TheQ EC dependence of evidence for a 17-keV neutrino from the55Fe radiative decay

The internal bremsstrahlung spectrum of⁵⁵Fe was studied using HPGe detector in low background and reduced pileup conditions. The data show that the conclusion on the presence of a heavy mass neutrino strongly depends from the experimental decay energy value taken in the analysis. The decay energy was found to beQ _EC =231.37 ± 0.10 keV. The obtained results also show the need for the higher accuracyQ _EC used in the analysis of the existence of a 17-keV neutrino in the⁵⁵Fe decay.The authors would like to thank A. Plochocki and J. ylicz for helpful discussion and assistance.     

Alkylation of cyclododecanone with α,ω-dibromoalkanes under conditions of phase-transfer catalysis

Alkylation of cyclododecanone with ,-dibromoalkanes Br(CH) _n Br (n=3, 4, 5) under conditions of phase-transfer catalysis in the presence of KOH results in the formation of either bicyclic ketones forn=3 and 5 or a mixture of bicyclic and spirocyclic ketones forn=4.Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 8, pp. 1436–1438, August, 1994.     

Modulated potential electrogenerated chemiluminescence of luminol and Ru(bpy) 3 2+

Chemiluminescence emission intensity is modulated by modulating the potential of a working electrode which is used to generate a key species in the electrogenerated Chemiluminescence (ECL) reaction. The emission is monitored synchronously using a lock-in amplifier. The reactions used in the characterization are luminol with hydrogen peroxide and tris(2,2-bipyridyl)ruthenium (II) (or Ru(bpy) ₃ ²⁺ ) with oxalate. Modulation widths of ± 50 mV yield maximum signals for luminol when centered at 0.45 V (vs Ag/AgCl) and for Ru(bpy) ₃ ²⁺ when centered at 1.05 V. The resulting signal decreases with increasing modulation frequency and shows that luminol/H₂O₂ is a faster ECL system than Ru(bpy) ₃ ²⁺ /oxalate. Working curves for luminol and for oxalate have essentially the same linear range and slope with the modulated potential approach as with a DC electrode potential. This approach provides capability for differentiating the analytical signal from constant background emission or stray light.     

Preparation and characterization of a viscosity index improver for naphthenic and paraffinic base oils

Copolymers of -methyl styrene and 2-ethylhexyl acrylate were prepared in a benzene solution. The presence of the copolymers were confirmed by solubility, IR and NMR tests. The molecular weight and the polydispersity of the polymers were estimated by GPC. The copolymers obtained were blended with paraffinic and naphthenic base oils. The viscosity, the viscosity index (VI) the Q value as well as the stability to shear and oxidation were obtained for these blends. The results are compared with the results obtained with an oil blend containing a commonly used high temperature additive. Two of the copolymers obtained have shown to be good alternatives for specific applications.Presented at the Symposium, 76^th CSC Congress, Sherbrooke, Quebec, May 30–June 3, 1993, honoring Professor Donald Patterson on the occasion of his 65^th birthday.     

具有界面依赖光致发光的双层WS2/Ga2O3异质结的能带工程(英文)

利用垂直WS₂/Ga₂O₃异质结构中异质界面诱导了反常的光致发光(PL)发射。垂直堆栈的WS₂/Ga₂O₃异质界面使其形成了II型能带结构,导致与Ga₂O₃层接触的底层WS₂的PL强度下降。而异质界面的强耦合作用也影响了双层WS₂中的同质层间相互作用,使得上层WS₂出现反常的PL增强。这种堆栈新型二维异质结构为定制目标能带结构并控制其光子和电子行为提供一种新的手段。     

一种基于电荷泵锁相环的快速啁啾发生器

调频连续波(FMCW)雷达常用于测量多个目标的距离和速度,被广泛用于自动驾驶场景中。FMCW雷达产生的线性调频波称为啁啾(Chirp),通常由锁相环(PLL)电路产生。由于带宽有限,传统锯齿啁啾下降时间过长,降低了雷达性能。文章提出了一种基于分段电流电荷泵的快速啁啾发生器设计方案。调频阶段采用最佳电荷泵电流,即最优环路带宽,可保证啁啾的线性度。啁啾下降阶段使用更大的电流,可缩短下降时间。仿真结果表明,啁啾发生器频率输出范围为19.25～20.25 GHz, 1.2 V电压下整体功耗为31.8 mW。PLL带宽为1.5 MHz时,锯齿形啁啾下降的最大调制速率为454 MHz/μs。与恒定电荷泵电流方式相比,下降时间缩短了80%。     

