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901.
环氧树脂电气绝缘性能优良, 但是其在脉冲功率设备中充当绝缘子时, 表面容易带电且不易衰减, 当表面电荷集聚到一定的程度会造成局部放电甚至发展为沿面闪络。为了提高环氧树脂的沿面闪络性能, 用中心粒径为1 m的氢氧化铝(ATH)无机填料来改善环氧树脂复合材料的表面性能。分别制备了ATH填料质量分数为0%(纯环氧) , 20%, 40%, 60%, 80%和100%的ATH/环氧树脂复合材料试样。用电声脉冲法研究了ATH填料对环氧树脂复合材料电荷衰减性能的影响, 对比了试样直流极化场强为10 kV/mm和30 kV/mm的试验结果。结果表明:ATH/环氧树脂复合材料电荷的衰减常数不仅与填料的质量分数有关, 而且与试样的带电量有关。 相似文献
902.
Tabish Aftab;Osbel Almora;Josep Ferre-Borrull;Lluis F. Marsal; 《固体物理学:研究快报》2024,18(11):2400144
This study investigates the preparation of nickel nanostructured electrodes for the enhancement of supercapacitor performance. The nanostructured electrodes are synthesized using nanoporous anodic alumina (NAA) as a template via the pulsed electrodeposition method. Structural properties are examined using field-emission scanning electron microscopy, while electrochemical characterization is conducted through cyclic voltammetry (CV) and electrochemical impedance spectroscopy. The results reveal that Ni nanorod arrays can be obtained embedded in the NAA matrix and with electrical contact with the aluminum substrate. On average, the rods are spaced 90 nm apart, with a diameter of 70 nm and a length of 2 μm. The Ni@NAA electrode exhibits an enlarged active area and exceptional electrochemical performance, demonstrating remarkable stability over 5000 cycles of CV at a scan rate of 50 mV s−1. Specific capacitance values exceeding 100 mF cm−2 and maximum charging times of less than 10 min are reported, highlighting its suitability for high-power energy devices requiring pseudo-supercapacitance. The study underscores the significance of nanostructured electrodes in advancing energy storage technologies and presents promising prospects for practical applications. 相似文献
903.
Niray Bhakta;Alexander S. Kaplitz;Destini Black;Kevin A. Schug; 《Journal of separation science》2024,47(18):e202400500
A commercially available dielectric barrier discharge ionization (DBDI) source was tested with supercritical fluid chromatography-mass spectrometry (SFC-MS). The compound mixture investigated comprised caffeine, theobromine, theophylline, uracil, testosterone, and pyrene, diluted in methanol. Dynamic response ranges were evaluated with multiple injections at different concentrations. Precision studies demonstrated the robustness and sensitivity of the ionization source across a concentration range of 10–1000 ng/mL. Results from this experiment showed linear regression of 0.99 or greater for all analytes tested over the range with a relative standard deviation (RSD) of less than 10% down to 10 ng/mL for all analytes except theobromine, which had an RSD of less than 10% down to 25 ng/mL. Notably, this study marks the first investigation of sensitivity for coupling a commercial DBDI source with SFC; a limit of detection less than 1 ng/mL was achieved for all compounds. This study demonstrates chromatographic separation by SFC and MS analysis for compounds that ionize poorly using traditional atmospheric pressure ionization, such as polycyclic aromatic hydrocarbons. Combining SFC with the DBDI source opens promising avenues for analyzing compounds that were previously challenging to characterize with standard atmospheric pressure ionization techniques. 相似文献
904.
