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991.
992.
为了解决电磁感应加热仿真中因目标体积太大或者太小、时间长而难以仿真的问题,介绍了一种对空间和时间进行多尺度变换的快速计算方法。通过有限元方法仿真计算和对比验证,尺度变换后所得结果与变换之前吻合良好,能够减少大物体建模仿真的运算数据量。当时间尺度分别缩小10倍和100倍时,计算所需的时间分别减少了81.7%和91.8%。 相似文献
993.
《Analytical letters》2012,45(11):2252-2270
Abstract A novel adsorptive fast Fourier transform cyclic voltammetry (AFFTCV) technique for the fast determination of tramadol in flow‐injection systems has been introduced in this work. The potential waveform, consisting of the potential steps for cleaning, stripping, and potential ramp, was continuously applied on an Au disk microelectrode (with a 12.5 µm in radius). The proposed detection method has some advantages, the greatest of which are as follows: first, it is no more necessary to remove oxygen from the analyte solution and second, it is a very fast and appropriate technique for determination of the drug compound in a wide variety of chromatographic analysis methods. The influences of pH of eluent, accumulation potential, sweep rate, and accumulation time on the determination of the tramadol were considered. The method was linear over the concentration range of 1.5–900,000 pg/ml (r=0.9968) with a limit of detection and quantitation 0.32 and 1.5 pg/ml, respectively. The method has the requisite accuracy, sensitivity, precision, and selectivity to assay tramadol in tablets and in biological fluids. 相似文献
994.
Chunrui Ding Shimei Xu Jide Wang Yang Liu Xiaoxia Hu Peng Chen Shun Feng 《先进技术聚合物》2012,23(9):1283-1286
The layer‐by‐layer (LbL) assembled multilayer films are widely used in the biomedical field for the controlled drug delivery. Here, multilayer films were assembled by LbL technique through alternating deposition of cationic polyurethane (PU) and poly(acrylic acid) (PAA) on glass slides. Methylene blue (MB) was used as a model drug to investigate the loading and release ability of the prepared multilayer film. The results showed that the loading rate and loading amount of MB were greatly influenced by pH value of the dye solution, and the release rate of MB was controlled both by ionic strength and pH value of immersing solution. The result also indicated that the film had a good reversibility of drug loading and release. It suggested that the PU/PAA multilayer film had potential applications in drug delivery and controlled release. Copyright © 2011 John Wiley & Sons, Ltd. 相似文献
995.
《Analytical letters》2012,45(4):747-762
Abstract In this work a novel method for the determination of piroxicam in flow‐injection systems has been developed. A system using fast Fourier transform continuous cyclic voltammetry (FFTCV), at a gold microelectrode in flowing solution, was used for determining piroxicam in its pharmaceutical formulations. The developed technique is very simple, precise, accurate, time saving, and economical, compared to all of the previously reported methods. The effects of various parameters on the sensitivity of the method were investigated. The best performance was obtained with a pH value of 2, scan rate value of 40 V/s, accumulation potential of (400) mV, and accumulation time of 0.4 s. The proposed method has some advantages over other reported methods, such as, no need for the removal of oxygen from the test solution, a picomolar detection limit, and finally that the method is fast enough for the determination of any such compound, in a wide variety of chromatographic methods. To obtain a sensitive determination, the integration range of currents was set for all the potential scan ranges, including oxidation and reduction of the Au surface electrode, while performing the measurements. The potential waveform, consisting of the potential steps for cleaning, accumulation, and potential ramp of analyte, was applied on an Au disk microelectrode (with a 12.5 µm in radius) in a continuous way. The method was linear over the concentration range of 1.5–364000 pg/ml (r=0.998) with a limit of detection and quantitation of 0.33 and 1.5 pg/ml, respectively. The method has the requisite accuracy, sensitivity, precision, and selectivity to assay piroxicam in tablets. 相似文献
996.
《Analytical letters》2012,45(11):851-861
Abstract A system is described for the non-flame atomisation of mercury, using sample heating pulses of a few microseconds duration. The rapid sample atomisation thus obtained leads to good analytical sensitivity; it also provides a technique for distinguishing between, and separately measuring, inorganic and organically-bound mercury. 相似文献
997.
苏北盆地海安凹陷钻井存在钻头选型复杂,单井钻头数量使用过多,钻井周期长,钻井效率低等问题,迫切需要解决钻头优选问题.用模糊优化理论对常用钻头选型的效益指数法进行了改造完善,建立了新的钻头优选模型,对海安已钻27口井的钻头进行了优选,确定了实钻效果最佳的钻头.运用优选的钻头在现场进行钻井作业,取得优良的效果,极大提高了钻井效率,缩短了钻井周期,同时也极大简化了钻头选型.探索了一条有效解决苏北盆地海安凹陷及相邻区块钻头优选的技术路径,为高效勘探开发苏北盆地提供了有力的技术支撑. 相似文献
998.
An Experimental Technique for Spalling of Concrete 总被引:1,自引:0,他引:1
The spalling strength of concrete is measured by examining the strain wave profiles in a polymer buffer bar behind the slender
concrete bar specimen placed between a large diameter (Φ100 mm) Hopkinson bar and the buffer bar. The experimental results indicate that the spalling strength is related to not only
the compressive strength of concrete but also the impact velocities (the loading rates). The rate effect of spalling strength
mainly results from the different cracking paths in concrete under different impact velocities. However when the input compressive
stress to specimen exceeds the threshold required to trigger the compressive damage, the spalling strength decreases due to
the evolution and cumulation of compressive damage in concretes. The repeated impact loading experiments indicate that damage
plays an important role in the spallation process of concrete. The high speed video of the spalling fracture process shows
that multiple spalling fractures may occur in the scab and damage accumulation resulting from stress wave propagation in scab
is the main reason for the producing of multiple spallations. 相似文献
999.
冲击荷载作用下混凝土材料的细观本构模型 总被引:8,自引:0,他引:8
将混凝土材料看成是水泥砂浆基体和粗骨料颗粒组成的2相复合材料,假设水泥砂浆基体和粗骨料颗粒均为弹性、均匀、各向同性的,粗骨料颗粒为球形。基于Mori-Tanaka理论和Eshelby 等效夹杂理论推出了混凝土材料弹性模量的计算公式。在Horii和Nemat-Nasser提出的脆性材料在双轴向压应力作用下破坏的滑移裂纹模型基础上,运用细观力学方法推导了微裂纹对材料弹性模量的弱化作用以及微裂纹的损伤演化方程。建立了混凝土材料在冲击荷载作用下的一维动态本构模型,模拟曲线与实验曲线符合良好,因而可以用该模型模拟混凝土材料在冲击荷载下的动态特性。 相似文献
1000.
When cyclic loading is applied to poroelastic materials, a transient stage of interstitial fluid pressure occurs, preceding a steady state. In each stage, the fluid pressure exhibits a characteristic mechanical behavior. In this study, an analytical solution for fluid pressure in two-dimensional poroelastic materials, which is assumed to be isotropic, under cyclic axial and bending loading is presented, based on poroelasticity. The obtained analytical solution contains transient and steady-state responses. Both of these depend on three dimensionless parameters: the dimensionless stress coefficient; the dimensionless frequency; and, the axial-bending loading ratio. We focus particularly on the transient behavior of interstitial fluid pressure with changes in the dimensionless frequency and the axial-bending loading ratio. The transient properties, such as half-value period and contribution factor, depend largely on the dimensionless frequency and have peak values when its value is about 10. This suggests that, under these conditions, the transient response can significantly affect the mechanical behavior of poroelastic materials. 相似文献