Thermal stability of poly(mono-n-alkylitaconates) and mono-n-alkylitaconate-co-vinylpyrrolidone copolymers I

Poly(monoitaconates) containing octyl, decyl and dodecyl groups and random monoalkylitaconate-co-vinylpyrrolidone copolymers were studied by thermogravimetric analysis. Copolymers of mono-n-octylitaconate (MOI), mono-n-decylitaconate (MDI), and mono-n-dodecylitaconate (MDoI), respectively, with N-vinyl-2-pyrrolidone (VP) of different compositions were studied by dynamic thermogravimetric analysis. The thermal stability of the copolymers depends on the structure of the monoitaconate comonomer and on the composition of the copolymer The kinetic analysis of the degradation data shows that the thermal decomposition of these copolymers can be described by several kinetic orders depending on the copolymer and on the composition. The relative thermal stability of the copolymers increases as the VP content increases and as the length of the side chain of the itaconate increases, following the same trend as the flexibility of the copolymers in solution.     

新型非蒸散消气剂的激活温度和吸气性能的实验研究

对主要成分为Zr和Co的新型非蒸散消气剂进行了活化温度及吸气性能的实验研究。实验表明其活化温度为200—250℃，对N2，H2等活性气体有很好的抽速，对惰性气体He等无抽速。     

High temperature transport kinetics in heteroepitaxial LaFeO3 thin films

Heteroepitaxial LaFeO₃(1 1 0) thin films with a thickness of 150 nm were grown on LaAlO₃(0 0 1) by reactive sputtering in an inverted cylindrical magnetron geometry. Equilibrium conductivity was measured as a function of partial pressure of oxygen at T=1000 °C, and logσ plotted vs. logP(O₂) showed a minimum in conductivity for P(O₂)=10⁻¹¹ atm and a linear response between 10⁻¹⁰ and 1 atm. This linear response makes thin films of LaFeO₃ a promising material for oxygen sensor applications. We have also measured the time response of the film conductivity upon an abrupt change in the partial pressure of ambient oxygen from 10⁻² to 10⁻³ atm, which was determined at 60 s for T=700 °C and <3.5 s at T=1000 °C.     

在p+GaAs体单晶材料上进行的NEA活化实验

NEA活化实验是利用体单晶材料进行的,未经任何外延或真空解理手续。为确立活化工艺,特别是表面清洁处理规范,作了相应AES分析。借助于测量样品附近高纯Al的熔点以校准及控制样品表面的温度。在不太好的本底真空(2×10^-7—6×10^-7Pa)条件下,活化好的GaAs样品之白光光电灵敏度可达1000μA/lm以上。     

中能区光学势的温度效应

本文在Skyr}e相互作用、核物质近似和自洽半经典方法的基础上，将微观光学势的自洽研究推J“到中能区(60-r300MeV)，研究了”+907r在该能区光学势的径向形状和温度效应     

Microstructure and thermal behavior of Sn-Zn-Ag solders

The microstructure and thermal behavior of the Sn-Zn-Ag solder were investigated for 8.73–9% Zn and 0–3.0% Ag. The scanning electron microscopy (SEM) analysis shows the Ag-Zn compound when the solder contains 0.1% Ag. X-ray diffraction (XRD) analysis results indicate that Ag₅Zn₈ and AgZn₃ become prominent when the Ag content is 0.3% and above. Meanwhile, the Zn-rich phase is refined, and the Zn orientations gradually diminish upon increase in Ag content. The morphology of the Ag-Zn compound varies from nodular to dendrite structure when the Ag content increases. The growth of the Ag-Zn compounds is accompanied by the diminishing of the eutectic structure of the Sn-9Zn solder. Differential scanning calorimetry (DSC) investigation reveals that the solidus temperature of these solders exists at around 198°C. A single, sharp exothermic peak was found for the solders with Ag content less than 0.5%. Liquidus temperatures were identified with the DSC analysis to vary from 206°C to 215°C when the Ag content ranges from 1.0% to 3.0%     

基于GMS97C2051的串行多路温度数据采集系统的设计

介绍了一种以GMS97C2051单片机为核心、利用新型集成化智能温度数字传感器DS1621实现的多路温度数据采集系统,利用MAX3232完成电平转换并将采集到的数据通过串行接口传送给上位机,在上位机中实现显示、控制等功能.叙述了DS1621的特性及工作方式,给出了硬件电路原理和软件流程,以及系统与上位机通信程序源代码.该系统实现了现场多点温度数据的采集,明显提高了检测可靠性和检测效率.现场实验证明该系统在测试过程中工作稳定,满足设计要求.     

Resonant Raman scattering from a spin density wave insulator

We present a calculation of the electronic Raman cross section for the scattering of light across the energy gap of an antiferromagnetic insulator. The antiferromagnet is described in terms of a spin density wave state for the Hubbard model at half filling. We consider the coupling of the light to the current density and the inverse mass tensor on equal footing. A comparison of the cross section for different scattering geometries is given.     

幕帘涂布工艺

本文主要介绍涂布与塞孔工艺,并对此工艺进行特征描述与释疑。     

光纤Bragg光栅监测钢筋混凝土结构应变的实验研究

研究了光纤Bragg光栅在钢筋混凝土结构应变监测中的应用。对其应变、温度灵敏系数进行标定,将其埋设在钢筋混凝土梁内,实现对结构内部应变的监测,并对其工作状态做出评价。实验结果与理论值、传统监测手段监测结果一致。研制出一种钢管封装Bragg光栅温度传感器监测温度,对光纤Bragg光栅的应变与温度的同时测量进行了研究。