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991.
Haruya Mizutani 《偏微分方程通讯》2013,38(2):169-224
The present article is concerned with Schrödinger equations on non-compact Riemannian manifolds with asymptotically conic ends. It is shown that, for any admissible pair (including the endpoint), local in time Strichartz estimates outside a large compact set are centered at origin hold. Moreover, we prove global in space Strichartz estimates under the nontrapping condition on the metric. 相似文献
992.
This paper shows the selective etching process of an AlInN sacrificial layer, lattice-matched to GaN, on N-face GaN by an aqueous solution of 1,2-diaminoethane. Using the wavelength dispersive X-ray (WDX) spectrometers on an electron probe micro-analyser, together with an optical spectrometer and silicon CCD array added to the light microscope, and sharing the same focus as the electron microscope, cathodoluminescence spectra are collected from exactly the same spot as sampled by the WDX spectrometers. This technique allows the compositional properties of the etched AlInN layer and the optical properties of the semiconductor layers underlying the sacrificial layer to be scrutinised, verifying the etching selectivity and the efficiency of the process. 相似文献
993.
994.
C. Herrero Latorre J. Álvarez MéndezAuthor VitaeJ. Barciela GarcíaAuthor Vitae S. García MartínAuthor VitaeR.M. Peña CrecenteAuthor Vitae 《Analytica chimica acta》2012
New materials have significant impact on the development of new methods and instrumentation for chemical analysis. From the discovery of carbon nanotubes in 1991, single and multi-walled carbon nanotubes – due to their high adsorption and desorption capacities – have been employed as sorption substrates in solid-phase extraction for the preconcentration of metal species from diverse matrices. Looking for successive improvements in sensitivity and selectivity, in the past few years, carbon nanotubes have been utilized as sorbents for solid phase extraction in three different ways: like as-grown, oxidized and functionalized nanotubes. In the present paper, an overview of the recent trends in the use of carbon nanotubes for solid phase extraction of metal species in environmental, biological and food samples is presented. The determination procedures involved the adsorption of metals on the nanotube surface, their quantitative desorption and subsequent measurement by means of atomic spectrometric techniques such as flame atomic absorption spectrometry, electrothermal atomic absorption spectrometry or inductively coupled plasma atomic emission spectrometry/mass spectrometry, among others. Synthesis, purification and types of carbon nanotubes, as well as the diverse chemical and physical strategies for their functionalization are described. Based on 140 references, the performance and general properties of the applications of solid phase extraction based on carbon nanotubes for metal species atomic spectrometric determination are discussed. 相似文献
995.
A novel one-step sample preparation technique called ultrasound-assisted matrix solid-phase dispersive liquid extraction was developed. After sample matrices being dispersed, target analytes were extracted into acid solutions and fat and lipin were dissolved in n-hexane while the interfering components were retained by dispersing sorbent. The extraction process could be rapidly accomplished within 9 min with high sample throughput under the synergistic effects of vibration, ultrasound action and heating. The extraction efficiency of approach was demonstrated for the determination of intermediates in commercial hair dyes with ion chromatography. Linearity ranges of 0.2–100 mg L−1 and detection limits varying from 0.019 to 0.048 mg L−1 were achieved. The recoveries ranged from 85.7 to 107.0% with the relative standard deviations (RSDs) of 0.31–3.7%. These results showed that the method was simple, time-saving, reliable and suitable for the routine analysis of intermediates in large numbers of hair dyes. 相似文献
996.
In the present study, a rapid, highly efficient and environmentally friendly sample preparation method named ionic liquid-based ultrasound-assisted dispersive liquid–liquid microextraction (IL-USA-DLLME), followed by high performance liquid chromatography (HPLC) has been developed for the extraction and preconcentration of four benzophenone-type ultraviolet (UV) filters (viz. benzophenone (BP), 2-hydroxy-4-methoxybenzophenone (BP-3), ethylhexyl salicylate (EHS) and homosalate (HMS)) from three different water matrices. The procedure was based on a ternary solvent system containing tiny droplets of ionic liquid (IL) in the sample solution formed by dissolving an appropriate amount of the IL extraction solvent 1-hexyl-3-methylimidazolium tris(pentafluoroethyl)trifluorophosphate ([HMIM][FAP]) in a small amount of water-miscible dispersive solvent (methanol). An ultrasound-assisted process was applied to accelerate the formation of the fine cloudy solution, which markedly increased the extraction efficiency and reduced the equilibrium time. Various parameters that affected the extraction efficiency (such as type and volume of extraction and dispersive solvents, ionic strength, pH and extraction time) were evaluated. Under optimal conditions, the proposed method provided good enrichment factors in the range of 354–464, and good repeatability of the extractions (RSDs below 6.3%, n = 5). The limits of detection were in the range of 0.2–5.0 ng mL−1, depending on the analytes. The linearities were between 1 and 500 ng mL−1 for BP, 5 and 500 ng mL−1 for BP-3 and HMS and 10 and 500 ng mL−1 for EHS. Finally, the proposed method was successfully applied to the determination of UV filters in river, swimming pool and tap water samples and acceptable relative recoveries over the range of 71.0–118.0% were obtained. 相似文献
997.
In this paper,the separation transformation approach is extended to the(N + 1)-dimensional dispersive double sine-Gordon equation arising in many physical systems such as the spin dynamics in the B phase of 3 He superfluid.This equation is first reduced to a set of partial differential equations and a nonlinear ordinary differential equation.Then the general solutions of the set of partial differential equations are obtained and the nonlinear ordinary differential equation is solved by F-expansion method.Finally,many new exact solutions of the(N + 1)-dimensional dispersive double sine-Gordon equation are constructed explicitly via the separation transformation.For the case of N 2,there is an arbitrary function in the exact solutions,which may reveal more novel nonlinear structures in the high-dimensional dispersive double sine-Gordon equation. 相似文献
998.
999.
Udo Lang Elisabeth Müller Nicola Naujoks Jurg Dual 《Advanced functional materials》2009,19(8):1215-1220
Electron microscopy studies are used to explore the morphology of thin poly(3,4‐ethylenedioxythiophene) and polystyrene sulfonate acid (PEDOT:PSS) films. The figures show that the films are composed of grains with diameters in the range of about 50 nm. Energy dispersive X‐ray spectroscopy analysis reveals that individual grains have a PEDOT‐rich core and a PSS‐rich shell with a thickness of about 5–10 nm. Atomic force microscopy (AFM) is then used to analyze the topography of fracture surfaces of ruptured PEDOT:PSS tensile specimens. These AFM scans also show that the films are composed of grains dispersed in a matrix. The investigations presented herein yield a picture of PEDOT:PSS morphology with unprecedented clarity. 相似文献
1000.
Samer Israwi 《偏微分方程(英文版)》2020,33(3):261-274
In this paper, a generalized nonlinear dissipative and dispersive equation
with time and space-dependent coefficients is considered. We show that the control of
the higher order term is possible by using an adequate weight function to define the
energy. The existence and uniqueness of solutions are obtained via a Picard iterative
method. As an application to this general Theorem, we prove the well-posedness of
the Camassa-Holm type equation. 相似文献