毛头鬼伞的红外光谱研究

利用傅里叶变换红外光谱法(FTIR)研究了人工栽培与野生的毛头鬼伞,及其液化前后的菌盖样品。毛头鬼伞的红外光谱主要由蛋白质、多糖的特征吸收峰组成。人工菌与野生菌的光谱差异表现为蛋白质和多糖的特征峰强度比,野生菌的多糖特征吸收峰要比人工菌的吸收峰明显。菌盖液化黑色物与液化前的菌盖光谱相比,多糖特征峰明显减弱,表明菌褶液化现象主要是多糖的变化。红外光谱结果为毛头鬼伞的进一步的开发研究提供了参考信息。     

Quantum codes from caps

Caps in a finite projective geometry over GF(4) are used for the construction of some quantum error-correcting codes, including an optimal ?27,13,5? code.     

流化床风帽故障的声发射检测

针对气固流化床中风帽故障影响流化质量问题,本文提出一种能够快速精确地检测出风帽故障位置和类型的声发射检测方法;声发射技术是一种实时、在线、非侵入流场的声波检测方法,利用均匀安装在流化床分布板下方的声发射传感器进行定位测量;采集气固流化床内颗粒撞击分布板产生的声信号,对该信号进行多尺度小波包分解,找出特征频段,由各个测点声发射信号总能量对比可以直观反应风帽故障存在位置,而各尺度能量分率的变化能进行故障类型判断;这种实时测量方法能更早,更精确的对风帽破损情况进行准确的判断。     

Chemical conjugation of an mRNA cap analogue with a cell-penetrating peptide as a potential membrane permeable translation inhibitor

We present a versatile method for chemical conjugation of a dinucleotide cap analogue with a cell-penetrating peptide. The final coupling reaction is between an azide-modified peptide (MPS-N₃)—a fragment that is responsible for transport of the conjugate through the cell membrane, with a biologically active compound—and an alkynylated cap structure, using the Cu(I)-catalyzed click reaction.     

On Kestenband–Ebert partitions

We study Kestenband–Ebert partitions from a group-theoretic point of view. © 1997 John Wiley & Sons, Inc. J Combin Designs 5: 367–375, 1997     

铜互连可靠性分析

在简要的对铜互连和铝互连进行了比较后,本文从材料特性和集成工艺两方面讨论了铜互连和铝互连对可靠性的不同影响,并详细的分析了一个关键的可靠性失效机理:电迁移(包括通孔损耗和连线损耗).最后讨论了影响铜电迁移的一些工艺要素,如通孔、阻挡层和覆盖层.     

Trace analysis of glyclazide in human plasma at microscale level by mass spectrometry

Green (reagents and organic solvents saving) analytical chemistry is a new strategy for pharmaceutical analysis. The principles of this idea include primary elimination or at least reduction of the amounts of organic reagents and solvents. In this study, we have provided two simple methods for the analysis of clinical drugs in human plasma. One is the capillary LC (Cap LC) connected to MS–MS, the other is the matrix‐assisted laser desorption ionization (MALDI) connected to TOF MS. Sulfonylurea drugs are usually used in diabetes mellitus patients. Diabetes is a syndrome of disordered metabolism resulting in abnormally high blood sugar levels (hyperglycemia). These microscale methods were successfully applied for the monitoring of drug levels in human plasma using gliclazide (a second‐generation sulfonylurea) as the test platform. The sensitivity of these methods is sufficient for detecting the gliclazide within a therapeutic range. All the analytical procedures (including human plasma, sample preparation, and flow rate of the analytical system) were at microscale level. These two methods would lower the consumption of organic solvents further safeguarding our environment.     

量子阱材料盖层对结构稳定性和能带隙的影响

介绍了应变量阱材料单结点失配位错能量平衡模型,计算了一些典型量子阱 阱层临界应变和应变体材料的最大允许应变。报告了Ｎｏ．５５８压应变量子阱材料的实际阱层应变和Ｎｏ．９１８２材料非应变盖层对有源层泊影响。