Haobo Lin;Ningtao Liu;Wei Wang;Xiaoli Zhang;Dongyang Han;Wenrui Zhang;Jichun Ye; 《固体物理学:研究快报》2024,18(6):2400023
Epitaxial thin films of tantalum-doped β-Ga2O3 (Ta-Ga2O3) are grown on MgO (001) substrates to study the effect of Ta doping on the electrical properties of β-Ga2O3 films. X-Ray diffraction (XRD) measurements show that the films with different Ta doping concentrations are (00l)-oriented single-crystalline β-Ga2O3 without impurity phases. The incorporation of the Ta element modifies the electrical properties of Ta-Ga2O3 films significantly. At a very low doping ratio of 0.05 mol%, the Ta-Ga2O3 film showed a minimum resistivity of 2.32 Ω cm and a carrier concentration of 2.48 × 1017 cm−3. The corresponding activation energy of Ta element in the film is 16.8 meV, suggesting that the Ta element is a promising shallow donor dopant. The X-ray photoelectron spectroscopy (XPS) analysis confirms that the Fermi level of the Ga2O3 films shifts toward the conduction band minimum after the introduction of Ta ions. These results indicate that the transition metal element Ta could be an effective n-type dopant for modulating the carrier transport behavior of β-Ga2O3 films. 相似文献
905.
The acoustic signals generated in solids due to interaction with pulsed laser beam is used to determine the ablation threshold
of bulk polymer samples of teflon (polytetrafluoroethylene) and nylon under the irradiation from a Q-switched Nd:YAG laser
at 1.06μm wavelength. A suitably designed piezoelectric transducer is employed for the detection of photoacoustic (PA) signals generated
in this process. It has been observed that an abrupt increase in the amplitude of the PA signal occurs at the ablation threshold.
Also there exist distinct values for the threshold corresponding to different mechanisms operative in producing damages like
surface morphology, bond breaking and melting processes at different laser energy densities. 相似文献
906.
907.
Self‐consistent two‐dimensional (2D) simulations of short‐pulsed dielectric barrier discharge (DBD) in pure xenon have been performed. It is shown that during short current pulse the traversal inhomogeneity of the plasma parameters can be important only at the end of the current pulse as an edge effect close to the side walls. During the current pulse, the gap voltage drops until the ionization wave reaches the cathode so the current in the cathode sheath is the displacement current. This means that almost all of the absorbed power is deposited into excitation of xenon atoms and not to the ion heating in the cathode sheath as in the traditional glow discharges. This fact is one of the reasons of high efficiency of short‐pulsed DBD. The developed model allows one to estimate the temporal position of the plasma‐sheath boundary. (© 2006 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim) 相似文献
908.
本文分析了原真空获得与测量实验装置结构上的不足之处.介绍了对原装置所进行的改进工作──主要用于取代感应圈的专用电源的制作。 相似文献
909.
S. Klagge 《Plasma Chemistry and Plasma Processing》1992,12(2):103-128
To consider the anisotropy of the plasma in the sheath regions, Langmuir probe characteristics are measured using a direction-resolving technique. The operation frequency, related to the neutral gas density (/p0), is chosen in such a way that the electron velocity distribution function (VDF) may be regarded as frozen and the probe diagnostic may be performed without time resolution. In order to prevent convolution of the VDF from the effect of the time-dependent plasma potential, the rf component of the probe bias voltage is compensated to a minimum. The plasma potential, the mean energy of the electrons, and the electron density, averaged over the discharge bulk, are presented as functions of the discharge current and the neutral gas pressure for the O2 gas. By means of a reactor model based on the theory of plane probes and using the plasma parameter measured, the sheath and bulk portions of the maintaining voltage are separated. In this procedure the thickness of the sheaths in front of the electrodes and the phase difference between discharge current and maintaining voltage are also obtained. 相似文献
910.
Experiments are performed to develop a pulsed corona discharge system for the conversion ofmethane to hydrogen at atmospheric pressure (≌760 Torr) without using a catalyst. The corona dischargewas energized by 10-12 μs wide voltage pulses (≤7 kV) at a repetition rate of about 1.0-1.5 kHz. Theresidual gases were characterized by mass spectrometry. The conversion of methane is as high as 50.8% producing the 70% yield of hydrogen. The influences of argon on the discharge of methane were studied.This result could be useful for the mass production of hydrogen in both academic and industrial point ofview. 相似文献