表面状态对强流脉冲电子束辐照诱发金属表面熔坑的影响

 为了考察材料晶体学特性对表面熔坑形成机制的影响,利用强流脉冲电子束（HCPEB）对喷丸前、后的304奥氏体不锈钢进行表面辐照处理,对HCPEB诱发的表面熔坑形貌进行了详细的表征。实验结果表明,HCPEB辐照后样品表面形成了大量的火山状熔坑,熔坑数密度和熔坑尺寸随电子束能量的增加而减小,材料表面的杂质或夹杂物容易成为熔坑的核心,并在熔坑形成的喷发过程中被清除,起到净化表面的作用。此外,喷丸前、后样品表面熔坑数密度遵循相似的分布规律,喷丸处理使熔坑数密度显著增大,表明材料的晶体学特性对表面熔坑形成有重要的影响,晶界、位错等结构缺陷是熔坑形核的择优位置。     

Pigment identification and decoration analysis of a 5th century Chinese lacquer painting screen: a micro‐Raman and FTIR study

To investigate the pigments and decoration applied to a wood‐based lacquer painting screen from the tomb of Si‐ma Jin‐long, Shanxi Province, central China, made by Chinese craftsmen in the 5th century, a combination of micro‐Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), wavelength dispersive X‐ray fluorescence (WDXRF), and microscopic examination was used. The obtained results are as follows: (1) the black, yellow, and red colors are identified as carbon black, orpiment and realgar, and cinnabar, respectively, by using micro‐Raman spectroscopy. The FTIR result shows that the white pigment filled in the leaves is not lead white, as assumed in the literature, but gypsum. Whether lead white was used at other locations remains unanswered and requires more samples for further work; (2) the thickness of each discernable pigment layer, as observed under the microscope, is approximately equal and the differences among them are small, suggesting a superfine painting skill; besides, a noticeable smooth interface between wood and the red grounding substance indicates that a polishing process might have been applied before the painting; (3) the red background was proved to contain cinnabar, but further FTIR analyses found no evidence for the presence of Chinese wood oil; and (4) the most interesting finding, rarely reported before, is that white grains of different sizes are found in both pigment layers and the grounding substance, which are perhaps an intentional addition. Further, in situ XRF and Raman analyses indicate that they are sourced from hydroxyapatite, coming probably from the intentional addition of animal bone ash to the lacquer. But how such a process could be finished and what purpose it served have not yet been answered. Copyright © 2009 John Wiley & Sons, Ltd.     

管内变密度流体的充分发展流动与换热

本文提出了圆管内变密度流体流动与换热充分发展的概念及其相关假设.在所提出的概念和假设基础上给出了摩擦阻力系数Cf与Nusselt数Nu的定义式和计算式.通过对圆管内密度随温度变化的氩气的流动与换热所进行的数值模拟,验证了在本文的计算条件范围内,圆管内变密度流体充分发展流动与换热的概念是合理的,并且CfRe=16,Nu=4.36.     

Rugged distal tips for CO2 laser medicine

Low-loss and rugged distal tips for CO₂ laser have been proposed and fabricated based on a commercially available stainless steel (St) pipe. A method of smoothening the inner surface of the St pipe with a rough inner surface is put forward. Fabrication parameters, transmission properties, and mechanical strength of the cyclic olefin polymer-coated silver hollow St distal tip are experimentally discussed.     

光电倍增管在磷酸液声致发光实验中的应用

对不同厚度液体进行光强测量,深入探索空化气泡的运动,研究发光机理很有意义。用超声激励法在磷酸液体中实现多泡声致发光,研究不同共振频率下发光的特点。利用光电倍增管多次测量发光强度相互比较,结果是在液体厚度10 cm、驱动频率f=21.061kHz和f=20.316kHz时,周期性较好为50μs,液体通过漩涡集中气泡可以使更多气泡发光;在液体厚度3 mm、驱动频率f=17.91kHz和f=19kHz时,周期性很好为25μs;且光信号都较强。结论是磷酸中声致发光强度、周期与液体厚度、驱动频率密切相关。本文以磷酸液多泡声致发光实验研究为基础,从内部和外部原理来出发,详细介绍了光电倍增管在多泡声致发光光强测量中的实用,为今后研究者提供了一些经验。根据实验过程中遇到的一些实际问题提出了建议和改善意见。     

