Determination of three compounds in Aloe vera by capillary electrophoresis

A capillary electrophoretic assay for determining aloe-emodin (AE), methyl p-coumarate (MC), and 3,4-dihydro-6,8-dihydroxyl-[(3s)-2'-acetyl-3'-hydroxyl-5'-methoxy-benzyl]-isocoumarin (DDI) in Aloe vera has been developed. Baseline separation was achieved within 15 min using a running buffer of 20 mm borax containing 10% (v/v) acetonitrile at pH 10.5. A linear relationship between the peak area and the concentration of the analytes was found in the ranges 5-500, 10-1000 and 2-1000 micro g/mL for AE, MC and DDI, respectively, with correlation coefficients of 0.9992-0.9998. The relative standard deviations of migration time and peak area were within 0.17-0.19 and 1.52-3.37%, respectively. The recoveries of AE, MC and DDI were 105, 102 and 96.4%. The contents of AE, MC and DDI in Aloe vera were measured to be 5.13, 0.768 and 1.30 mg/g, respectively.     

考虑振源阻抗影响的动力吸振器优化设计

本文从四端参数技术入手,着重研究振源特性对动力吸振器优化设计的影响,进行了理论推证。且与传统优化设计进行比较,最后通过回转惯性振源的计算,进行了讨论.     

Six‐Coordinate Group 13 Complexes: The Role of d Orbitals and Electron‐Rich Multi‐Center Bonding

Bonding in six‐coordinate complexes based on Group 13 elements (B, Al, Ga, In, Tl) is usually considered to be identical to that in transition‐metal analogues. We herein demonstrate through sophisticated electronic‐structure analyses that the bonding in these Group 13 element complexes is fundamentally different and better characterized as electron‐rich hypervalent bonding with essentially no role for the d orbitals. This characteristic is carried through to the molecular properties of the complex.     

Taming Tin(IV) Polyazides

The first charge‐neutral Lewis base adducts of tin(IV) tetraazide, [Sn(N₃)₄(bpy)], [Sn(N₃)₄(phen)] and [Sn(N₃)₄(py)₂], and the salt bis{bis(triphenylphosphine)iminium} hexa(azido)stannate [(PPN)₂Sn(N₃)₆] (bpy = 2,2′‐bipyridine; phen = 1,10‐phenanthroline; py = pyridine; PPN = N(PPh₃)₂) have been prepared using covalent or ionic azide‐transfer reagents and ligand‐exchange reactions. The azides were isolated on the 0.3 to 1 g scale and characterized by IR and NMR spectroscopies, microanalytical and thermal methods and their molecular structures determined by single‐crystal XRD. All complexes have a distorted octahedral Sn[N]₆ coordination geometry and possess greater thermal stability than their Si and Ge homologues. The nitrogen content of the adducts of up to 44 % exceed any Sn^IV compound known hitherto.     

On Cartan's theorem for linear operators

In this paper, we describe a second main theorem of holomorphic curves in , of hyper‐order strictly less than 1, that involves a general linear operator . As an application, we derive a truncated second main theorem of degenerate holomorphic curves of hyper‐order strictly less than 1 using Nochka weights.     

水资源短缺风险因子的筛选模型

水资源短缺评价首先需要确定指标体系,投影寻踪模型与灰色关联度法相结合,可以有效地筛选出水资源短缺风险因子,为进一步进行风险评价奠定了基础,同时也为制定风险的防范措施和对策提供了理论依据.综合应用这两种模型,对北京市2001～2009年的水资源短缺风险进行研究,结果表明:降水量、日照时数、雨日数、单位GDP污水排放量、人均GDP、工业总产值占有率、污水处理率和水循环使用率这8个指标是北京市水资源短缺的主要风险因子.     

12 MeV直线感应加速器主开关的优化设计

介绍了12MeV直线感应加速器主开关的一种优化设计。在保持原有主开关的设计风格和接口结构的条件下,通过优化设计局部结构和调整开关电极尺寸,把主开关的结构电感从63.7nH减小到35nH,使得加速腔的高压脉冲前沿从39.6ns减小到27ns,从而有利于提高12MeV直线感应加速器的性能,验证了优化设计的可行性。     

放电等离子体极紫外光源中的主脉冲电源

描述了Z箍缩放电等离子体极紫外光源系统中的主脉冲电源,给出了主电路拓扑结构,重点介绍了三级磁脉冲压缩网络,给出了关键参数的设计计算,并且介绍了新颖的末级磁脉冲压缩放电结构。实验结果显示:各级磁脉冲压缩效果达到设计指标,电源输出电压峰达30 kV,输出电流峰值大于40 kA,电流脉冲宽度200 ns,满足Z箍缩放电等离子极紫外光源对主脉冲的要求。     

高性能水基钻井液处理剂研究进展及发展趋势

钻井液是石油钻井工程的“血液”,具有清洁井眼、保护钻具、稳定井壁和平衡地层压力等重要作用。本文综述了高性能水基钻井液处理剂的研究进展,主要包括抑制剂、润滑剂、包被剂和降滤失剂,包含了国内外的最新研究成果,也涉及国外油服公司和化学品公司在工程现场已经规模应用的先进产品。最后在现有高性能水基钻井液处理剂研究及应用的基础上,对其发展趋势进行了展望。