5G时代,有线接入网基础资源布局思路探讨

双千兆时代,网络规模空前巨大,有线接入网更是因覆盖范围广,建设规模大,投入人力多,投资占比高等因素,成为研究重点。文章根据有线接入网架构演进,从“点(各类业务及分纤点)、线(各级管线)、面(业务汇聚区)”三个层面对基站、家客、集客等业务接入、分纤点规划及业务汇聚机房等基础资源规划进行研究。     

粗DEM辅助的广域PS-InSAR数据预处理方法及应用

PS-InSAR技术是一种高精度的地表形变探测方法,小区域PS-InSAR处理的研究较为深入,但处理方法并不适用广域的形变探测和数据处理方法。本文针对卫星实时轨道精度差的问题,首先提出利用辅助DEM进行斜距误差和轨道系统误差校正提升差分干涉相位反演精度的方法;其次,针对广域图像配准误差的空变性,提出了一种由粗到精的层级配准方法,解决了配准误差空变对PS-InSAR永久散射体选取和图像相干性的影响;最后,通过对形变观测结果的地理编码结合加权处理,实现对超广域观测图像的拼接。利用仿真数据验证了粗DEM对系统误差校正的有效性,并进一步通过Sentinel-1A的2000多景雷达影像对云南省全境39.4万平方千米的覆盖区域进行了处理,结果表明了本文方法对系统误差校正和对广域形变探测处理的有效性。     

不对称合成中手性磷配体催化剂的研究进展（I）（待续）

评述了作为配体催化剂的手性三配位及四配位磷化合物的合成及其在某些不对称的合反应中的应用。     

基于杂环有机锡化合物的水杨酸根离子选择电极研究

A novel heterocyclic haxacoordinated organotin(Ⅳ) complex, bis (o-vanillin)-semi-ethylenediamine dibenzyltin (VEDBT) was synthesized and used as anion ionophore for PVC membrane electrode; the novel electrode exhibits a linear response towards salicylate and an anti-Hofmeister selectivity pattern with high specificity for salicylate over many common anions, the selective pattern is: Sal^- > SCN^- > ClO₄^- > I^- > NO₂^- > NO₃^- > Cl^- ≈ Br^- > SO₄^2-. The behaviour of the electrode is influenced by the experimental conditions. The response mechanism was also investigated by UV spectroscopy. The electrode was applied to the determination of salicylate in pharmaceutical samples with satisfactory results.     

Three New Anthraquinones from Polygonum cillinerve

Three new anthraquinones, emodin-8-β-D-（2＂-O-coumarate）glucoside 1, emodin-8-β-D-（6＇-O-acetyl）glucoside 2 and physicon-8-β-D-（6＇-O-acetyl）glucoside 3, were isolated from the roots of Polygonum cillinerve and their structures were established by spectroscopic methods. The biological activity indicated that compound 1 had the scavenging activity on 1,1-diphenyl-2-picrylhydrazyl （DPPH） radicals （the IC50 = 8.5 μmol/L）, and compound 1-3 showed no activities against HL-60 and BCJC-823 cells by MTT method in vitro.     

Two New Isobutyltartrate Monoester from Coeloglossum viride （L.） Hartm.var.bracteatum（Willd.） Richter

Two new isobutyltartrate monoesters,coelovirin A (1) and B(2),were isolated from the rhizomes of Coeloglossum viride (L.) Hartm. var. bracteatum (Willd.) Richter (Orchidaceae). Their structures were elucidated as (2R,3S)-2-isobutyltartrate-1-(4-β-D-glucopyranosyloxybenzyl) ester 1 and (2R,3S)-2-isobutyltartrate-4-(4-β-D-glucopranosyloxybenzyl) ester 2 on the basis of physical constants and spectroscopic methods including 2D NMR techniques.     

配糖蛋白B—阳离子丙烯酸树脂微胶囊的性能研究

本文研究了配糖蛋白B-阳离子丙烯酸树脂微胶囊的形态、粒径及粒径分布,并在模拟胃液的酸性缓冲液中进行了微胶囊的溶解释放试验。结果表明该微胶囊能溶于人体的胃液中,可配制适合儿童口服的混悬剂。     

配糖蛋白B肠溶微胶囊的研究

采用双乳液法研制配糖蛋白Ｂ的肠溶微胶囊，考察了微胶囊的形态、粒径及其分布，在摸拟肠液的缓冲液中进行溶解释放试验。配制了两种口服微胶囊混悬制剂，并考察了它的稳定性。     

Two New Xanthone Glycosides from Securidaca inappendiculate

Two new xanthone glycosides, securixanside B and C, were isolated fron the stems of Securidaca inappendiculate. Their structures were determined as 3-O-β-D-glucopyranosyl-1,7-dihydroxyl-2-methoxyxanthone and 6-O-β-D-glucopyranosyl-1-hydroxy-4,7-dimethoxyxanthone by spectroscopic methods.