Inter-cell spectrum efficiency improvement technology

Improvement in inter-cell spectrum efficiency is a valuable research topic in mobile communication system, which affects cell edge user experience especially. According to current research results, there are three methods to deal with inter-cell interference to improve inter-cell spectrum efficiency, including inter-cell interference randomization, inter-cell interference cancellation and inter-cell interference coordination. This paper analyzes three important inter-cell spectrum efficiency improvement technologies, soft frequency reuse (SFR), uplink power control, and downlink coordinated multi-point transmission/reception (CoMP), and relative research progress.     

基于宽频调谐特征和谱残差分析的显著性目标检测

根据人眼视觉系统的基本特点,提出一种基于宽频调谐特征和谱残差分析的显著性目标检测算法。该方法通过在上下文信息中提取图像的宽频调谐特征,运用线性叠加融合宽频调谐特征子图得到初步特征图,然后利用多尺度方法构建多分辨率显著图谱子序列,最后利用谱残差分析融合位置特征对显著性子图进行操作运算得到最终的显著图。基于自然图像的显著性目标检测实验结果证明,该方法具有较好的实用性和较强的稳定性,能够获取较为精确的检测结果。     

基于时频分析的高频地波雷达目标检测算法

为提高海事监测中高频地波雷达(High Frequency Surface Wave Radar,HFS-WR)对运动目标的检测准确率,提出了一种基于频谱细化和小波尺度谱重排时频分析的运动目标检测算法.对HFSWR的接收信号进行频率细化处理以提高后续时频分析的频率分辨率;然后,进行基于Morlet小波的时频分析以提取目标的时频分布特征,为提高时频分布的集中性和抑制交叉项干扰,对小波尺度谱进行重排;根据得到的时频分布特征实现可疑目标区的精确检测.实验结果表明:该算法能有效检测多普勒频率相差很小的运动目标以及海杂波附近的运动目标,可用于对常规目标检测算法无法判定的可疑目标区域进行精细、准确的目标检测与分析.     

One-Pot Synthesis and Fungicidal Activities of Derivatives of Imidazo [2,1-b]-1,3,4-thiadiazol-5(6H)-one

The isothiocyanates 2, obtained from aza-Wittig reactions of vinyliminophosphoranes 1 with CS ₂ , reacted with hydrazine to give 3-amino-2-thioxo-4-imidazolidinones 4. One-pot reactions of 4, aromatic isocyanates, Ph ₃ P, C ₂ Cl ₆ , and Et ₃ N generated imidazo[2,1-b]-1,3,4-thiadiazol-5(6H)-ones 7. Compound 7 exhibited good fungicidal activities, especially against Sclerotinia sclerotiorum de Bary and Botrytis Cinerea Pers.     

A FACILE SYNTHESIS OF DIETHYL 1- ISOTHIOCYANO)ALKYLPHOSPHONATES[1]

Abstract

Novel, diethyl 1-(isothiocyano)alkylphosphonates 3 have been efficiently synthesized via a one-pot reaction of diethyl 1-azidoalkylphosphonates 1 with triphenylphosphine, followed by in situ transformation of thus formed phosphazenes 2 with carbon disulfide. Application of the title compounds in the synthesis of diethyl (N-phenylthioureido)- and (benzothiazol-2-ylamino)methylphosphonates was also described.     

THE PREPARATION OF TRIALKYL PHOSPHITES DIRECTLY FROM THE ELEMENT

Abstract

The reaction between finely divided white phosphorus and several alkoxide ions in the presence of tetrachloromethane and excess of alcohol has been investigated under a variety of conditions. High yields of trialkylphosphite are obtained when two equivalents of alkoxide are used. With one equivalent of alkoxide, dialkylphosphonate is formed in comparable yield. Maximum yields of triester are obtained within 1–3 h at room temperature. Prolonged treatment results in the conversion of trialkylphosphite to phosphate by reaction with tetrachloromethane. Phenolate ions are unreactive under the same experimental conditions. The mechanism of the reaction is discussed.     

Synthesis and Antibacterial Studies of Some Novel 2-(Coumarin-3-yl)-5-mercapto-1,3,4-oxadiazoles Containing 2,4,6-Trisubstituted s-Triazine Derivatives

A new series of 2-(coumarin-3-yl)-5-mercapto-1,3,4-oxadiazoles based on various aryl thiourea/ureas incorporating a 1,3,5-s-triazine moiety is reported. The components of this series have been obtained by the reaction of cyanuric chloride (1) with 2-(coumarin-3-yl)-5-mercapto-1,3,4-oxadiazole (2). The prepared 2-{(coumarin-3-yl-1,3,4-oxadiazolyl)-5-thio}-4,6-dichloro-s-triazine (3) was subsequently treated with morpholine (4) to form 2-{(coumarin-3-yl-1,3,4-oxadiazolyl)-5-thio}-4-(morpholino)-6-chloro-s-triazine (5). This was further treated with various substituted aryl urea/thioureas (6a–k/7a–k) to afford the title compounds 8a–k and 9a–k, which were and tested for their antibacterial activity (MIC) against different microorganisms. The structures of the novel synthesized compound have been established on the basis of ¹H NMR and FT-IR data together with elemental analysis.

Supplemental materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements to view the free supplemental file.     

Diastereoselective Synthesis of γ-Butenolides Catalyzed by Potassium tert-Butoxide

Potassium tert-butoxide (0.1 mol%) catalyzed a vinylogous Mukaiyama aldol reaction between aromatic and aliphatic aldehydes with 2-(trimethylsilyloxy)furan. The corresponding γ-butenolides were obtained in good yields with good diastereoselectivities.