XRD Analysis on the Fluorescence Material of Sm Doped Si-Ca-Mg System

Fluorescence material of Sm doped Si-Ca-Mg system was synthesized by using the method of solid phase reaction at high temperature. The phase composition and crystal structure of this material were analyzed with XRD method for its composition and the existence form of Sm atom. We aimed to exactly determine the phase composition of this fluorescence material and the doping position and environment of rare-earth Sm atom in the system because these factors have significant effects on the properties. The analytical results show that the Sm atoms dope in Ca2O26Si6Sm8 lattice in the form of atomic site-occupation in three different space positions with different occupancy rates. Therefore, based on the XRD analytical results, the fluorescence material of Sm doped Si-Ca-Mg system with high performance can be synthesized.     

微波萃取-全自动凝胶色谱净化-气相色谱法同时测定太湖沉积物中多氯联苯和有机氯

建立了沉积物中多氯联苯和有机氯农药等39种持久性有机污染物的同时测定方法。样品用正己烷和丙酮(体积比为1∶1)进行微波提取,提取溶液经凝胶色谱和弗罗里硅土净化,浓缩后采用气相色谱法测定。回收率在68.8%~84.2%,检出限为0.05~0.25ng/g。方法适用于沉积物样品中多种多氯联苯和有机氯农药含量的同时测定。     

Jacobi polynomials used to invert the laplace transform

Given the Laplace transform F(s) of a function f(t), we develop a new algorithm to find an approximation to f(t) by the use of the classical Jacobi polynomials. The main contribution of our work is the development of a new and very effective method to determine the coefficients in the finite series expansion that approximation f(t) in terms of Jacobi polynomials. Some numerical examples are illustrated.     

加强计量管理,为企业发展保驾护航

计量是保证产品质量提高的技术基础,是企业提高经济效益的有效手段.本文从建立和完善计量管理体系、加强产品计量保证和计量基础管理、更新计量管理观念等方面,阐述了计量对企业科研、生产、经营的监督、保障作用.     

Continuous TLC as a pilot technique for optimization of gradient HPLC. 1. Theoretical considerations for stepwise gradient TLC with binary mobile phase

Equations describing gradient elution in TLC, with a mobile phase of a constant composition in each step, have been derived. These equations are useful for calculating retention volumes from isocratic TLC data. Equations originally derived for gradient HPLC were adapted for TLC. The validity of the equations has been experimentally verified. The satisfactory agreement between experiment and theory for binary mobile phase composed of methyl ethyl ketone and n-heptane suggests that TLC can be used as a pilot technique for gradient HPLC.     

微波消解-原子荧光法测定山茶油中痕量砷

微波消解优化-原子荧光光谱法测定了山茶油中痕量砷;在多组实验研究的基础上,研究了不同消解酸配比条件下,微波消解方法对测定结果的影响.试验结果表明：微波消解0.3g茶叶对照品和0.3g山茶油样品过程中,消解酸为6mL硝酸+4mL过氧化氢的平行性和回收率最好.山茶油样品回收率为92%-102%;RSD为5.06% 。该法适用于山茶油中痕量砷的测定。     

基于背向衍射图像特征的熊猫光纤定轴方法

对激光束与熊猫光纤相互作用形成的背向衍射图像进行了研究,结果表明,衍射图像中,多级明条纹的长度曲线和其中心位置曲线都与熊猫光纤偏振轴的方位角有关,而且用明条纹的长度曲线作为定轴特征量比用其中心位置曲线作为定轴特征量更灵敏.基于这两个特量提出了一种熊猫光纤的定轴新方法,实现了1°的定轴分辨率,并用图像互相关的方法对这种基于特征量的定轴方法进行了验证,所得的实验结果两者一致.     

论实数的基本性质与求解存在性问题

大学微积分的教学内容是在实数集合上展开的．存在性问题贯穿微积分教学的始终．从深入讨论实数的基本性质开始，引入了求解存在性问题的一般思路．希望从微积分教学的一开始，就让学生深刻体会到数学思想方法的无穷魅力．     

X-s-置换子群

设$X$是群$G$的一个非空子集.子群$H$在$G$中称为是$X$-$s$-置换的,如果对于$G$的每个Sylow子群$T$,存在一个元素$x\in X$,使得$HT^{x}=T^{x}H$.本文中,我们得到有关$X$-$s$-置换子群的一些结果,并利用它们刻画了一些有限群的结构.