WO3掺杂的La2/3Sr1/3MnO3电输运与磁电阻特性

通过溶胶-凝胶法制备了La2／3Sr1／3MnO3＋xWO3（x=0～25％）系列多晶陶瓷样品．结果表明。随着WO3掺杂量的增加，样品的电阻率增大，金属-绝缘体相变温度（Tp）值下降．在1．4T磁场下，当0≤x≤12．5％时，样品的室温磁电阻值从5％增大到15％，提高了200％．当12．5％〈x≤25％时，室温磁电阻值从15％降低到0．这对磁电阻材料在室温下的应用提供实验依据．     

异硫氰酸荧光素标记抗体的固体基质室温磷光性质研究

研究了异硫氰酸荧光素（FITC）标记的羊抗人抗体（GAHAb-FITC)和兔抗羊抗体9RAGAb-FITC)，及其以三种免疫方式与人免疫球蛋白（IgG)反应所得免疫复合物在多种固体薄膜基质上发射室温磷光（RTP）的适宜条件及其光谱，强度和寿命等性质。研究发现，标记抗体及其免疫复合物保留了FITC优良的固体基质室温磷光性质，λ m0643em^(max)=525/650nm，其RTP强度与其浓度线性相关，并有很高的灵敏度，更为重要的是，免疫反应及其RTP检测能结合于同一基质，方便地相继完成，在聚酰胺膜（PM）上，以Pb(Ac)2为重原子微扰剂，稀释比为1：10（ψ）的GAHAb-FITC,RAGAb-FITC及其与人IgG形成的免疫复合物均能发射较强制 RTP信号并有较长的RTP寿命，本结果为建立相应的固体基质室温磷光免疫分析（SS-RTP-IA）新方法奠定了相应的实验基础。     

Co离子注入TiO2薄膜的显微结构和磁性研究

利用直流磁控溅射技术在玻璃衬底上沉积了TiO₂薄膜,并对其进行了Co离子注入,最后在真空中500 ℃退火50 min,得到系列薄膜样品. 利用剥离-分散方法制备了薄膜的透射电镜样品,并用扫描电镜(SEM)、X射线能量散射谱(EDX)和高分辨透射电镜(HRTEM)对样品做了近似原位观察,研究了薄膜样品中不同Co离子注入深度的成分分布和显微结构. 结果表明,薄膜呈锐钛矿结构,Co元素主要分布在薄膜表层,Co离子的注入使TiO₂薄膜的晶粒被部分破坏,并形成CoO,而5 关键词： 2薄膜')" href="#">Co注入TiO₂薄膜 电镜原位观察 室温铁磁性     

Radiation background due to radioactive sources in a luminescence dating laboratory

For practical reasons, usually, luminescence dating laboratories contain in the same room (or in adjacent rooms) the equipment and the radioactive sources, as well as the storage cabinet for the samples. It is generally assumed that the absorbed dose due to ambient radioactivity is null or at least negligible in terms of human health (below the dose limit).To test the actual dose rate inside our laboratory room, an investigation combining portable dose rate meter, portable NaI(Tl) gamma spectrometry, and blue-OSL dosimetry using Al₂O₃:C pellets was made. Although our measurements show the presence of X-rays as far as 3 m from the sources, the dose rates are below the safety regulation and does not affect the dating of the sample stored in the same room as the radioactive sources.     

Growth and characterization of InAs quantum dots with low-density and long emission wavelength

The growth parameters affecting the deposition of self-assembled InAs quantum dots （QDs） on GaAs substrate by low-pressure metal-organic chemical vapor deposition （MOCVD） are reported. The low-density InAs QDs （- 5 × 10^8cm^-2） are achieved using high growth temperature and low InAs coverage. Photoluminescence （PL） measurements show the good optical quality of low-density QDs. At room temperature, the ground state peak wavelength of PL spectrum and full-width at half-maximum （FWHM） are 1361 nm and 23 meV （35 nm）, respectively, which are obtained as the GaAs capping layer grown using triethylgallium （TEG） and tertiallybutylarsine （TBA）. The PL spectra exhibit three emission peaks at 1361, 1280, and 1204 nm, which correspond to the ground state, the first excited state, and the second excited state of the ODs, respectively.     

