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Abstract To improve performances of mass spectrometers dedicated to isotopic or chemical analysis, the methods of the ion optics are to be used. To apply the transfer matrix method of ion optics in mass spectrometer design, the matrix elements of various mass analyzers as Wien filters and crossed field sectors, of energy analyzers as electric prisms, were presented. These elements result from ion trajectory calculations representing solutions of the Euler–Lagrange equations. The basic parameters of an unconventional double focusing mass spectrometer were calculated and compared with those of classical design instruments. 相似文献
123.
ZnO hexagonal prisms have grown on MgO-coated Si (111) substrates by chemical vapor deposition. The process has two steps : the preparation of MgO-coated Si (111) substrates and the preparation of uniform ZnO hexagonal prisms. Some nucleation sites are provided on the Si substrates by the MgO layers, which have the capability to improve the growth of ZnO prisms in the heteroepitaxy. The prisms are single crystals with a preferential growth along the c axis and they are well-faceted at both the end and side surfaces. Room-temperature photoluminescence measurement of these ZnO prisms have shown a strong ultraviolet (UV) emission band centered at 393 nm and a weak green emission band centered at 507 nm, which may be provide an improvement in novel ultraviolet light-emitting devices. In addition, a possible mechanism for the prism growth is proposed based on the analysis by electron microscopy. 相似文献
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125.
采用两种方案对WDF棱镜单色仪的定标曲线进行非线性拟合。通过实验找出棱镜的折射率与TT鼓轮的关系,得到利用科希公式拟合定标曲线的可行性方案;利用高阶多项式对定标曲线进行拟合,运用统计的方法探讨不同的拟合阶数对拟合结果的影响,并得到了最佳的拟合阶数和高精度的拟合结果。 相似文献
126.
讨论在反射法测量三棱镜顶角的实验中,三棱镜在分光计载物台上摆放位置对测量的影响,并提出三棱镜在载物台上的最佳摆放位置。 相似文献
127.
以AlCl3·6H2O为前驱物,在氨水介质中用水热法制备了具有新颖形貌特征的六棱柱状多晶γ-Al2O3颗粒。采用X射线衍射(XRD)、扫描电镜(SEM)、透射电镜(TEM)及N2物理吸脱附等方法对所制备的γ-Al2O3颗粒进行了表征,并对其形貌形成机制进行了分析。结果表明,铝前驱物在氨水介质中通过水热处理后,经焙烧可以形成形貌规整的六棱柱状γ-Al2O3颗粒,其边长与长度分别约为0.3 μm和2.5 μm。TEM图片显示,六棱柱颗粒是由尺寸在10 nm左右的粒子聚集而成,因而具有多晶γ相特征。所制备的γ-Al2O3材料具有发达的孔隙结构,比表面积为274 cm2/g,孔容为0.51 cm3/g,孔径集中分布在5.5 nm周围。研究发现,γ-Al2O3六棱柱形貌的形成机制与AlOOH二次粒子在NH4+正电荷作用下发生的最稳态排列形式具有密切的关联。 相似文献
128.
Single-prism systems are used to fabricate electrically switchable Photonic Crystal (PhC) structures in Polymer Dispersed Liquid Crystal (PDLC) films. The optical configuration is simple, stable and repeatable. A good agreement between theoretical and experimental results is obtained for the PhC structures. Hexagonal far-field diffraction patterns and electrical switching characteristics are also investigated. The smallest droplets of liquid crystals are 10 nm in diameter. The switching voltage can be decreased to 13.3 V/μm. 相似文献
129.
A passively Q-switched laser with Cr4+:YAG/Nd:YAG composite crystal using a corner cube prism cavity has been realized, in which the corner cube prism is the key element as it aids the compensation of the thermal lens effect of laser crystal. Compared with plane–plane mirror cavities under the same conditions, the stability of the laser performance using the corner cube prism cavity was improved remarkably over temperatures ranging from −40 to 65 °C. The decrease of Nd:YAG stimulated emission cross section with temperature was considered to be the main reason for the increase of average output pulse energy under the same cycle for the two different cavities when the ambient temperature changed −40 to 65 °C. The mode properties produced by the prism cavity were analyzed, and the theoretical results were verified by experimental observations. 相似文献
130.
本文提出测量单模波导参数的新方法.用棱镜耦合器测量两种偏振基导模和基漏模的模折射率,并由相应的四个模方程确定单模波导参数.其测量精度优于纯导模测量.用这种方法测量了单模玻璃波导参数,并对误差来源作了理论分析. 相似文献