基于安德雷德通式的旋转黏度计校准方法研究与应用

基于安德雷德通式提出两种旋转黏度计校准方法:安德雷德通式运用法和标准黏度液定值数据拟合法。经过实验验证,安德雷德通式运用法得到旋转黏度计计算黏度示值同实测黏度示值的相对误差在±1%之内;标准黏度液定值数据拟合法得到的旋转黏度计计算修正系数同实测修正系数的相对误差为0.2%~0.4%。安德雷德通式运用法和标准黏度液定值数据拟合法在实际旋转黏度计校准工作中可行,可以提高校准效率。     

头发铅含量测定的应用价值评价

调查了125例2－5岁儿童铅中毒状况,测定其全血铅含量和头发铅含量,以全血铅含量为标准,应用诊断试验评价方法评价头发铅测定的应用价值。结果表明,该试验的灵敏度可达88．3％,应用串联试验,即同时测定头发中锌、铁、钙含量,可将该试验的特异度提高至81．8％,阳性预测值达69．6％,阴性预测值达78．8％。     

Nutritional potential of edible Russula species from Alédjo Wildlife Reserve (AWR)

In order to contribute to the valorisation of wild fungi whose nutritional potential, although considerable, is not sufficiently known in some countries such as Togo, a study has been carried out on Russula species. The diversity of Russula species from Alédjo Wildlife Reserve has been assessed using a focused inventory in woodlands dominated by Isoberlinia doka Craib & Stapf, Isoberlinia tomentosa (Harms) Craib & Stapf, Monotes kerstingii Gilg, Uapaca togoensis Pax and gallery forests dominated by Berlinia grandiflora (Vahl) Hutch & Dalz and Uapaca guineensis Müll. Ethnomycological surveys have been carried out among Tém and Kabyè, two riparian ethnic groups that are mainly represented. Biochemical analyses have been carried out using the AOAC method. Fifteen (15) taxa of edible Russula species are commonly used by Tém and Kabyè people living along the Alédjo Wildlife Reserve among which thirteen (13) taxa have been identified up to species level. R. oleifera is eaten by all interviewed people in both sociolinguistic groups (Fr = 100%) followed by R. compressa (Fr = 92.31%), R. ochrocephala (Fr = 87.18%) among Tém people and R. ochrocephala (Fr = 91.67%), R. compressa (Fr = 83.33%) among Kabyè people. Five (05) new species of edible Russula have been identified for the first time in Togo. The Russula species analysed have been rich in macronutrients with contents ranging from 2.88 g/100 g of dw for fat to 65.83 g/100 g of dw for total carbohydrates. In addition, these Russula species have shown a relatively high mineral content with contents ranging from 405.70 mg/100 g of dw for Ca to 2784 mg/100 g of dw for K. Furthermore, the results have revealed that Russula species analysed are a source of energy with 309.50 Kcal/100 g of dw. The edible Russula species analysed can thus contribute to food security in Togo.     

当代医学生践行社会主义核心价值观现状及对策研究

社会主义核心价值观理论的提出在医学生中产生了广泛的影响。医学生作为国家未来医疗事业的接班人必须树立正确的价值观,但如今医学生对社会主义核心价值观的学习与践行存在着不同的差异,要充分利用校园这一主要的教育阵地,通过加强教师自身教育、医学生人文教育、医学生诚信教育、开展校园文化活动和加大校园宣传等5个方面进行教育指导,帮助医学生树立正确的价值观。     

前置胎盘剖宫产术中止血方案的选择及临床应用价值探讨

目的探讨前置胎盘剖宫产术中止血方案的选择及临床应用价值。方法选取佛山市顺德区妇幼保健院于2011年3月—2014年2月收治的177例剖宫产术中出血的前置胎盘产妇为研究对象,采用随机号码表法分成A、B、C三组,各59例,其中A组予以环形间断缝合术,B组予以"8"字缝合术,C组则采用宫腔纱条填塞术。比对3组产妇术中出血量、输血例数、输血量、术程、止血时间等治疗指标差异,行为期6个月随访,记录其相关并发症发生情况及子宫切除率。结果 1 A组产妇在出血量、输血量、术程及止血时间等治疗指标对比上明显低于B、C组,B组次之,C组止血效果最差,对比差异具有统计学意义(P0.05);2随访期内,A组并发症发生率及子宫切除率低于C组,对比差异具有统计学意义(P0.05)。结论对前置胎盘剖宫产术中出血产妇予以环形间断缝合止血方案,止血效果确切,可有效降低术后并发症发生风险,保宫效果理想,值得临床推广。     

聚异丁烯丁二酰亚胺系列衍生物的合成及其对TiO2纳米粒子的分散性能研究

合成了含有确定长度的聚异丁烯链段与4种不同的乙烯胺链段（乙二胺、二乙烯三胺、三乙烯四胺和四乙烯五胺）组合的聚异丁烯丁二酰亚胺系列衍生物,并将它们用作TiO2纳米粒子在非极性溶剂中的分散剂.详细考察了亲水/亲油基团大小对分散性能的影响规律：当聚异丁烯链段的分子量为2000时,随着乙烯胺段链长的增加,TiO2粒子的粒径和Z...     

参加国家金标准物质定值测试工作的研究报告

近20年来,武警黄金指挥部测试中心参加了12个国家矿石金、12个国家痕量金分析标准物质定值测试工作.该文对取样量、样品均匀性检验、样品焙烧、分析方法的选取、样品稳定性检验等技术进行了总结,并对今后金标准物质的研制提出了建议.     

差示扫描量热法对芝麻酚纯度标准物质的定值

建立了采用差示扫描量热法对芝麻酚纯度标准物质的定值及不确定度评价的数学模型、有效检测技术和分析方法.采用差示扫描量热法测量芝麻酚样品纯度的实验条件为升温速率3.0 K/min,称样量3.4～4.7 mg,炉内气体为静态空气.对通过均匀性检验和长期稳定性考察的芝麻酚纯度标准物质进行定值和不确定度评价,同时采用高效液相色谱...     

Anion and pH-regulated assembly of three Cd(II) coordination polymers based on 3,5-di(1H-benzo[d]imidazol-1-yl)benzoate

Three coordination polymers, {[CdI(DBBA)]?0.5H₂O}_n (1, DBBA = 3,5-di(1Hbenzo[d]imidazol-1-yl)benzoate), [Cd(DBBA)(CH₃COO)]_n (2) and [Cd(DBBA)₂]_n (3), were obtained through reactions between Cd(II) salts and 3,5-di(1H-benzo[d]imidazol-1-yl)benzoic acid under different pH conditions. Compounds 1 and 2 are 3-D frameworks with rtl topology based on different binuclear Cd(II) secondary building units. Compound 3 was formed at lower pH and showed a 1-D chain assembled with M₂L₂ ring units. Moreover, phase purities, thermal behaviors, and photoluminescent properties have also been investigated.     

氢火焰离子化检测器校正因子的理论计算

根据FID检测器工作原理,提出一种相对质量校正因子的计算公式。由该公式出发可以推导出相对摩尔响应值（RMR）与化合物碳数的线性关系式和有效碳数的近似计算方法,并赋予原计算方法中的参数以明确的含意,解决了参数之间的矛盾。新方法的计算值同文献数据吻合良好。