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Summary An equilibrium sandwich chamber for continuous thinlayer chromatography was used to study overloaded systems of the heptane + methylene chloride-silica type. Mixtures of two or three dyes were used as the model samples. Wide starting zones were formed using a glass distributor (frontal chromatography stage), then the movement of the zones was recorded during continuous elution. The effect of sample concentration and volume on the maximum separation yield was investigated. Band compression effects are illustrated for samples dissolved in solvents having a low eluent strength. Satisfactory analogy was found to separations in preparative column chromatography. Good separation yield was obtained for frontal + elution TLC: depending on the differences in the RF values of the components, 6–16 mg samples were completely separated on 0.5×100×75 mm layers containing ca. 1 g of silica.Presented at the Eighth International Symposium on Liquid Chromatography, Baden-Baden, 3–7 May 1983. 相似文献
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低Z流体的单次冲击波压缩极限是判断各种研究高压物态方程理论和实验正确与否的重要参数。维里定律和Hugoniot方程表明,单次冲击波压缩率是由各种因素的相对重要度决定的,包括平均势能、平均动能、内部自由度的激发度和逆幂函数型势能曲线的幂指数。如果幂指数大于2,相互作用势能使流体变得比理想气体更难压缩,否则流体就比理想气体更容易压缩。内部自由度的激发总是让流体变得更容易压缩。在各种不同因素起主导作用的压强段,低Z流体的单次冲击波压缩极限不同。用一个简单的单次冲击波压缩极限的表达式解释了低Z流体在离解区域和电离区域的行为。 相似文献
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The Heavy Ion Research Facility and Cooling Storage Ring(HIRFL-CSR)accelerator in Lanzhou offers a unique possibility for the generation of high density and short pulse heavy ion beams by non-adiabatic bunch compression longitudinally,which is implemented by a fast jump of the RF-voltage amplitude.For this purpose,an RF cavity with high electric field gradient loaded with Magnetic Alloy cores has been developed.The results show that the resonant frequency range of the single-gap RF cavity is from 1.13 MHz to 1.42 MHz,and a maximum RF voltage of 40 kV with a total length of 100 cm can be obtained,which can be used to compress heavy ion beams of 238U72+ with 250 MeV/u from the initial bunch length of 200 ns to 50 ns with the coaction of the two single-gap RF cavity mentioned above. 相似文献
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对嗜酸乳杆菌、变异链球菌和保加利亚乳杆菌这三种菌的荧光光谱进行研究,发现在紫外光的激励下,益生菌溶液发出荧光.在最佳激发波长290 nm的激励下,荧光峰值在300—650 nm范围内.采用小波变换对测得的150组光谱数据进行压缩,压缩后每组数据由原来的1341个点减少为168个点,既保留了原图谱的特征,又提高了神经网络的处理速度.径向基函数神经网络方法对压缩后的数据进行研究,对每种菌的40组实验数据进行训练,在此基础上对30组未知数据进行识别.结果表明经过训练之后,径向基函数神经网络能够准确预测未知菌种. 相似文献
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In [Found. Comput. Math., 2 (2002), pp. 203-245], Cohen, Dahmen, and DeVore proposed an adaptive wavelet algorithm for solving general operator equations. Assuming that the operator defines a boundedly invertible mapping between a Hilbert space and its dual, and that a Riesz basis of wavelet type for this Hilbert space is available, the operator equation is transformed into an equivalent well-posed infinite matrix-vector system. This system is solved by an iterative method, where each application of the infinite stiffness matrix is replaced by an adaptive approximation. It was shown that if the errors of the best linear combinations from the wavelet basis with terms are for some , which is determined by the Besov regularity of the solution and the order of the wavelet basis, then approximations yielded by the adaptive method with terms also have errors of . Moreover, their computation takes only operations, provided , with being a measure of how well the infinite stiffness matrix with respect to the wavelet basis can be approximated by computable sparse matrices. Under appropriate conditions on the wavelet basis, for both differential and singular integral operators and for the relevant range of , in [SIAM J. Math. Anal., 35(5) (2004), pp. 1110-1132] we showed that , assuming that each entry of the stiffness matrix is exactly available at unit cost.
Generally these entries have to be approximated using numerical quadrature. In this paper, restricting ourselves to differential operators, we develop a numerical integration scheme that computes these entries giving an additional error that is consistent with the approximation error, whereas in each column the average computational cost per entry is . As a consequence, we can conclude that the adaptive wavelet algorithm has optimal computational complexity.
180.
An approach to highly enhance the compression efficiency of the integral images by applying the Karhunen-Loeve transform (KLT) algorithm to the motion-compensated sub-images is proposed. The sub-images transformed from the elemental images picked-up from the three-dimensional (3D) object might represent the different perspectives of the object. Thus, the similarity among the sub-images gets better than that among the elemental images, so that an improvement of compression efficiency of the sub-images could be obtained. However, motion vectors occurred among the sub-images might result in an additional increase of image data to be compressed. Accordingly, in this paper, motion vectors have been estimated and compensated in all sub-image in advance. Then the KLT algorithm was applied to these motion-compensated sub-images for compression. It is shown from some experimental results that compression efficiency of the proposed method has been improved up to 24.44%, 40.62%, respectively, on the average compared to that of the conventional KLT compression method and that of the JPEG. 相似文献