迭加法适用于在高频分量嵌入水印，而量化法适用于在低频分量嵌入水印。并以实验验证了这一结论。     

采用氮气氛保护的再流焊接技术

叙述了先进再流焊接技术的新发展,描述了提高BGA再流焊接效果的工艺要点,优化倒装芯片再流焊接和固化的新方法。最后,讲述了先进的降低氮消耗量的方法即:通过最大限度地提高潜在收益,以促进再流焊接技术的发展,以此来满足装配厂商的需要。     

利用UTD修正的MoM-PO混合算法研究

介绍了利用矩量法(MoM)和物理光学(PO)混合方法处理复杂线体结构的电磁散射问题，提出利用pulse基函数对线电流进行展开，使得处理复杂线体结构问题变得简化，并推导出一般的矩阵方程。然后针对PO在阴影区域失效等问题，利用UTD(一致性几何绕射)对该简化模型结构下的PO区域电流进行了修正，使得其应用范围得到扩展、计算精度得到提高。文中的实例结果与传统的MoM很好的一致，从而说明了该方法的有效性和精确性。     

图像边缘检测在关节镜图像处理中的应用

主要论述了采用图像边缘检测和图像跟踪算法对采集的关节镜图像进行图像处理和分析的过程。在图像处理的基础上，系统自动测量出指定目标的形状参数，实现了系统的测量要求。本研究为实现关节镜手术过程图像的保存和手术的准确性提供了可行的方法。     

Relating the Morphology of Poly(p‐phenylene vinylene)/Methanofullerene Blends to Solar‐Cell Performance

The performance of bulk‐heterojunction solar cells based on a phase‐separated mixture of donor and acceptor materials is known to be critically dependent on the morphology of the active layer. Here we use a combination of techniques to resolve the morphology of spin cast films of poly(p‐phenylene vinylene)/methanofullerene blends in three dimensions on a nanometer scale and relate the results to the performance of the corresponding solar cells. Atomic force microscopy (AFM), transmission electron microscopy (TEM), and depth profiling using dynamic time‐of‐flight secondary ion mass spectrometry (TOF‐SIMS) clearly show that for the two materials used in this study, 1‐(3‐methoxycarbonyl)propyl‐1‐phenyl‐[6,6]‐methanofullerene (PCBM) and poly[2‐methoxy‐5‐(3′,7′‐dimethyloctyloxy)‐1,4‐phenylene vinylene] (MDMO‐PPV), phase separation is not observed up to 50 wt.‐% PCBM. Nanoscale phase separation throughout the film sets in for concentrations of more than 67 wt.‐% PCBM, to give domains of rather pure PCBM in a homogenous matrix of 50:50 wt.‐% MDMO‐PPV/PCBM. Electrical characterization, under illumination and in the dark, of the corresponding photovoltaic devices revealed a strong increase of power conversion efficiency when the phase‐separated network develops, with a sharp increase of the photocurrent and fill factor between 50 and 67 wt.‐% PCBM. As the phase separation sets in, enhanced electron transport and a reduction of bimolecular charge recombination provide the conditions for improved performance. The results are interpreted in terms of a model that proposes a hierarchical build up of two cooperative interpenetrating networks at different length scales.     

(a,b,n)-临界图的几个充分条件

设G是一个图 .设g和f是两个定义在V(G)上的整值函数使得对V(G)所有顶点x有g(x) ≤f(x) .图G被称为 (g ,f,n) 临界图 ,如果删去G的任意n个顶点后的子图都含有G的 (g ,f) 因子 .本文给出了图是 (a ,b ,n) 临界图几个充分条件 ,即度和邻域条件 .进一步指出这些条件是最佳的 .