基于宽带吸波体的微带天线雷达散射截面缩减设计

利用加载集总电阻的方式设计出一种极化稳定且宽入射角的宽带超材料吸波体(wide-band metamaterial absorber, WBMA), 在平面波垂直入射时, 其吸波半波功率带宽达12.7 GHz, 吸波率大于90%的带宽达10.42 GHz, 峰值吸波率达99.9%. 将其与微带天线共基板共接地板的方式加载, 制备出WBMA微带天线, 实现了天线宽频域内雷达散射截面(radar cross section, RCS)大幅缩减. 仿真与实测结果表明: 将WBMA加载于微带天线后, 天线的前向增益提高了0.53 dB, 整体辐射特性基本保持不变; 在不同极化波下, 天线的工作频带带内和带外等宽频域(6.95-17.91 GHz)内的单站RCS缩减大于3 dB以上, 最大缩减值达21.2 dB; 在天线的中心频点8 GHz处± 48°的宽角域内, 双站RCS缩减效果明显, 很好地实现了天线的宽频域大角度的隐身设计.     

雷达天线控制系统频域辨识与仿真方法研究

雷达天线控制系统仿真是雷达系统目标跟踪动态仿真中一个重要环节。为解决雷达天线控制系统仿真中滞后误差大、动态效果差等问题,依据某雷达天线控制系统性能实际测试结果,以典型系统模型作为研究对象,利用频域最小二乘法完成模型参数辨识,建立系统模型,并对辨识模型进行验证。在此基础上,采用基于时域的增广矩阵法对系统进行了数字快速仿真分析。结果表明,辨识模型满足精度,且增广矩阵法能够有效快速地完成系统数字仿真,对天线控制系统建模以及快速动态仿真研究具有一定的参考价值。     

Determination of teniposide in rat plasma by ultra performance liquid chromatography electrospray ionization tandem mass spectrometry after intravenous administration

A novel, specific and rapid ultra performance liquid chromatography electrospray ionization tandem mass spectrometry method has been developed and validated for determination of teniposide in rat plasma. A one‐step liquid–liquid extraction method was used and the separation was carried out on an Acquity UPLC^TM BEH C₁₈ column with gradient elution using a mobile phase composed of acetonitrile and water (containing 0.1% formic acid) at a flow rate of 0.20 mL/min. A triple quadrupole tandem mass spectrometer in multiple‐reaction monitoring mode via an electrospray ionization interface was used for the detection of teniposide. The detection was complete within 3.0 min. A linear calibration curve was obtained over the concentration range 10–10,000 ng/mL for teniposide, with a lower limit of quantification of 10 ng/mL. The intra‐day precision and inter‐day precision (relative standard deviation) were less than 10.23 and 13.09%, respectively. The developed method was applied for the first time to the pharmacokinetic study of teniposide in rats following a single intravenous administration of 4.5 mg/kg teniposide. Copyright © 2009 John Wiley & Sons, Ltd.     

ADAPTIVE NEURO-FUZZY INFERENCE SYSTEM FOR COMPUTING THE PHYSICAL DIMENSIONS OF ELECTRICALLY THIN AND THICK RECTANGULAR MICROSTRIP ANTENNAS

A new method for calculating the patch length and width of rectangular microstrip antennas (MSAs) with thin and thick substrates, based on adaptive neuro-fuzzy inference system (ANFIS), is presented. The ANFIS is a class of adaptive networks which are functionally equivalent to fuzzy inference systems (FISs). It combines the powerful features of FISs with those of artificial neural networks (ANNs) to achieve a desired performance. The results of ANFIS are in excellent agreement with the experimental results available in the literature.     

A New Associated Pumping Mechanism for Interstellar H2O and OH Masers

A new associated pumping mechanism for masers in regions of star formation is presented, giving a unified interpretation for both H₂O and OH interstellar masers. A very wide range of photons contributes to this mechanism, thus sufficient numbers of photons are available. A reasonable mechanism for the regeneration of interstellar H₂O and OH molecules is presented. Therefore this model overcomes several drawbacks of former radiative mechanisms. It is both simple and compatible with astronomical conditions.     

