催化光度法时间程序测定土壤中痕量碘

碘是评价环境的重要元素之一,是地球化学勘察样品常测元素。本实验建立了艾斯卡试剂分解-热水提取样品,催化分光光度法时间程序测定碘的方法。详细讨论了艾斯卡试剂手工制作与行星球磨机制作的利弊;;参比液的选择;17℃-25℃不同环境温度条件对实验结果的影响;全程序空白溶液,与36g/L的碳酸钠溶液两种方法制作标准曲线及标准曲线线性范围;样品烧结时间及温度;乙酸用量对样品测试吸光度的影响。结果表明：利用行星球磨机制作艾斯卡试剂,选择试剂空白为参比液,在19℃的恒温环境下,采用36g/L的碳酸钠溶液制作0-8ug/mL标准曲线,样品采用0-300℃、300-500℃、500-750℃三阶段升温,750℃保持30min的烧结程序,乙酸用量为5mL时可以得到可靠的结果。该方法克服了艾斯卡试剂制作困难、样品烧结结块及实验反应速率过快等困难。通过方法学考察表明：基于所建方法碘元素校准曲线系数＞0.999;方法检出限为0.2 mg/kg;测定GSS36、GSS37、GSS38、GSS40、GSS47、GSS48、GSS49等9种国家一级标准物质,结果均在参考值范围内,相对标准偏差RSD＜5%。该方法测定的结果准确度及精密度高、 检出限低、减少碘记忆效应的存在,适用于地球化学勘察土壤样品中碘的测定。     

Monotone Span Program vs.Linear Code

Monotone span program(MSP) and Linear code(LC) are efficient tools to construct Linear secret sharing scheme (LSSS) for a given access structure.Since the size of an MSP or the length of an LC corresponds to the communicational complexity of an LSSS,one main motivation to study MSPs or LCs is the lower bound for their sizes or lengths.Therefore,it is one of the most important open problems how to efficiently construct an MSP or LC for a given access structure Γ with the smallest sizes or shortest length.Our contributions are:We extend TANG et al.'s result,showing that,for any given access structure Γ,there exists an MSP or an LC to realizeΓ if and only ifa system of quadratic equations has solutions;We utilize the relationship between LCs and MSPs to obtain the greatest lower bound on the row size and the column size of MSPs realizing a given Γ,as well as an upper bound on the column size of MSPs;We give an algorithm to construct an MSP with the smallest sizes.     

Weak and strong stationarity in generalized bilevel programming and bilevel optimal control

In this article, we consider a general bilevel programming problem in reflexive Banach spaces with a convex lower level problem. In order to derive necessary optimality conditions for the bilevel problem, it is transferred to a mathematical program with complementarity constraints (MPCC). We introduce a notion of weak stationarity and exploit the concept of strong stationarity for MPCCs in reflexive Banach spaces, recently developed by the second author, and we apply these concepts to the reformulated bilevel programming problem. Constraint qualifications are presented, which ensure that local optimal solutions satisfy the weak and strong stationarity conditions. Finally, we discuss a certain bilevel optimal control problem by means of the developed theory. Its weak and strong stationarity conditions of Pontryagin-type and some controllability assumptions ensuring strong stationarity of any local optimal solution are presented.     

Tightening concise linear reformulations of 0-1 cubic programs

A common strategy for solving 0-1 cubic programs is to reformulate the non-linear problem into an equivalent linear representation, which can then be submitted directly to a standard mixed-integer programming solver. Both the size and the strength of the continuous relaxation of the reformulation determine the success of this method. One of the most compact linear representations of 0-1 cubic programs is based on a repeated application of the linearization technique for 0-1 quadratic programs introduced by Glover. In this paper, we develop a pre-processing step that serves to strengthen the linear programming bound provided by this concise linear form of a 0-1 cubic program. The proposed scheme involves using optimal dual multipliers of a partial level-2 RLT formulation to rewrite the objective function of the cubic program before applying the linearization. We perform extensive computational tests on the 0-1 cubic multidimensional knapsack problem to show the advantage of our approach.     

管理信息系统方案评价和选择的可行方法

本文由管理信息系统[1,2]的总体目标出发,建立系统的综合评价指标体系;对[4]中的“两两对比价值法”作了改进;以矩阵方式描述了[3]中的关联分析法。这两种方法用于管理信息系统方案评价、选择是可行的和有效的,并以实例进行说明。     

单片微机系统时钟软件的一种实现方法

本文介绍一种用MCS—51汇编语言设计的单片微机系统时钟软件。该软件所需的中断服务时间短,因而不影响CPU进行其他实时性较高的处理工作,该软件还能提供时间显示功能,文中给出了相应的显示硬件结构。     

计算机在配合物研究中的应用一处理电位溶出法、极谱法、电位法数据的通用程序

本文根据电化学方法研究配合物的特性,设计了一个计算配合物稳定常数的通用程序,其程序用BASIC语言编写。此程序能用于电位溶出法、极谱法和电势法研究配合物的实验数据处理。     

中子引起单粒子翻转过程的Monte Carlo计算模拟

从中子与硅原子相互作用的物理机理出发,利用Monte Carlo方法编制了中子引起单粒子翻转的计算模拟程序,并对14 MeV中子环境下的16K位静态存储器硅片翻转过程中的物理量进行了计算,同时可为中子引起的单粒子翻转的研究提供截面和描述内部物理过程的参考数据。     

Convergence and Error Bound for Perturbation of Linear Programs

In various penalty/smoothing approaches to solving a linear program, one regularizes the problem by adding to the linear cost function a separable nonlinear function multiplied by a small positive parameter. Popular choices of this nonlinear function include the quadratic function, the logarithm function, and the x ln(x)-entropy function. Furthermore, the solutions generated by such approaches may satisfy the linear constraints only inexactly and thus are optimal solutions of the regularized problem with a perturbed right-hand side. We give a general condition for such an optimal solution to converge to an optimal solution of the original problem as the perturbation parameter tends to zero. In the case where the nonlinear function is strictly convex, we further derive a local (error) bound on the distance from such an optimal solution to the limiting optimal solution of the original problem, expressed in terms of the perturbation parameter.