Crystallization of Poly(ethylene adipate) within γ-Phase Poly(vinylidene fluoride) Matrix

The effects of PEA on the γ-phase PVDF crystal structure and the crystallization of PEA within the pre-existing γ-phase PVDF spherulites have been investigated by optical microscopy(OM), infrared spectroscopy(IR) and scanning electron microscopy(SEM). The results demonstrate that the γ-phase PVDF spherulites consist of the lamellae exhibiting a highly curved scroll-like morphology and develop preferentially in PEA-rich blend. With increasing PEA concentration, the scroll diameter increases and the scrolls are better separated from each other. PEA crystallizes first in the interspherulitic region and transcrystalline layer develops. Subsequently, the transcrystalline layer of PEA continues to grow within the γ-phase PVDF spherulites, e.g., in the region between the scrolls, until impinging on other PEA transcrystalline layers or spherulites. The crystallization kinetics results indicate that the growth rate of PEA crystals in the intraspherulitic region of γ-phase PVDF shows a positive correlation with content of PEA, but a negative one with the crystallization temperature of γ-phase PVDF.     

Mass and isotopic concentrations of water-insoluble refractory carbon in total suspended particulates at Mt.Waliguan Observatory(China)

Mass concentration and isotopic values δ¹³C and ¹⁴C are presented for the water-insoluble refractory carbon（WIRC） component of total suspended particulates（TSP）,collected weekly during 2003,as well as from October 2005 to May 2006 at the WMO-GAW Mt.Waliguan（WLG） site.The overall average WIRC mass concentration was（1183±120）ng/m³（n = 79）,while seasonal averages were 2081 ±1707（spring）,454±205（summer）,650±411（autumn）,and 1019±703（winter） ng/m3.Seasonal variations in WIRC mass concentrations were consistent with black carbon measurements from an aethalometer,although WIRC concentrations were typically higher,especially in winter and spring.The δ¹³C PDB value（-25.3 ± 0.8）%.determined for WIRC suggests that its sources are C₃ biomass or fossil fuel combustion.No seasonal change in δ¹³C PDB was evident.The average percent Modern Carbon（pMC） for ¹⁴C in WIRC for winter and spring was（67.2 ± 7.7）%（n = 29）.Lower pMC values were associated with air masses transported from the area east of WLG,while higher pMC values were associated with air masses from the Tibetan Plateau,southwest of WLG.Elevated pMC values with abnormally high mass concentrations of TSP and WIRC were measured during a dust storm event.     

一个p(x)-Laplace方程组非平凡解的存在性

在广义Lebesgue空间L~(p(x))(Ω)和广义Sobolev空间W~(1,p(x))(Ω)基本理论体系的基础上,利用山路引理,Young不等式,H(o|¨)lder不等式和嵌入定理,获得了一p(x)-Laplace方程组非平凡解的存在性.     

一类具非光滑位势p(x)-Laplace方程解的存在性

在非光滑临界点理论的基础上,利用带非光滑(PS)条件的山路引理,结合嵌入定理和Lebourg中值定理,获得了一类具非光滑位势p(x)-Laplace方程解的存在性.     

以MnO2纳米棒为自反应模板通过一锅法制备PPy/Fe3O4复合材料及其吸波性能研究

以MnO_2为自反应模板,采用一锅法制备了PPy/Fe_3O_4复合材料,对比研究了MnO_2及PPy/Fe_3O_4复合材料的吸波性能。用透射电镜(TEM)、扫描电镜(SEM)、X射线衍射仪(XRD)、傅立叶-红外光谱仪(FT-IR)和矢量网络分析仪(VNA)等分析测试手段对材料进行了微观形貌观测、结构表征、电磁参数测试以及吸波性能评估。结果表明:PPy/Fe_3O_4复合材料在厚度为5.0 mm、频率为6.9 GHz处反射损耗(RL)达到最佳反射损耗-39.5 dB,有效频宽为3.0 GHz。     

基于TDOA和PTP的高精度WLAN定位系统的设计和实现

针对室内WLAN定位目前难以达到分米甚至厘米级的高精度问题,以IEEE1588v2(PTP)精确网络时钟同步技术和到达时差原理(TDOA)为基础,结合非视距(NLOS)测距误差消除等技术,研究和设计出一套基于现有WLAN(IEEE802. 11x系列标准)设备的高精度实时定位解决方案。实验表明,该系统实现的到达时间测量和定位精度等参数优于UWB、CSS无线定位方案。本案可广泛应用于移动互联网、物流管理、矿业勘探、医疗健康等需要精准位置服务(LBS)的行业领域。     

激光辅助电化学放电加工微通道的特性

玻璃材料近年来被广泛应用于微电子机械系统(MEMS),对于玻璃材料的加工,电化学放电加工(ECDM)是一种被广泛运用的手段。针对目前的电化学放电加工存在热影响区和过切现象的问题,提出了一种激光辅助电化学放电加工玻璃的加工方法,阐述了其作用机理,设计了实验装置,并与传统电化学放电加工进行了微通道加工的对比实验。通过与传统电化学放电加工对比,发现激光辅助电化学放电的加工方式能明显减少放电加工过程中的热影响区和过切现象,故激光辅助有效改善了电化学放电在玻璃材料上加工微通道的质量和精度,在MEMS领域具有良好的应用前景。     

基于关键路径延时检测的自适应电压缩减技术

为了减小传统的最差情况设计方法引入的电压裕量,提出了一种变化可知的自适应电压缩减(AVS)技术,通过调整电源电压来降低电路功耗.自适应电压缩减技术基于检测关键路径的延时变化,基于此设计了一款预错误原位延时检测电路,可以检测关键路径延时并输出预错误信号,进而控制单元可根据反馈回的预错误信号的个数调整系统电压.本芯片采用SMIC180 nm工艺设计验证,仿真分析表明,采用自适应电压缩减技术后,4个目标验证电路分别节省功耗12.4％,11.3％,10.4％和11.6％.     

基于RRPP技术的以太网组网应用

本文阐述了一种基于RRPP技术的环网拓扑传输系统及传输方法,主要适用于以太网的环网保护应用。该传输方法为:所述环网拓扑的结构包括一个汇聚节点和所述汇聚节点下带的多个环网,所述汇聚节点由若干台汇聚设备构成,所述传输方法通过IFR2(第二代智能弹性架构技术)将所述若干台汇聚设备虚拟化为一个设备,即虚拟化设备。在不降低双汇聚设备可靠性的前提下,简化了网络架构,确保了业务的快速倒换,提高了网络的可靠性。