一种43 GHz超高带宽线性驱动电路设计

基于0.13μm SiGe BiCMOS工艺,设计了一种线性驱动电路。该电路具有高速和大摆幅的优势,能线性驱动行波马赫-曾德尔调制器(TW-MZM),可满足光通信系统100 Gbit/s单通道的应用需求。驱动电路包括连续时间线性均衡(CTLE)电路、可变增益放大(VGA)电路和基于Cascode结构改进优化的输出级电路,实现了增益可调,且避免发生由较大输出摆幅导致的晶体管击穿。仿真结果表明,电路的-3 dB带宽为43 GHz,其增益在15～25 dB内可调。在56 Gbaud NRZ/PAM4的输入信号下,测得的眼图形状良好,差分输出摆幅峰-峰值达4 V,电路整体功耗为1.02 W,面积为0.33 mm²。     

一种L~E波段的A型上电极MEMS单刀三掷开关设计

针对单刀多掷开关(SPMT)在相控阵雷达、宽带收发器中用于切换滤波器和传输线时需要满足宽频带、高隔离度的性能需求,设计了一种宽频带、高隔离度的MEMS单刀三掷开关(SP3T)。通过ANSYS电磁仿真软件中的HFSS模块对MEMS SP3T开关进行优化,利用COMSOL软件对上电极的机械性能进行仿真。仿真结果表明,所设计的MEMS SP3T开关可工作在1~90 GHz的频带内,且插入损耗小于1 dB@90 GHz,隔离度大于35 dB@90 GHz,其整体体积约为0.75 mm³。     

基于TW3-C RUS法的骨龄评估方法研究

经典TW3-C RUS (Tanner and Whitehouse 3-Chinese RUS)法将手骨的关键骨骺区域严格划分为9个等级,未充分考虑骨骺发育的连续性,导致骨龄评估存在一定误差。针对该问题,本文提出一种基于TW3-C RUS法的改进骨龄评估方法。采用阈值法的思想,动态选择网络模型输出的前N个等级概率值,并将前N个概率值作为权值计算手骨的加权得分,降低由于手骨单一等级判定引起的误差。针对网络模型冗余问题,采用跨阶段局部网络(cross stage partial network, CSP-Net)轻量化深度残差网络(residual network 50,Resnext50)。实验表明,改进后的方法对男性骨龄评估的平均绝对误差(mean absolute error,MAE)为0.421 4岁,女性MAE为0.412 8岁,相比于经典TW3-C RUS法,骨龄评估准确率有明显提升。轻量化后的网络模型参数量为46.28 MB,相比Resnext50网络模型有明显降低。     

基于改进ICP的复杂机械零件测量点云配准方法

点云配准是基于机器视觉进行复杂机械零件三维非接触精密测量的关键环节。针对传统迭代最近点(iterative closest point, ICP)算法对初始位置依赖性强,迭代收敛速度慢,错误对应点对多,难以满足大批量复杂机械零件测量点云配准效率和精度要求的问题,提出了一种基于ISS-FPFH(intrinsic shape signature-fast point feature histogram)特征结合改进ICP的复杂机械零件测量点云配准方法。为了减少点云配准数量,并保留点云表面原来的细微特征,提出了基于重心邻近点的体素滤波器对点云进行下采样预处理。为解决传统ICP算法因合适初始位置难以确定而导致多视角测量点云配准失败的问题,采用了基于ISS-FPFH特征的采样一致性初始配准(sample consensus intial alignment, SAC-IA)算法进行粗配准。为解决传统ICP算法迭代收敛速度慢、错误对应点对多的问题,提出结合法向量夹角约束的点到平面ICP算法进行精配准。以斯坦福大学的bunny点云模型为对象,验证了本文提出方法对噪声点云的鲁棒性。以常见的复杂机械零...