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61.
Atsuhisa Mimoto Sojiro Kon Takuya Motomura Minoru Inaba 《Journal of fluorine chemistry》2005,126(7):1101-1110
The Ni-based alloys, such as Ni-Co, Ni-Mn, Ni-Ag, Ni-Cu, Ni-Al and Ni-Si, prepared by hot isostatic pressing (HIP) at 1000 °C under 2 × 108 Pa for 2 h were employed as the anodes for electrolytic production of NF3. The current efficiencies for NF3 formation were 42-38, 52-40, 52-47, 63-62, 50 and 41% for Ni-Co, Ni-Mn, Ni-Ag, Ni-Cu, Ni-Al and Ni-Si alloys, respectively. The current efficiencies only on Ni-Cu alloys with Cu concentrations lower than 10 mol% were almost the same as those on Ni sheet and HIPed Ni anodes, whereas those on the other alloys used in this study were smaller compared with those on both Ni anodes. On the other hand, the current losses caused by anodic dissolution of Ni-Co, Ni-Mn, Ni-Ag, Ni-Cu, Ni-Al and Ni-Si alloy electrodes were 7.95-4.42, 6.40-7.02, 5.60-6.30, 3.34-6.33, 5.10 and 0.18%, respectively. The anode consumptions of Ni-5 mol% Cu and Ni-5 mol% Si alloys were almost the same or smaller compared with those of Ni sheet and HIPed Ni electrodes, though those of other alloys used were large compared with those of both Ni anodes. Consequently, addition of Cu to the nickel matrix is available for a cheaper cost of anode with keeping a same current efficiency as that on the Ni anode and addition of Si to the nickel matrix is effective for decreasing anode consumption largely. A Ni sheet electrode containing a trace of impurities, such as Co, Mn, Ag and Al, is also favorable as the anode for electrolytic production of NF3. 相似文献
62.
M. Lundbäck 《Polymer Degradation and Stability》2006,91(5):1071-1078
Plaques of branched polyethylene stabilized with 0.1 wt.% 4,4′-thiobis(6-tert-butyl-3-methylphenol) [Santonox® R] were aged at different temperatures between 75 and 95 °C in anaerobic (nitrogen or water) and aerobic (air or water saturated with air) media. Antioxidant concentration profiles were obtained by oxidation induction time (OIT) measurements using differential scanning calorimetry. Results obtained by high performance liquid chromatography of extracts confirmed that the gradual decrease in OIT with increasing ageing time was due to migration of antioxidant to the surrounding medium. The antioxidant concentration profiles along the plaque thickness direction were flat in the plaques aged in the non-aqueous media indicating that the migration of antioxidant to the surrounding medium was controlled by the low evaporation rate at the material boundary. Crystals of antioxidant were detected by optical microscopy on the samples exposed to nitrogen. The similarity of the antioxidant concentration profiles obtained after ageing in nitrogen and in air suggested that the fraction of the antioxidant oxidized is negligible in comparison with the loss of antioxidant by migration to the surrounding media. The antioxidant concentration profiles along the plaque thickness direction obtained after ageing in water were less flat, suggesting faster dissolution in the water phase than evaporation in the case of non-aqueous ageing. The antioxidant diffusivity could be determined from the aqueous experiments and was in reasonable agreement with data reported by Moisan. For the samples exposed to water, the loss of antioxidant was faster from the samples exposed to water saturated with air. This difference is attributed to a faster degradation of the antioxidant in the oxygen-containing water phase increasing the mass transport from the polymer phase boundary to the water phase. 相似文献
63.
This paper presents an approach to power-conserving routing of ad hoc mobile wireless networks. This approach relies on entropy-constrained routing algorithms, which were developed by utilizing the information-theoretic concept of the entropy to gradually reduce the uncertainty associated with route discovery through a deterministic annealing process. Entropy-constrained routing algorithms were tested using a single performance metric related to the distance between the nodes and to the power consumption associated with packet transmission. This paper also expands the versatility of entropy-constrained routing algorithms by making them capable of discovering routes based on multiple performance metrics. In this study, the second performance metric employed for route discovery relied on the power availability in the nodes of the network. The proposed routing approach was evaluated in terms of the power consumption associated with the routing of packets over an ad hoc mobile network in a variety of operating conditions. 相似文献
64.
