新工科视阈下石油化工类高校应用化学专业课程体系重构

Taking a typical local and industry-orientated applied chemistry major as an example with focusing on the major changes in the form and content of the petrochemical industry, the way to reform the core curriculum system and teaching contents is presented. Based on the changing tendency of refinement of the petrochemical industry, a complete curriculum system with distinctive industry characteristics is set up according to the principles of the emerging engineering education (3E) with several reasonable suggestions. A new model for the construction of a 3E major in chemistry-related majors is suggested. It is a good reference for the construction of curriculum systems for other local and industry-orientated colleges who want to make 3E reform.     

基于创新能力培养的化学专业本科实验教学新体系的构建与实践

课程体系是人才培养的载体。为了更好地培养拔尖创新人才,南京大学化学国家级实验教学示范中心依据化学学科的特点和发展趋势,以科学内容的内在联系和研究规律为主线构建了“化学实验基础?化学合成与表征+化学原理与测量?化学功能分子实验+化学生物学综合实验+基于项目的研究实验”实验课程新体系,按照一流课程建设要求(高阶性、创新性和挑战度)对实验教学内容进行了优化,并建立起与之相适应的实验教学平台。新课程体系综合考虑了化学一级学科的整体性和关联学科的交叉性,在南京大学化学化工学院“拔尖计划”和“强基计划”学生中实施,教学效果显著。     

Tutorial review on validation of liquid chromatography–mass spectrometry methods: Part II

This is the part II of a tutorial review intending to give an overview of the state of the art of method validation in liquid chromatography mass spectrometry (LC–MS) and discuss specific issues that arise with MS (and MS–MS) detection in LC (as opposed to the “conventional” detectors). The Part II starts with briefly introducing the main quantitation methods and then addresses the performance related to quantification: linearity of signal, sensitivity, precision, trueness, accuracy, stability and measurement uncertainty. The last section is devoted to practical considerations in validation. With every performance characteristic its essence and terminology are addressed, the current status of treating it is reviewed and recommendations are given, how to handle it, specifically in the case of LC–MS methods.     

多曲面反射体的计算机辅助设计及优化

研究了自由曲面反射式照明系统的设计理论和方法.根据反射器的尺寸、位置以及配光要求按点光源设计得到曲面型值点初始坐标后,将双三次B样条曲面引入照明系统的设计,反算出控制顶点.给出了空间任意一条入射光线与反射器区块的交点及其曲面法线向量的求法,为了提高光路追迹的效率,针对多曲面反射体给出了一种快速判断相交区块的算法.探讨了用阻尼最小二乘法对B样条曲面反射器进行优化设计的方法,通过优化运算修正控制顶点Z轴坐标,使得曲面在使用扩展光源时光形分布尽可能满足设计要求.     

面向化妆品产业升级的江南大学应用化学专业建设思考与实践

Based on the development prospect of cosmetics industry, the advantage of light industry characteristic and the foundation of applied chemistry in Jiangnan University, a systematic upgrading of applied chemistry was carried out through \"emerging engineering education (3E)\" project \"upgrade and practice of chemistry-related majors of local and/or trade university responding to the social developments\" supported by the Ministry of Education. On the basis of investigation and analysis, the orientation and training goal of applied chemistry were updated first, and then the curriculum system was determined and the curriculum construction is strengthened, so as to achieve more distinctive characteristics, more solid foundation and more comprehensive quality. In view of the new requirements of the 3E for talent training, some practices have been formed in the aspects of multi-disciplinary integration, multi-angle coordination and close integration to industry. Contributing the development of cosmetics industry and seizing the commanding point of science and technology from the perspective of talent training, will play a unique role in human social progress.     

Thermal effect on vibration of non-homogenous visco-elastic rectangular plate of linearly varying thickness

An analysis for vibration of non-homogenous visco-elastic rectangular plate of linearly varying thickness subjected to thermal gradient has been discussed in the present investigation. For visco-elastic, the basic elastic and viscous elements are combined. We have taken Kelvin model for visco-elasticity that is the combination of the elastic and viscous elements in parallel. Here the elastic element means the spring and the viscous element means the dashpot. The governing differential equation of motion has been solved by Galerkin’s technique. Deflection, time period and logarithmic decrement at different points for the first two modes of vibration are calculated for various values of thermal gradients, non homogeneity constant, taper constant and aspect ratio for non-homogenous visco-elastic rectangular plate which is clamped on two parallel edges and simply supported on remaining two edges. Comparison studies have been carried out with homogeneous visco-elastic rectangular plate to establish the accuracy and versatility.     

简易多路气体分流装置在有机实验教学中的应用

介绍了一种简易多路气体分流装置,可以简单方便地将惰性气体分流供应多个学生同时使用,并确保每条支路气流量充足。该套装置可以提高操作的安全性同时减少资源的浪费,它拆装方便,可以在不使用时进行存放储藏,有效地减小占有空间。     

高分子玻璃化转变过程的分子动力学模拟本科教学实验

玻璃化转变是高分子专业教学中的重要内容,转变过程中自由体积的变化和分子链段的运动是理解玻璃化转变的难点。在计算机上使用分子模拟的方法得到三维的可视化图形,可以更直观地观察到自由体积和分子链的变化。提炼近年分子模拟技术在玻璃化转变研究中的最新科研成果,得到既有理论基础又适合本科教学的课程素材。分子模拟可以实现了仪器测试无法达到的超快速升降温,并与仪器测试得到的实验结果相对照,验证了普通实验很难验证的理论观点,从而拓展了本科实验的范围,达到了很好的教学效果。     

以应用型人才培养为导向的材料科学基础课程教学改革

为响应国家加强应用型人才培养的号召,应用型本科院校培养材料类专业人才应侧重材料的开发应用、材料改性和材料加工等方面。针对应用型本科院校的特点和唐山师范学院材料化学专业的具体情况,提出了适宜应用型本科材料科学基础课程的教学改革方法。从教学内容、教学手段及方法、实践教学环节和考核方式等方面探讨了材料科学基础课程教学改革的主要思路并进行了实践。实践证明,教学内容上选取贴近实际的例子和教学方法上多采用引导式教学,能够提高学生的学习兴趣, 增强学生分析问题和解决问题的能力。