角量控制的激光天线设计

在多环检测系统理论的基础[4,5]上,通过对激光天线单镜和双反射镜的高斯光束的传播规律和双镜距控制光斑稳定不变的实验数据[1,2],来进行激光天线的设计。设计采用了高斯光束控制入射光束的光腰位置,对天线副镜和主镜的入射角、反射角和天线发散角的控制方法,设计了天线的副镜和主镜的曲率半径、焦距和直径,达到了光斑保持的目的。计算公式简单,使用方便,计算公式和实验测定的数据误差在工程设计要求的范围以内,适合工程设计的需要。     

Speciation and detection of arsenic in aqueous samples: A review of recent progress in non-atomic spectrometric methods

Inorganic arsenic (As) displays extreme toxicity and is a class A human carcinogen. It is of interest to both analytical chemists and environmental scientists. Facile and sensitive determination of As and knowledge of the speciation of forms of As in aqueous samples are vitally important. Nearly every nation has relevant official regulations on permissible limits of drinking water As content. The size of the literature on As is therefore formidable. The heart of this review consists of two tables: one is a compilation of principal official documents and major review articles, including the toxicology and chemistry of As. This includes comprehensive official compendia on As speciation, sample treatment, recommended procedures for the determination of As in specific sample matrices with specific analytical instrument(s), procedures for multi-element (including As) speciation and analysis, and prior comprehensive reviews on arsenic analysis. The second table focuses on the recent literature (2005–2013, the coverage for 2013 is incomplete) on As measurement in aqueous matrices. Recent As speciation and analysis methods based on spectrometric and electrochemical methods, inductively coupled plasma-mass spectrometry, neutron activation analysis and biosensors are summarized. We have deliberately excluded atomic optical spectrometric techniques (atomic absorption, atomic fluorescence, inductively coupled plasma-optical emission spectrometry) not because they are not important (in fact the majority of arsenic determinations are possibly carried out by one of these techniques) but because these methods are sufficiently mature and little meaningful innovation has been made beyond what is in the officially prescribed compendia (which are included) and recent reviews are available.     

Ultra‐high‐performance liquid chromatography–tandem mass spectrometry for pharmacokinetics of bakuchiol in rats

Psoralea Corylifolia L. is a traditional Chinese medicine with many beneficial effects in medical therapies. Bakuchiol was the main active ingredient of Psoralea Corylifolia L., used for the treatment of various diseases and also as a natural food additive. A specific and reliable ultra‐high performance liquid chromatography–tandem mass spectrometry has been developed and fully validated for the quantification of bakuchiol in rat plasma. Chromatographic separation of bakuchiol and an internal standard, daidzein, was achieved on a Hypersil Gold C₁₈ column with gradient elution that consisted of methanol and water at a flow rate of 0.2 mL/min. The compounds were detected at negative ionization mode using mass transition m/z 255.2 → 172.0 and 252.9 → 132.0 for bakuchiol and daidzein, respectively. Good linearity was obtained over the range of 2–1000 ng/mL and the lower limit of quantification was 2 ng/mL. The intra‐ and inter‐day accuracies ranged from 91.1 to 105.7% and precisions (relative standard deviations) were within 9.3%. Bakuchiol was found to be stable under three freeze–thaw cycles, short‐term temperature, post‐preparative and long‐term temperature conditions. The method was applied to a pharmacokinetic study of bakuchiol intravenously administered to rats at a dose of 5 mg/kg. Copyright © 2013 John Wiley & Sons, Ltd.     

消除与WLAN同频干扰的UWB正交成形脉冲序列设计

提出了产生避免与WLAN同频干扰的UWB正交成形脉冲序列方法,并到了期望的正交成形脉冲序列.仿真结果表明,利用这种方法产生的UWB瞬时成形脉冲的功率谱密度分布符合FCC频谱规定的要求,具有很高的频谱利用率,既可以降低用户间干扰,又解决了UWB与窄带系统同频干扰的问题,可以提高系统的发射功率.     

Creep behavior of ultra‐thin polymer films

A novel microbubble inflation method has been used to determine the creep compliance of poly(vinyl acetate) and polystyrene ultra‐thin films (13–300 nm thick) at temperatures from below to above the glass temperature. We present results that suggest that time‐temperature and time‐thickness superposition hold in the glassy relaxation regime. Although time‐temperature superposition is found for the entire response curve for each thickness, we also find that time‐thickness superposition fails as the long‐time compliance is approached. This effect occurs because of a strong stiffening as the film thickness decreases. We also show first evidence of stiffening in the glassy regime of free standing films of polystyrene. © 2008 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 46: 1952–1965, 2008