安徽电信宽带骨干传输网构建方案介绍

随着IP业务的超常规发展，传输瓶颈日渐显现出来；以安微电信骨干传输网的发展规划为例，介绍安微电信宽带骨干传输网的构建方案。     

GMPLS中基于子网保护的LSP保护机制探讨

主要探讨了GMPLS中基于子网保护的LSP保护机制。首先描述了子网保护机制的含义;然后,重点分析了子网保护机制的实现过程,并对子网保护机制中存在的入口问题提出了相应的解决方案;最后,通过比较说明了该保护机制的优点。     

金属有机框架(MOFs)材料在锂离子电池及锂金属电池电解液中的应用

总结了金属有机框架(MOFs)材料在锂离子电池电解液中的研究进展.通过归纳锂离子电池长期存在的一些缺陷,随后将MOFs材料作为离子筛、人造负极保护层、准固态电解质以及用来调节电解液构型,使得锂离子电池的性能得到显著提升.最后,基于MOFs材料本身的特性,还对MOFs材料在电化学储能领域中的后续应用进行了合理地前瞻性展望...     

Microwave-assisted synthesis of 1,3-benzodioxole derivatives from catechol and ketones or aldehydes

An efficient synthetic procedure for the preparation of a diverse library of 1,3-benzodioxoles was developed by applying controlled microwave heating in comparison with currently available conventional heating. Reactions were completed in less than 3 h. The isolation of product is simple, the isolated yields are good to excellent, and this method is applicable to large scale production.     

Microwave assisted mild, rapid, solvent-less, and catalyst-free chemoselective N-tert-butyloxycarbonylation of amines

Microwave assisted simple, rapid, solventless, and catalyst-free chemoselective method for the protection of amino group in aromatic, aliphatic, heterocyclic, aralkyl amines, phenyl hydrazine, and amino acid esters in good to excellent isolated yield (83-98%) in short reaction time (2-12 min) has been reported.     

基于共铁塔的基站天线对在线监测设备电磁影响研究

随着共享铁塔建设的全面开展,基站天线对同塔布置的输电线路在线监测设备的电磁干扰问题开始凸显。结合在线监测设备的电磁兼容标准,揭示了基站天线对在线监测设备的电磁干扰机理。通过建立电大尺寸金属散射体无源干扰求解模型,采用物理光学-矩量法混合算法求解基站天线在铁塔表面产生的感应电流,获得了在线监测设备处的散射电场值。以山东35 kV 共享铁塔为算例,以天线工作频率、天线与在线监测设备之间的间距为变量,分析了铁塔塔头型式、天线功率、天线倾角等不同工况下的散射电场变化规律。结果表明,铁塔塔头型式对干扰影响较小,而天线功率和倾角对干扰影响较大。以此为计算依据,建议天线与在线监测设备之间的防护间距为18m。     

实验室安全环保意识的调查与分析——以中山大学化学类专业学生为例

A survey about students' laboratory safety and environmental protection consciousness was performed in the freshmen majored in chemistry at Sun Yat-Sen University. Results showed that laboratory safety and environmental protection consciousness of most students' are weak. After analyzing the reasons, we put forward some suggestions. Cultivating students' laboratory safety and environmental protection consciousness should be carried out from several aspects such as emphasizing and regulating from school level, training in laboratory teaching, maintaining good cultural atmosphere of laboratory, as well as providing perfect laboratory safety and environmental protection facilities. We should guide students to actively learn knowledge and skills of laboratory safety and environmental protection in order to develop their good behavior and raise their consciousness.     

Efficient tetrahydropyranyl and tetrahydrofuranyl protection/deprotection of alcohols and phenols with Al(OTf)3 as catalyst

A simple and efficient method for the conversion of alcohols and phenols into their corresponding THP and THF ethers at room temperature has been developed using 1 mol % aluminium triflate as catalyst. The deprotection reaction in the presence of methanol using Al(OTf)₃ was equally successful and could be performed at ambient temperature in high yields.