Constant amplitude broadband refocusing pulses from numerical optimization

Broadband refocusing pulses for high-field NMR can be constructed with broadband 90× pulses from numerical optimization of Bloch simulations concatenated with their time and phase reversed transformations. This work describes the search for minimal duration 18-kHz modulation frequency constant amplitude refocusing pulses made in this manner for bandwidths of 40, 60 and 80 kHz. Variants optimized at multiple frequencies and with sine squared amplitude truncation also are described. The resulting pulses are expected to have immediate application especially for (13)C refocusing in multidimensional experiments.     

基于千兆以太网的非编网解决方案

由于在价格和兼容性上千兆以太网比FC网有明显的优势，随着计算机网络及终端技术的发展、采用千兆以太网架构非线性编辑网络正成为一种趋势。本文主要分析了采用NAS和IP SAN架构非编网络的解决方案。     

Zero‐Dimensional Hybrid Cd‐Based Perovskites with Broadband Bluish White‐Light Emissions

Recently, low‐dimensional organic‐inorganic hybrid metal halide perovskites acting as single‐component white‐light emitting materials have attracted extensive attention, but most studies concentrate on hybrid lead perovskites. Herein, we present two isomorphic zero‐dimensional (0D) hybrid cadmium perovskites, (HMEDA)CdX₄ (HMEDA=hexamethylenediamine, X=Cl ( 1 ), Br ( 2 )), which contain isolated [CdX₄]^2? anions separated by [HMEDA]²⁺ cations. Under UV light excitation, both compounds display broadband bluish white‐light emission (515 nm for 1 and 445 nm for 2 ) covering the entire visible light spectrum with sufficient photophysical stabilities. Remarkably, compound 2 shows a high color rendering index (CRI) of 83 enabling it as a promising candidate for single‐component WLED applications. Based on the temperature‐dependent, powder‐dependent and time‐resolved PL measurements as well as other detailed studies, the broadband light emissions are attributed to self‐trapped excitons stemming from the strong electron‐phonon coupling.     

固相微萃取纤维研究进展

固相微萃取是一种新型的萃取分离技术. 由于它具有富集能力强、分析速度快、操作简便及便于现场分析和仪器联用等优点,成为痕量物质分离检测分析的重要工具. 固相微萃取技术的核心是固相微萃取纤维. 总结了固相微萃取纤维在稳定性、使用寿命及选择性方面的一些特点,并综述了近年来在这些方面所进行的研究工作及发展方向.     

Universal power law behavior of the AC conductivity versus frequency of agglomerate morphologies in conductive carbon nanotube‐reinforced epoxy networks

The Jonscher universal power law for ac conductivity versus frequency (f = ω/2π) in the dispersion region was tested for a multiwall carbon nanotube/epoxy nanocomposite. The effect of changes in agglomerate morphology on the fitting parameters A and n in the equation σ_{ac =} Aωⁿ was investigated. Changing nanotube agglomerate morphology was tracked by optical microscopy through curing. Evolving morphology was compared alongside ac conductivity obtained via a broadband dielectric spectrometer to elucidate possible physical meaning of the universal power law in the context of this system. The ?logA/n was unaffected by changes in agglomerate morphology affected during cure, yet connected with each other in their dependence on temperature. For this system, the relationship between the fitting parameters in the universal dynamic response equation remains empirical at this stage with regard to biphasic “texture” or morphology within such a network. Electrical conductivity σ versus frequency ω for a composite consisting of agglomerated multiwalled carbon nanotubes dispersed throughout a cured epoxy matrix was discovered to follow the empirical universal dynamic response equation of Jonscher. The frequency behavior of the exponent n is discussed in terms of underlying morphology throughout which charge carriers migrate. © 2016 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2016 , 54, 1918–1923     

NMR‐based analysis of the chemical composition of Japanese persimmon aqueous extracts

Japanese persimmon (Diospyros kaki L.) is recognized as an outstanding source of biologically active compounds relating to many health benefits. In the present study, NMR spectroscopy provided a comprehensive metabolic overview of Japanese persimmon juice. Detailed signal assignments of Japanese persimmon juice were carried out using various 2D NMR techniques incorporated with broadband water suppression enhanced through T₁ effects (BB‐WET) or WET sequences, and 26 components, including minor components, were identified. In addition, most components were quantitatively evaluated by the integration of signals using conventional ¹H NMR and BB‐WET NMR. This is the first detailed analysis combined with quantitative characterization of chemical components using NMR for Japanese persimmon. Copyright © 2015 John Wiley & Sons, Ltd.     

宽带固定无线接入技术及市场分析

本文综述了当前几种发展极为迅速的宽带固定无线接入技术，讨论了其演变过程及在国内的发展现状，并总结了无线接入在未来的主要发展趋势。     

A Study of Schemes for Internet Data Transmission Based on CATV Networks

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A Resource Allocation Approach for the Generation of Service-Dependent Demand Matrices for Communications Networks

Estimating point-to-point demands from partially available information, such as total demand volumes originating and terminating at nodes and traffic volumes routed on links, has significant applications in various areas, such as communications network planning and transportation planning. Existing methods include matrix and link scaling methods, statistical methods, more complex mathematical programming models, and forecasting using demographic data. We present a new mathematical programming model based on equitable resource allocation. The model considers multiple services, e.g., data, video, and voice, and generates a point-to-point demand matrix for each service. Originating and terminating demands for each service and link loads, aggregated over all services, are viewed as resources. Each point-to-point demand is associated with a performance function that measures its weighted, normalized deviation from a target defined by a service-dependent community of interest matrix. The model formulation has a lexicographic minimax objective function and multiple knapsack resource constraints. The model has an intuitively appealing interpretation and a specialized algorithm can generate demand matrices for large network problems very fast.     

一种新型校园社区网建设方案

提出了一套校园网建设方案,通过该方案的实现,使教职员工可用一张201卡进行语音通信和上网.极大地方便了师生的工作和学习;同时通过灵活的计费策略,很好地解决了学生上网对网络资源和宽带过渡占用的问题.保证了网络资源得以充分的利用.