A novel slotted helix slow-wave structure for high power Ka-band traveling-wave tubes

A novel slotted helix slow-wave structure （SWS） is proposed to develop a high power, wide-bandwidth, and high reliability millimeter-wave traveling-wave tube （TWT）. This novel structure, which has higher heat capacity than a conven- tional helix SWS, evolves from conventional helix SWS with three parallel rows of rectangular slots made in the outside of the helix tape. In this paper, the electromagnetic characteristics and the beam-wave interaction of this novel structure operating in the Ka-band are investigated. From our calculations, when the designed beam voltage and beam current are set to be 18.45 kV and 0.2 A, respectively, this novel circuit can produce over 700-W average output power in a frequency range from 27.5 GHz to 32.5 GHz, and the corresponding conversion efficiency values vary from 19% to 21.3%, and the maximum output power is 787 W at 30 GHz.     

基于扭秤的激光干涉差动测量微小冲量方法

基于扭秤测量冲量原理,结合激光干涉法差动测量角度的方法,提出一种基于扭秤的激光干涉差动测量微小冲量的方法。介绍系统的基本组成和测量过程,给出扭秤结构设计参数,并对系统参数进行了标定,结合设计参数与标定结果,对系统的分辨率、量程和精度进行了校核,在典型的测量环境下,对激光烧蚀靶材所形成的Ns量级微小冲量进行了测量,给出了典型的测量结果并进行分析。结果表明:所提出的基于扭秤的激光干涉差动测量微小冲量方法,系统分辨率可达10-7Ns量级,测量范围跨5个数量级,最大可以测量10-2Ns量级冲量,测量精度优于95%。     

微型X射线管靶材厚度理论计算与出射光谱模拟研究

根据端窗透射微型X射线管阳极靶的结构,建立了数理模型,讨论了电子束打靶的平均厚度与光管高压的关系,得到了X光管出射特征光谱强度的角度分布特征。同时利用Monte Carlo方法,对出射光谱在2π方向上的强度分布特征开展模拟研究。结果表明,微型X射线管阳极靶材平均厚度在2 μm左右,在与入射电子束垂直方向几度的范围内获得的出射光谱其单色性较好。这些结论对于微型X射线管的结构设计和出射光谱单色化应用具有一定的理论指导意义。     

Influence of oxidation time on semiconductive behaviour of thermally grown oxide films on AISI 304L

The oxide films formed on AISI 304L stainless steel at 300 °C in the oxidation time range between 2 and 4 h have been studied by photoelectrochemistry. Photocurrents were investigated as a function of the wavelength of the incident light and the electrode potential. The investigation allowed the determination of the semiconductive properties of the oxides. The oxide films showed n-type behaviour. A duplex structure of the oxide films has been suggested on the basis of the photocurrent spectra, with an internal oxide layer having an optical gap (E_g2 = 2.16-2.3 eV) depending on the applied potential and oxidation time, higher to that of the external oxide layer (E_g1 ≈ 1.9 eV). Significant variations in the amplitude of the photocurrent were detected as a function of the applied potential and the oxidation time.     

小波时-频变换的高强钢丝弹性波传播模态分析

超声导波是近年来桥梁拉索无损检测研究的重要方法之一。针对弹性波在高强钢丝介质中传播的多模态频散问题,采用单点时域波形的小波时频变换进行混叠信号的模态识别分离。通过数值求解Pochhammer频率超越方程,计算得到0~1.5 MHz范围内纵向导波模态理论频散曲线;采用有限元模拟半波正弦脉冲激励导波在钢丝中传播过程,由小波时-频变换得到导波模态分布,并进行了不同腐蚀程度钢丝实验对比分析。结果表明,经小波时-频变换得到的第1、2、3阶纵向导波模态与理论值对应吻合,单点时域波形的小波时-频变换结果能够有效识别高强钢丝中的导波模态;钢丝在无腐蚀状态下,一阶纵向导波模态能量占比达57.74%,随腐蚀程度增加,能量更为集中到一阶纵波模态,二阶模态能量逐渐减小。