Quantification of Tin and Lead in Binary Alloys Using Voltammetry of Immobilized Microparticles

Voltammetry of immobilized microparticles (VMP) has been used in this work for the quantitative determination of tin and lead particles in their binary alloys. Carbon paste electrodes, which contained small amounts of tin and lead or their mixtures, were used as working electrodes and square wave voltammograms of each electrode were recorded. Quantification was performed using optimum experimental conditions, obtained by an experimental design technique. The calibration was made by measuring the percentage peak height of each metal taking the sum of peak currents of the both metals as 100 %. The results were compared with quantitative results of X‐ray fluorescence (XRF) technique to evaluate the capability of VMP method in its quantitative determination of solid samples.     

A mammographic phantom to measure mean glandular dose by thermoluminescent dosimetry

We have designed a phantom to evaluate mean glandular dose (MGD) as part of the regulatory dosimetry control for mammographic equipment. The phantom is constituted by TLD-100 thermoluminescent dosemeters (TLDs) inserted within semicircular plates of acrylic. Different groups of TLDs are used to determine entrance surface air kerma and half-value layer (HVL). Calibration of both tasks has been performed using a Senographe 2000D system and an ionization chamber. The phantom has been tested in five clinical systems. The HVL and MGD obtained by this method agree, on average, within 3%, with those from standard procedures based on the use of ionization chambers. The phantom MGD measurements have a combined uncertainty better than 10% (k = 1).     

A global pinching theorem for surfaces with constant mean curvature in

Let be a compact immersed surface in the unit sphere with constant mean curvature . Denote by the linear map from into , , where is the linear map associated to the second fundamental form and is the identity map. Let denote the square of the length of . We prove that if , then is either totally umbilical or an -torus, where is a constant depending only on the mean curvature .

     

变频调速应用技术（十一）——第六讲经济效益赞变频（上）

本文分析了节能问题的几个方面。主要有：负载需求与节能的关系，调速方法与节能的关系，以及大马拉小车的节能问题等。     

Some remarks on compact constant mean curvature hypersurfaces in a halfspace of ℍ n+1

We consider embedded compact hypersurfacesM in a halfspace of hyperbolic space with boundaryM in the boundary geodesic hyperplaneP of the halfspace and with non-zero constant mean curvature. We prove the following. Let {M _n } be a sequence of such hypersurfaces withM _n contained in a disk of radiusr _n centered at a point P such thatr _n 0 and that eachM _n is a large. H-hypersurface,H > 1. Then there exists a subsequence of {M _n } converging to the sphere of mean curvatureH tangent toP at. In the case of smallH-hypersurfaces orH 1, if we add a condition on the curvature of the boundary, there exists a subsequence of {M _n } which are graphs. The convergence is smooth on compact subset of ³ .     

一种用于GSM系统的神经网络均衡器

在泛欧GSM移动通信系统中，由于存在码间干扰，必须采用信道均衡技术。常用的最大似然序列估计(MLSE)均衡器采用维特比算法(VA)，它只能用于具有较小时延扩展的信道。本文给出了一种适用于GSM系统的部分连接神经网络均衡器．其复杂度与信道的时延扩展成正比．特别适用于具有较大时延扩展的恶劣信道。为了消豫神经网络局部极小点引起的性能恶化．我们采用了均场退火技术。本文提出的均衡器既适于用模拟集成电路实现．又适于用数字集成电路实现。计算机仿真表明本文的方法具有比最常用的16状态和32状态VA更好的性能。     

H_2辉光放电清洗时轰击器壁的离子能量测量与分析

一、引言 辉光放电是清洗锻炼环流器真空室器壁的有效手段。H_2辉光放电时,氢离子轰击器壁与器壁中的C和O发生化学反应,生成CH_4,H_2O等气体;同时,这些离子提供能量使得吸附在器壁表面的杂质气体脱附,从而被泵出真空室外,达到清洗锻炼的目的。由于辉光放电时,离子轰击的能量较高,会引起一定的溅射沉积。我们在模拟真空室(六通装置)进行了辉光放电,对各种参数下的离子能量进行了测量,从中找出了离子能量与极间电压(阳极与器壁之间的电压)、放电电流、以及气压、离子流密度之间的某些关系。     

Work function of metals: Relation between theory and experiment

Theoretical approaches to calculation of work function within jellium model and the problem of extension of this model to include the lattice corrections to the work function are briefly discussed. Lattice corrections to the work function obtained from the experiment are estimated and compared with those calculated theoretically.

It is found that the mean value of the experimental lattice correction <δψ_hkl>_hkl compared to the mean work function is negligible. It is stated that the mean work function can be treated as a material constant characterizing a given metal, such as, e.g., binding energy.An expression for the dependence of jellium work function on r_s, valid in a metallic range of r_s, is given. A comparison between then theoretical and experimental results is presented and the role of correlation energy is examined. It is shown that more accurate approximations of the correlation energy than that given by Wigner's formula lead to a better agreement with experiment. A simple model is presented for explanation of work function changes on single crystal planes. Some recent results concerning the thermal dependence of work function are given. The dependence of the work function on the degree of coverage is discussed both for alkali and non-alkali atoms adsorption. Theoretical models are briefly reviewed and comparison between theory and experiment is made. A simple model is presented for explanation of the work function variation on rough planes in metallic non-alkali atoms chemisorption.     

Design of smallest size two-dimensional linear-phase FIR filters with magnitude error constraint

This paper presents an online procedure that produces the smallest feasible size of two-dimensional FIR filters with prescribed magnitude error constraint. The procedure uses the mean square normalized error of constrained and unconstrained least-square filters to produce the initial and the subsequent sizes that converge to the smallest feasible one in a few iterations, where the constrained least-square filters are defined as the least-square filters satisfying the magnitude error constraint. The procedure finally returns a smallest size filter that satisfies the magnitude error constraint and has least total squared magnitude error. Design examples of diamond-shaped, rectangular, and elliptic filters are provided, and comparisons with an exhaustive search are given.     

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利用分裂的屏蔽氢不透明度模型计算了Ar、Kr、Xe惰性元素混合物随光子能量变化的不透明度以及Rosseland平均不透明度。研究了温度为100～250eV,密度为0.5～2g·cm-3范围内惰性元素混合物的Rosseland平均不透明度与混合物质、混合比例、温度和密度的密切关系。结果显示,Ar-Xe混合以及Xe-Kr混合后的Rosseland平均不透明度比它们为纯元素时有较大的增加;而Ar-Kr混合后的Rosseland平均不透明度则比纯Kr低。通过对比纯惰性元素随光子能量变化的不透明度峰、谷值,分析了造成混合后不透明度增加或降低的原因,同时给出了获得惰性元素混合物平均不透明度为最大时的混合比例。