A discrete dislocation plasticity analysis of a single-crystal semi-infinite medium indented by a rigid surface exhibiting multi-scale roughness

Discrete dislocation plasticity was used to analyse plane-strain indentation of a single-crystal elastic–plastic semi-infinite medium by a rigid surface exhibiting multi-scale roughness, characterised by self-affine (fractal) behaviour. Constitutive rules of dislocation emission, glide and annihilation were used to model short-range dislocation interactions. Dislocation multiplication and the development of subsurface shear stresses due to asperity microcontacts forming between a single-crystal medium and a rough surface were examined in terms of surface roughness and topography (fractal) parameters, slip-plane direction and spacing, dislocation source density, and contact load (surface interference). The effect of multi-scale interactions between asperity microcontacts on plasticity is elucidated in light of results showing the evolution of dislocation structures. Numerical solutions yield insight into plastic flow of crystalline materials in normal contact with surfaces exhibiting multi-scale roughness.     

Interdiffusion and solid solution strengthening in Ni–Co–Pt and Ni–Co–Fe ternary systems

Diffusion couple experiments are conducted in Co–Ni–Pt system at 1200?°C and in Co–Ni–Fe system at 1150?°C, by coupling binary alloys with the third element. Uphill diffusion is observed for both Co and Ni in Pt rich corner of the Co–Ni–Pt system, whereas in the Co–Ni–Fe system, it is observed for Co. Main and cross interdiffusion coefficients are calculated at the composition of intersection of two independent diffusion profiles. In both the systems, the main interdiffusion coefficients are positive over the whole composition range and the cross interdiffusion coefficients show both positive and negative values at different regions. Hardness measured by performing the nanoindentations on diffusion couples of both the systems shows the higher values at intermediate compositions.     

On the comparative assessment of ratcheting-induced dislocation density in 42CrMo4 steel by X-ray diffraction profile analysis and hardness measurement

The phenomenon of ratcheting occurs under the influence of non-zero mean stress during cyclic loading; it singificantly reduces the low cycle fatigue life of engineering structures. The present investigation deals with a detailed comparison on the estimation of dislocation densities in the 42CrMo4 steel induced by ratcheting using two different methods, i.e. X-ray diffraction (XRD) profile analysis and hardness. The dislocation densities in the ratcheted specimens were assessed using XRD profile analysis following the modified Williamson–Hall method as well as hardness measurements following the modified Nix and Gao model. The results showed that dislocation density increased in the ratcheted specimens as compared to the unratcheted ones and increase in accumulation of ratcheting strain was correlated with the increase in dislocation densities in the ratcheted specimens. It was established that both hardness and X-ray diffraction profile analysis methods can very effectively be used to assess the dislocation densities in the ratcheted specimens.     

Experimental investigation on surface deformation of soft half plane indented by rigid wedge

In this work, the mechanical behavior of a block of soft material subject to large deformation from a series of wedge-shaped indenters is evaluated. Data fields acquired from digital image correlation (DIC) are compared with the existing theoretical models. The slope angles of the wedges vary from 5° to 73.5°, and the minimum measurement uncertainties of the DIC system are established in advance to define the accuracy. It is concluded that the assumptions underpinning the analytical theory make it difficult to characterize large deformation of soft materials during contact. The strain fields are also obtained from the measured displacement field and verify the previously postulated existence of two deformation sectors, namely, a so-called shrinkage sector symmetric to the loading axis and an expansion sector, which become smaller with the increasing load and decreasing wedge angle.     

Monitoring the effect of sonoporation on the cells using electrochemical approach

Sonoporation is applied to enhance the permeability of the cell to bioactive materials by employing the acoustic cavitation of microbubbles. This phenomena would be helpful in molecular biology, delivery of large molecules into the cells and gene therapy. Many methods have been applied to monitor the biological effects and trace of sonoporation on the cells such as scanning/transmission electron microscopy, confocal imaging and flow cytometry. Here, we monitored the effect of sonoporation on the cells using electrochemical method with an integrated three electrode system. Electrochemical responses of stimulated cells, compared to flow cytometry and electron microscopy results, presented different patterns of sonoporation in the cells detectable by cyclic voltammetry. In addition, confocal microscopy from actin stress fibers and young’s modulus measured by AFM revealed the correlation of cell mechanics and amount of induced sonopores in the cells. This method could be applied as a new trend in cellular mechanochemical studies.     

Mechanical properties of low porosity Dy123 bulks with different Dy211 content

Mechanical properties of low porosity Dy123 (DyBa₂Cu₃O_x) bulks with different Dy211 (Dy₂BaCuO₅) content were evaluated through bending tests and Vickers indentation tests of specimens cut from the bulks. The bending strength and the Young’s modulus of the low porosity bulks were higher than those of porous Dy123 bulks evaluated in the previous study. The bending strength of the low porosity bulks, which was decreased by the oxygen annealing, increased with increase of the Dy211 content. The fracture toughness of the area with uniform dispersion of the Dy211 particles was superior to that with low density of the Dy211 particles.     

Prediction of strength using flat cylindrical indentation method

Strength of structural components is predicted. Two cases have been studied to explore the possibility of determining the damage level of the materials by the flat cylindrical indentation method with the help of the finite element method (FEM). The first uses the Gurson model for analyzing the elastic–plastic damage. The second uses the Katchanov–Robotnov law to predict the creep damage. The analytical results show that the damage levels can be determined by the flat cylindrical indentation experimental method.     

边坡岩体质量分级的模糊层次分析

基于深度测量压入方法，以材料试验机Instron 5848 Microtester作为加载平台，外接高分辨力位移传感器，设计专用夹具，开发出该材料试验 机的宏观压入功能. 研究发现：对于机架柔度，无需再进行修正；对于压针接触面积， 可用相关的方法计算. 采用Oliver-Pharr方法处理测试数据，可获得材料的 硬度和弹性模量. 为了验证试验的可靠性，选用5种典型金属材料，将宏观压入测试结果与 MTS Nano Indenter XP测试结果进行对比，二者基本一致，其分散性均在10{\%}以内. 显示了开发传统材料试 验机宏观压入测试功能的可行性.