随着微电子技术的飞速发展,高速大规模集成电路的广泛应用,高速系统的设计也越来越受到重视,高速系统与低速系统的PCB设计有很大不同。本文从实际设计的角度介绍了高速系统中电源、接地、时钟电路、过孔等的设计和需要注意的问题。 相似文献
65.
使用PSD作为大口径光学元件表面加工质量的评价参数,针对不同的波前调制进行了初步的模拟计算,得到了不同调制频率和不同调制深度情况下的PSD曲线变化情况。当调制频率不同时,PSD曲线的突变部分会发生相应的频移,调制频率高则突变发生在空间频率较高的频段,同时PSD峰值不变。相对应调制深度不同时,PSD曲线的突变部份峰值发生变化,调制深度大则峰值大,与此同时峰值出现的位置不会发生变化。计算和分析结果表明PSD分析结果能够在频率域反应出元件表面受到的不同程度的调制信息。 相似文献
66.
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68.
Using a field-programmable gate array (FPGA) development board, a digital signal processor (DSP) builder, and the phase-to-amplitude conversion principle, a low-cost system for measuring the amplitude-to-amplitude (AM/AM) and amplitude-to-phase (AM/PM) distortion curves of radio frequency (RF) power amplifiers (PAs) is presented. The state of the art based on the measurements and preliminary studies of AM/AM and AM/PM distortion curves is discussed. A full digital control of the test bed simulated/emulated in Matlab/Simulink is introduced to recalculate the known AM/AM and AM/PM measurements stored as look-up table (LUT). Finally, the low-cost system comprises the memory polynomial model (MPM) that involves the nonlinearity order and memory effects of real PAs. 相似文献
69.
《Microelectronics Reliability》2014,54(9-10):1867-1871
Power cycle reliability of Cu nanoparticle joint has been studied for high temperature operation of power devices. Al2O3 heater chips and Cu–65 wt% Mo baseplates were joined by Cu nanoparticles and Sn–0.7Cu and power cycle tests of 65/200 °C and 65/250 °C were carried out on the joints. The Cu nanoparticles were prepared by reducing Cu carbonate in ethylene glycol with dodecanoic acid + dodecyl amine (C12) and decanoic acid and decyl amine (C10) as capping agents. A power cycle test of 65/200 °C did not inflict severe damage on the Cu nanoparticle joints so that there were not many cracks formed after 3000 cycles. Vertical cracks were formed in the C12 Cu nanoparticle joint after 3000 cycles of 65/250 °C test, however the maximum temperature during the power cycle test did not change at all because vertical cracks did not have an effect on preventing heat flow. On the contrary, lateral cracks were completely formed in the Sn–0.7Cu soldered joint after 200 cycles of 65/200 °C test and in the C10 Cu nanoparticle joint after 360 cycles of 65/250 °C test. In these experiments, the maximum temperatures were rapidly increased because heat conduction was prevented across the formed lateral cracks. 相似文献
70.
This paper presents a link adaptation algorithm dedicated for 100 Gbps wireless transmission. Interleaved Reed-Solomon codes are selected as forward error correction (FEC) algorithms. The redundancy of the codes is selected according to the channel bit error rate (BER). The uncomplicated FEC scheme allows implementing a complete data link layer processor in an FPGA (field programmable gate array). In our case, we use the Virtex7 FPGA to validate the functionality of our implementation. The proposed FPGA-processor achieves 169 Gbps throughput. Moreover, the implementation is synthesized into 40 nm CMOS technology and the described link adaptation algorithm allows reducing consumed energy per bit to values below 1 pJ/bit at BER <1e−4. With higher BER, the energy increases up to ∼13 pJ/bit. 相似文献