冷原子吸收光谱法测定磷酸二氢钾中的汞

用冷原子吸收光谱法测定磷酸二氢钾中的汞含量,研究了测定介质及其浓度、重铬酸钾用量、还原剂用量、共存元素干扰等因素对测定的影响,在本试验条件下方法的回收率为97%-104%,相对标准偏差＜10%.     

冷等离子体提纯硅的速率模型分析

应用反应动力学方法建立基元反应速率方程并按工艺条件进行耦合,得出了以宏观工艺参数表达的提纯速率方程,这种方程便于计算,能指导工艺优化并容易为工程师应用,计算结果与实验数据能较好的吻合。     

共价氢化物与汞离子反应的研究：Ⅱ.痕量硒的高灵敏分析新方法

本文详细研究了硒化氢与汞离子反应条件并建立了氢化物发生－冷原子荧光法间接测定痕量硒的新方法。考察了各种实验条件，并将此方法用于合成水样分析，得到一些有意义的结果。     

Measurements of velocity distributions in the deformation zone in cold rolling by a scanning LDV

Experimental determination of the velocity distribution in the deformation zone is of significant importance to investigate the metal flow in both conventional and asymmetrical rolling processes. In this paper, a scanning laser Doppler velocimetry (LDV) system, designed for measuring the velocity distributions in the deformation zone in plate rolling is reported. The LDV used for the rolling process is briefly described and then the scanning mechanism based on beam displacement by a rotating transparent plate is introduced. The relationship among the scanning distance, the beam-cross angle of the LDV system and the rotating angle of the plate is established. The scanning LDV was first tested with a rotating disk and then applied in the rolling process. The test results have demonstrated the feasibility of the scanning LDV.     

Analysis of triglycerides by capillary gas chromatography with programmed-temperature injection

The capillary gas chromatographic analysis of complex naturally occurring and food-product triglyceride mixtures is accomplished qualitatively and quantitatively on columns coated with methyl and methyl-phenyl (65%) silicones using programmed-temperature split/splitless and on-column injection. Faster analysis times are achieved using elevated initial column oven temperatures with cold initial injector temperatures.     

An MSFIA system for mercury speciation based on an anion-exchange membrane

A new methodology for the in-line preconcentration, clean-up and speciation of mercury by use of an anion-exchange membrane is proposed. The speciation of mercury is based on retention of its tetrachloro complex onto the membrane while organic mercury flows freely through it. A multisyringe is used as a liquid driver and a cold vapour atomic fluorescence detector is employed to ensure a high sensitivity. Organic mercury is decomposed into to inorganic mercury by using a UV lamp. The carrier and reductant streams consist of 1.5% (m/v) hydrochloric acid and 2% (m/v) tin chloride, respectively. Certified reference material DORM-2 was digested with 37% hydrochloric acid and analysed directly without the need for extraction. The proposed system is more environmental friendly than the classical liquid-liquid extraction procedure. Mercury recoveries from spiked samples and the reference material were all close to 100%. An LOD of 14 and 16 ng/L was obtained for total and organic mercury, respectively, both with an RSD less than 1.3%.     

低频Alfvén波谱与冷等离子体的非共振作用研究

本文讨论了低频率Alfvén波谱与冷等离子体的非线性相互作用。研究表明,对于多个低频Alfvén波,在波的振幅相对于背景磁场较小时,随着时间的增加,粒子动理学温度的各向异性会降低;随着振幅的增加,平行方向的动理学温度不断升高,且在A2=0.1处,平行方向的动理学温度将超过垂直方向的动理学温度。     

越南火龙果冷藏现状分析

随着全球化经济的快速发展,食品冷藏技术日益重要.文中综述了越南火龙果的现有冷藏技术及其存在的问题,并提出解决方案.     

冷绝缘高温超导电缆绝缘设计的研究

目前随着国内外高压输电系统的不断发展,许多研究机构一直试图开发高电压等级的高温超导电缆系统,这就要求设计的HTS电缆要有可靠的绝缘性能和优化的绝缘设计技术.根据超导电缆的结构特点和高温超导电缆系统的运行特点,对Nomex和PPLP进行了交流耐压、雷电冲击、局部放电(PD)起始电压和热循环等高压绝缘特性试验.根据不同厚度...