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121.
Shahrukh T. Asundaria Keshav C. Patel Kalpesh M. Mehta 《Phosphorus, sulfur, and silicon and the related elements》2013,188(7):1554-1562
Abstract Novel 3-[4-(6-bromo-4-oxo-2-phenylquinazolin-3(4H)-yl)benzoyl]-2-substituted-1,3,4-thiazolium-5-thiolate 7(a–j) and 3-{4-[(6-bromo-2-phenylquinazolin-4-yl)amino] benzoyl}-2-substituted-1,3,4-thiadiazolium-5-thiolate 12(a–j) were synthesized from 6-bromo-2-phenyl-4H-3,1-benzoxazin-4-one (1). The structures of the newly synthesized compounds were confirmed by spectral data and elemental analysis. Supplemental materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements to view the free supplemental file. GRAPHICAL ABSTRACT 相似文献
122.
3-phenyl-2-thioxo-quinazolin-4(3H)one 1 was utilized for the construction of some novel 2-substituted quinazolin-4(3H)one derivatives through the formation of 2-hydrazinyl quinazolinone, which was used as the key starting material for the synthesis of 2-heteryl quinazolines via the reaction with one carbon donors, β-diketones and β-ketoester. Infrared, 1H NMR, and mass spectra of the synthesized compounds were discussed. Some of them showed promising anti-inflammatory activity. Supplemental materials are available for this article. Go to the publisher's online edition of Synthetic Communications® to view the free supplemental file. 相似文献
123.
124.
Nader M. Boshta Farag A. El-Essawy Mohammed B. Alshammari Safaa G. Noreldein Osama M. Darwesh 《Molecules (Basel, Switzerland)》2022,27(12)
In this paper, we report on the design and synthesis of a novel series of quinazoline-2,4(1H,3H)-dione derivatives as fluoroquinolone-like inhibitors of bacterial gyrase and DNA topoisomerase IV to identify and develop antimicrobial agents to prevent bacterial resistance problems. Their structures were confirmed using spectroscopic analyses (IR, NMR, and EI-MS). The novel quinazoline-2,4(1H,3H)-dione derivatives were evaluated for their antimicrobial activities against Gram-positive and Gram-negative bacterial strains using the Agar well diffusion method to study the antimicrobial activities and compared them with the standard drugs. Most compounds displayed moderate activity. Among the tested compounds, the most promising compounds 13 and 15 provided broad bioactive spectrum against Gram-positive and Gram-negative strains compared to the standard drugs. 相似文献
125.
Swadhin Chetia Samprity Sarmah Dr. Apurba Dutta Prof. Diganta Sarma 《European journal of organic chemistry》2023,26(26):e202300390
A copper acetate monohydrate catalyzed simple, effective and economic protocol has been developed for the construction of quinazoline derivatives via acceptorless dehydrogenative coupling of easily available 2-aminoaryl methanols and nitriles. The methodology was also highly effective for the synthesis of medicinally important quinolines analogues. The reactions proceeded in presence of KOtBu in toluene at 110 °C for 5 h without the requirement of inert condition, external additives and ligands. 相似文献