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51.
Kamal YT Mohammed Musthaba S Singh M Parveen R Ahmad S Baboota S Ali I Siddiqui KM Arif Zaidi SM 《Biomedical chromatography : BMC》2012,26(10):1183-1190
An attempt has been made to develop and validate a simultaneous HPLC method for novel approach of drug release via oil‐in‐water (o/w) nanoemulsion formulation and Habb‐e‐Khardal Unani tablet containing piperine and guggul sterones E and Z as main ingredients. Nanoemulsion was prepared by titration method using sefsol‐218 as an oily phase, cremophor‐EL as a surfactant, transcutol as a co‐surfactant and distilled water as an aqueous phase. The formulation was optimized on the basis of thermodynamic stability and dispersibilty test. The nanoformulation was evaluated for particle size, surface morphology, electrical conductivity and viscosity determination. The in vitro dissolution was carried out by dialysis bag method. Drugs were quantified using an HPLC method developed in‐house with a C18 column as stationary phase and acetonitrile and water as mobile phase at λmax of 240 nm. The optimized formulation showed higher drug release, lower droplet size and less viscosity as compared with the conventional Habb‐e‐Khardal Unani tablet. The present study illustrated the potential of nanoemulsion dosage form in improving biopharmaceutic performance of piperine and guggul sterone. The HPLC method was also found to be quite sufficient for the routine quality control of formulations containing piperine and guggul sterone E and Z as ingredients and also for in vitro drug release studies. Copyright © 2011 John Wiley & Sons, Ltd. 相似文献
52.
FtsZ蛋白和细菌的繁殖过程有关,是药物设计理想的靶点。本文采用Sybyl分子模拟软件,利用比较分子场方法(CoMFA)及比较分子相似性指数的方法(CoMSIA)对已报道的33个噁唑-苯甲酰胺类FtsZ受体抑制剂进行了分析,建立了三维定量构效关系(3D-Qsar)模型。CoMFA模型的交互验证系数q2为0.619,线性回归系数r2为0.988;CoMSIA模型的q2为0.633,r2为0.936。模型具有较好的预测能力,为今后噁唑-苯甲酰胺类化合物的设计和改造提供了理论依据。 相似文献
53.
A robust two-stage shape retrieval (TSR) method is proposed to address the 2D shape retrieval problem. Most state-of-the-art shape retrieval methods are based on local features matching and ranking. Their retrieval performance is not robust since they may retrieve globally dissimilar shapes in high ranks. To overcome this challenge, we decompose the decision process into two stages. In the first irrelevant cluster filtering (ICF) stage, we consider both global and local features and use them to predict the relevance of gallery shapes with respect to the query. Irrelevant shapes are removed from the candidate shape set. After that, a local-features-based matching and ranking (LMR) method follows in the second stage. We apply the proposed TSR system to MPEG-7, Kimia99 and Tari1000 three datasets and show that it outperforms all other existing methods. The robust retrieval performance of the TSR system is demonstrated. 相似文献
54.
格非Magi1000自动播出系统主备数据库同步和快速切换 总被引:1,自引:0,他引:1
结合实际使用,简单介绍北京格非Magi1000板卡式硬盘自动播出系统主备数据库同步和切换的方法以及存在的不足,给出了用Delphi7.0编写主备数据库服务器快速切换软件的方法和关键代码,减少了维护工作量,确保播出系统安全不问断运行。 相似文献
55.
Comparative study of spectroscopic properties of Er^3+/Yb^3+-codoped tellurite glass and fibres under 980nm excitation* 下载免费PDF全文
A tellurite fibre of TeO_{2}-ZnO-La_{2}O_{3}-Li_{2}O glass codoped with 20000 ppm ytterbium and 5000 ppm erbium was fabricated by the suction casting and rod-in-tube technologies. The absorption spectrum of Er^{3+}/Yb^{3+} -codoped bulk glass has been measured. From the Judd-Ofelt intensity parameters, the spontaneous emission probability and radiative lifetime τ_{rad} of Er^{3+}:{}^{4}I_{13/2}→{}^{4}I_{15/2} transition for the bulk glass have been calculated. The emission fluorescence spectra and lifetimes around 1.5μm, and subsequent upconversion fluorescence in the range of 500-700nm were measured in fibres and compared with those in bulk glass. The changes in amplified spontaneous emission with fibre length and pumping power was also measured. It was found that the emission spectrum from erbium in fibres is almost twice as broad as the corresponding spectrum in bulk glass when pumped at 980nm. 相似文献
56.
We introduce the notion of strong supercommutativity of self-adjoint operators on a
-graded Hilbert space and give some basic properties. We clarify that strong supercommutativity is a unification of strong commutativity and strong anticommutativity. We also establish the theory of super quantization. Applications to supersymmetric quantum field theory and a fermion-boson interaction system are discussed. 相似文献
57.
High-performance, low-cost joint equalizer and trellis decoder for 1000BASE-T gigabit Ethernet transceiver 总被引:2,自引:0,他引:2
ZHU Yue RONG Meng-tian Department of Electronic Engineering School of Electronic Information Electrical Engineering Shanghai Jiao Tong University Shanghai China 《中国邮电高校学报(英文版)》2007,14(2):106-111
This article presents an M-algorithm (MA) decoder with 4 survival paths (MA4) for Institute of Electrical and Electronics Engineers (IEEE) 802.3ab 1000BASE-T gigabit Ethernet (GbE) transceiver. To fulfill the entire requirements, various methods were introduced to accelerate the MA4 decoder while retaining the desired high performance and low complexity. Optimized look-ahead architecture was employed to solve the critical path problem with minimal gate consumption. Symbol compression methods saved registers during pipeline stages. A sorting network accelerated the kernel sorting operation at low hardware cost by utilizing the special characteristics of MA4. Simulations and synthesis results show that the proposed decoder achieves 125 MHz clock frequency and 1 Gb/s throughput in 1.8 V 0.18 μm standard cell complementary metal-oxide-semiconductor (CMOS) process. It achieves additional 0.4 dB coding gain over 14tap parallel decision feedback decoder (PDFD) with 39% area reduction. 相似文献
58.
DDoS攻击是Internet面临的最大威胁之一。论文综合分析了近年来DDoS防御与反应技术的研究成果,指出了现有方法的不足,并根据IDC业务的实际情况,阐述了IDC中对DDoS攻击的预防与防御对策。 相似文献
59.
60.
Shih‐I Lu 《Journal of computational chemistry》2009,30(14):2176-2180
In this article, we examined the Gibbs energy of activation for the Z/E thermal isomerization reaction of (1Z)‐acetaldehyde hydrazone and (1Z)‐acetaldehyde N,N‐dimethylhydrazone, at 298.15 K in the solvent of cyclohexane. We carried out computations employing both the Gaussian‐4 (G4) theory and the coupled cluster method using both single and double substitutions and triple excitations noniteratively, CCSD(T). The CCSD(T) energy is extrapolated to the complete basis set (CBS). We compared the calculated results to the available experimental observation. It appeared that both G4 and CCSD(T)/CBS computations overestimated the experimental value by as much as about 6 and 12 kcal/mol in the present two cases. We discussed possible sources of error and proposed the experimental kinetic data could be questionable. © 2009 Wiley Periodicals, Inc. J Comput Chem, 2009 相似文献