MEMS微波功率传感器的三维等效电路模型

为了得到热电式MEMS微波功率传感器的三维温度分布和时间常数,建立了传感器的三维等效电路模型。首先根据热-电参数的等效关系和传感器的结构建立等效电路模型。接着,对等效电路的单元模块进行理论分析。最后,根据建立的三维等效电路模型研究传感器的温度分布和响应时间。传感器的灵敏度为0.076 mV/mW@10 GHz,时间常数为56.24μs。测试结果表明,传感器的灵敏度为0.06 mV/mW@10 GHz,时间常数为85μs。所建立的三维等效电路模型不但可以得到微波功率传感器的响应时间,而且可以准确地得到热量在衬底的耗散情况。因此,本研究对热电式MEMS微波功率传感器设计具有一定的参考价值。     

MEMSE类放大器

对采用 MEMS开关的 E类放大器进行了原型仿真 ,并且通过工艺流片制作 MEMS开关 ,搭建 E类放大器电路进行测试 .测试结果显示 ,这种机械式的放大器同样能实现有源放大器的功能 .测试得到的放大器实际效率与原型模拟结果一致 ,而放大器的功率增益高达 2 0 0 0 .     

微型电磁继电器的制作和仿真分析

介绍了一种基于MEMS技术的微型电磁继电器的制作过程和仿真分析.这种微继电器的大小约是4mm×4mm×0.5mm,主要采用普通的微加工技术来完成全部制作工艺.与传统继电器相比,这种继电器采用平面线圈来代替螺线管线圈,有利于MEMS工艺,并且提出了一种双支撑的悬臂梁结构做为活动电极,具有较高的灵敏性和稳定性.另外,还进行了一些有关线圈通过激励电流后对活动电极产生电磁力的理论计算和仿真分析,利用这些结果可以对这种电磁继电器的结构和参数进一步优化.     

基于旋转式反射镜的飞行视觉系统设计

在MEMS麦克风贴片工艺中,真空吸嘴吸取MEMS芯片以后需要进行芯片位姿的精确校正。为实现高速高精度贴片功能,提出了一种基于旋转式反射镜的飞行视觉系统,该方案利用齿轮齿条将吸嘴的升降运动转化为反射镜的旋转运动,通过设计齿轮参数,实现反射镜不干涉吸嘴的拾放功能。当反射镜旋转到与水平位置夹角呈45°时,视觉系统可以获得MEMS芯片的静止的清晰图像,CCD相机采集一幅图像后,在贴片头飞行的过程中,控制系统完成MEMS芯片的位置和角度的校正。实验结果表明,该系统可以获取高质量MEMS芯片图像。该系统结构简单紧凑,成像无失真,不限制贴片头的运动轨迹,显著提高了MEMS芯片的贴片质量和贴片效率,可广泛地应用于贴片机系统中。     

顶空气相色谱法测定聚氯乙烯固体药用硬片中氯乙烯单体含量的测量不确定度评定

依据CNAS-GL06,对顶空气相色谱法测定聚氯乙烯固体药用硬片中氯乙烯单体含量的测量不确定度进行系统分析,找出影响测量结果不确定度的主要因素。对各不确定度分量进行了评定和量化,计算了合成标准不确定度和扩展不确定度,聚氯乙烯固体药用硬片中氯乙烯单体含量的测定结果表示为(4.17±0.18)×10-7,k=2。     

固相微萃取-气相色谱法测定食品包装材料中残留有机溶剂

提出了一种以固相微萃取与气相色谱-氢火焰联用技术为基础的测定食品包装材料中15种常用有机溶剂(苯类、醇类、酮类、酯类等)的方法。选择聚二甲亚砜作为固相微萃取的萃取相,采用DB-624毛细管色谱柱进行分离。在优化的试验条件下,15种有机残留溶剂在20min内能很好地分离,15种溶剂的测定下限(10S/N)为0.08～0.69μg.dm-2。加标回收率为60.0%～115.0%,相对标准偏差(n=5)为2.17%～8.34%。     

固相萃取-高效液相色谱法同时测定食品塑料包装材料中9种光稳定剂

建立了同时测定食品塑料包装材料中9种紫外光稳定剂含量的高效液相色谱方法。样品用甲醇-乙酸乙酯混合溶剂超声提取,经固相萃取小柱净化后,以ZORBAX SB-C18柱(250 mm×4.6 mm, 5 μm)为分离色谱柱,甲醇和水为流动相,梯度洗脱,以310 nm为检测波长进行定性、定量分析。该方法前处理简单、易操作,9种紫外光稳定剂分离效果良好。9种紫外光稳定剂在0.2～10 mg/L范围内呈良好的线性关系,线性相关系数大于0.999;方法检出限为0.05～0.1 mg/L;实际样品中的加标回收率为70.2%～89.0%,相对标准偏差为0.4%～4.5%。该方法简单、准确,能够满足食品塑料包装材料中紫外光稳定剂的检测要求。     

Study of migration of active components of phosphorescent oxygen sensors for food packaging applications

A study of migration of the active components of oxygen sensors into food is presented. Six types of sensors, based on different oxygen sensitive dyes (two metalloporphyrins and one ruthenium dye), polymers (polystyrene and polysulfone) and support materials, were exposed to a number of standard ‘food simulants’ recommended by FDA/EU guidelines and then assayed for migration or sensor components and changes in oxygen calibration. Both metalloporphyrin sensor dyes leached only in olive oil and in 95% ethanol (used as a positive control), at maximum levels of 19.22 μg/dm² for PtOEPK and 113.96 μg/dm² for PtTFPP. The RuDPP dye showed maximum leaching in 95% ethanol (25.19 μg/dm²) while also migrating in an acidic aqueous simulant. Planar supports such as polyester tended to enhance the stability of the sensor. Migration of the styrene monomer from the polystyrene encapsulation medium was concluded to be low enough to be insignificant. Migration of sensor components was shown to correlate with the changes in sensor response to oxygen. Based on these results, sensor combinations were ranked on the basis of their resistance to leaching and their general stability, safety and suitability for use on a large scale in packaged foods and related food applications was proven.     

单扫示波极谱法测定食品包装材料中双酚A的研究

研究发现，在0.12mol/L Na2HPO4-KH2PO4(pH7.5)底液中，双酚A于峰电位（Ep)-1.0V(vs.SCE)处产生灵敏的极谱还原波，该波的二阶导数峰电流（ip)与双酚A浓度在2.0-10.0mg/L范围内呈良好的线性关系，检出限为1.0mg/L，萃取后测定，检出限为0.1mg/L。本法操作简便、快速、准确。用于食品包装材料中双酚A含量的测定，结果令人满意。     

Enhanced Quality Control of Recycled Paperboard for Food Packaging

A method is reported for the industrial quality control of recycled paperboard for food contact applications. Benzophenones, phthalates, and diisopropyl naphthalene were selected as contamination markers. These compounds are commonly found in recycled paperboard packaging and are known to migrate even into dry nonfatty foods. The method was used to analyze commercial recycled board and involved sample pretreatment by accelerated solvent extraction, evaporation, and purification of the extract, and analysis by gas chromatography–mass spectrometry. The accelerated solvent extraction yields were compared with those obtained by Soxhlet extraction and extraction by immersion, and the recoveries of optimized procedures were estimated. The optimized method showed good repeatability, intermediate precision, and sensitivity. Because of the simplicity and partial automation, this method has potential application for the characterization of recycled paperboard.