Size Effect of the Immediate Surround for the Border between the Natural and Unnatural Object Color Appearance

The border luminance of the test stimulus between the natural and unnatural object color, y_ynB_u was obtained for different spatial sizes of the immediate surround to prove that _nB_u can be determined based on a new recognized visual space of illumination (RVSI) that is assumed to be constructed for the immediate surround separately from the RVSI for the subjects room itself. The _nB_u of five test stimuli were determined for six different sizes covering from zero to 1866 cm² with four different lightnesses, N4, N6 and N8, while keeping the room illuminance constant at 100 or 600 lx. The results showed that luminance of the border _nB_u gradually decreased as the size of the immediate surround was increased and that the decrease was larger for immediate surround with lower lightness. The results were interpreted as showing a new RVSI constructed for the spatial extent of the immediate surround of the test stimulus, and the RVSI was more completely constructed for larger spatial size of the immediate surround. © 2005 The Optical Society of Japan     

喷水室典型空气处理过程中空气流速的实验研究

针对纺织厂空调系统的核心-喷水室,研究喷水室内处理空气的冷却减湿和等焓加湿两个典型热湿交换过程。提出Re准数对传热传质有显著作用,而Re数的大小取决于流体速度。通过实验研究当空气流速从3m/s提高到5m/s时对喷水室热湿交换性能的影响,从而确定空气流动速度因素对两个热湿交换效率的影响趋势。根据拟合的数学曲线,总结出当空气的流动速度提高后,热湿交换效率相应提高。从而推动高速喷水室在实际工程中的应用。     

Performance Evaluation and Effectiveness of the Reverberation Room

This research presents a thorough evaluation of the reverberation room at Acoustics Laboratory in National Institute of Standards (NIS) according to the related international standards. The evaluation aims at examining the room performance and exploring its effectiveness in the frequency range from 125 Hz to 10000 Hz according to the international standard requirements. The room, which was designed and built several years ago, is an irregular rectangular shape free from diffusers. Its volume is about 158.84 m³, which meets the requirement of the ISO 354 standard L_max < 1.9V^1/3. Cut-off frequencies of one and one-third octave are 63 Hz and 100 Hz respectively; however Schroder frequency is 400 Hz. Calculations of cut-off frequency and modal density showed adequate modes that give acceptable uniformity starting comfortably from frequency of 125 Hz. The room has a reverberation time that is suitable for its size over the frequency range of interest. The room sound absorption surface area and its sound absorption coefficient satisfy the criteria given in ISO 3741 and ISO 354. There is an accepted diffuse sound field inside the room due to the standard deviation of measured sound level, which is less than 1.5 dB over all the frequency range. The only exception was 125 Hz which may be due to a lack of diffusivity of the sound field at this frequency. The evaluation proves that the NIS reverberation room is in full agreement with the international standards, which in turns qualifies the room to host measurements inside without concerns.     

A Hydrogen Peroxide Biosensor Based on Room Temperature Ionic Liquid Functionalized Graphene Modified Carbon Ceramic Electrode

A room temperature ionic liquid (IL) 1‐butyl‐3‐methylimidazolium hexafluorophosphate functionalized graphene (GE) was prepared and a hydrogen peroxide (H₂O₂) biosensor was fabricated by immobilizing hemoglobin (Hb) into the IL‐GE composite film. UV‐visible and Fourier transform infrared spectra of the composite film indicated that Hb retained its native structure in the film. Electrochemical investigation of the biosensor showed a pair of well‐defined, quasi‐reversible redox peaks with E_pa=?0.209 V and E_pc= ?0.302 V (vs. SCE) in pH 7.0 phosphate buffer solution at the scan rate of 100 mV/s. To the reduction of H₂O₂, the biosensor had a good linear range from 8.0×10^?7 to 1.8×10^?4 mol/L with a detection limit of 3.0×10^?7 mol/L. The apparent Michaelis‐Menten constant K^app_M was estimated to be 3.4×10^?5 mol/L.