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71.
K. M. A. Salam Hidekazu Konishi Masahiro Mizuno Hisashi Fukuda Shigeru Nomura 《Applied Surface Science》2002,190(1-4):88-95
Polycrystalline (1−x)Ta2O5−xTiO2 thin films were formed on Si by metalorganic decomposition (MOD) and annealed at various temperatures. As-deposited films were in the amorphous state and were completely transformed to crystalline after annealing above 600 °C. During crystallization, a thin interfacial SiO2 layer was formed at the (1−x)Ta2O5−xTiO2/Si interface. Thin films with 0.92Ta2O5–0.08TiO2 composition exhibited superior insulating properties. The measured dielectric constant and dissipation factor at 1 MHz were 9 and 0.015, respectively, for films annealed at 900 °C. The interface trap density was 2.5×1011 cm−2 eV−1, and flatband voltage was −0.38 V. A charge storage density of 22.8 fC/μm2 was obtained at an applied electric field of 3 MV/cm. The leakage current density was lower than 4×10−9 A/cm2 up to an applied electric field of 6 MV/cm. 相似文献
72.
B. Hannoyer A. A. M. Prince M. Jean R. S. Liu G. X. Wang 《Hyperfine Interactions》2006,167(1-3):767-772
Crystalline LiFePO4 has been synthesized using solid-state, spray pyrolysis, and wet chemical methods. The crystal parameters were obtained from Rietveld’s refinement methods of the X-ray diffraction patterns. A detailed investigation of the Fe valency carried out using Mössbauer spectroscopy at room temperature indicates that Fe is predominantly present in its bivalent state. 相似文献
73.
We consider a composite material composed of fibres included in a resin which becomes solid when it is heated up (reaction of reticulation). The mathematical modelling of the cure process is given by a kinetic equation describing the evolution of the reaction of reticulation coupled with the heat equation. In this paper, we are interested in the computation of approximate solutions. We propose a family of discretized problems depending on two parameters (β1, β2) ε [0, 1]2 which split the linear and non‐ linear terms in implicit and explicit parts. We prove the stability and convergence of the discretization for any (β1, β2) ε [½, 1 ] × [0, 1]. We present also some numerical results. Copyright © 2006 John Wiley & Sons, Ltd. 相似文献
74.
A. C. Orifici R. S. Thomson R. Degenhardt C. Bisagni J. Bayandor 《Mechanics of Composite Materials》2007,43(1):9-28
Analysing the collapse of skin-stiffened structures requires capturing the critical phenomenon of skin-stiffener separation,
which can be considered analogous to interlaminar cracking. This paper presents the development of a numerical approach for
simulating the propagation of interlaminar cracks in composite structures. A degradation methodology was introduced in MSC.Marc,
which involved the modelling of a structure with shell layers connected by user-defined multiple-point constraints (MPCs).
User subroutines were written that employ the virtual crack closure technique (VCCT) to determine the onset of crack growth
and modify the properties of the user-defined MPCs to simulate crack propagation. Methodologies for the release of failing
MPCs are presented and are discussed with reference to the VCCT assumption of self-similar crack growth. The numerical results
obtained by using the release methodologies are then compared with experimental data for a double-cantilever beam specimen.
Based on this comparison, recommendations for the future development of the degradation model are made, especially with reference
to developing an approach for the collapse analysis of fuselage-representative structures.
Russian translation published in Mekhanika Kompozitnykh Materialov, Vol. 43, No. 1, pp. 15–42, January–February, 2007. 相似文献
75.
The nanogranular nature of C-S-H 总被引:6,自引:0,他引:6
Despite its ubiquitous presence as binding phase in all cementitious materials, the mechanical behavior of calcium-silicate-hydrates (C-S-H) is still an enigma that has deceived many decoding attempts from experimental and theoretical sides. In this paper, we propose and validate a new technique and experimental protocol to rationally assess the nanomechanical behavior of C-S-H based on a statistical analysis of hundreds of nanoindentation tests. By means of this grid indentation technique we identify in situ two structurally distinct but compositionally similar C-S-H phases heretofore hypothesized to exist as low density (LD) C-S-H and high density (HD) C-S-H, or outer and inner products. The main finding of this paper is that both phases exhibit a unique nanogranular behavior which is driven by particle-to-particle contact forces rather than by mineral properties. We argue that this nanomechanical blueprint of material invariant behavior of C-S-H is a consequence of the hydration reactions during which precipitating C-S-H nanoparticles percolate generating contact surfaces. As hydration proceeds, these nanoparticles pack closer to center on-average around two characteristic limit packing densities, the random packing limit (η=64%) and the ordered face-centered cubic (fcc) or hexagonal close-packed (hcp) packing limit (η=74%), forming a characteristic LD C-S-H and HD C-S-H phase. 相似文献
76.
Kwangwon Park 《Talanta》2007,73(4):791-794
It is very challenging to decompose a plastic product for the purpose of analysis of hazardous elements contained. To circumvent such technical problem, it is imperative that an analyst employ a nondestructive analytical method free of any pretreatments. The analytical results of the concentrations of toxic metals such as Cd and Cr in polypropylene for seven samples at two different levels were obtained using the instrumental neutron activation analysis. This work was intended ultimately to establish certified reference materials (CRMs) of these metals in the polypropylene, traceable to the SI. The uncertainties associated with the analytical procedures were estimated in accordance with the ISO guideline. The results were subsequently validated by a comparison with those for CRM-680 and −681 of the Bureau Communautaire de Reference (BCR), which demonstrated acceptable agreement within their uncertainty ranges. 相似文献
77.
本文介绍了一种新近研制的光折聚合物。实验表明,除去吸收和反射,入射光束经聚合物后的第一布拉格衍射效率高达86%,材料也显示出双光束耦合的净增益高于240cm^-1。这些结果表明,这种新型研制的光折聚合物材料是替代无机光折晶体的实用材料。 相似文献
78.
介绍了几种结构合理的超导/半导兼容材料的制作技术及其测试结果,重点讨论了超导体(YBCO)与半导体(Si,CaAs)间缓冲层的选取,并对这几种复合材料的性能作了较详细的分析。 相似文献
79.
80.
系统采用XENIX操作系统和FoxBASE~+关系型数据库。本文简要介绍了该系统设计的基本原理、系统功能,并比较了XENIX多用户系统与DOS单用户系统的优缺点。 相似文献