电镀铜薄膜力学性能的实验研究

电子器件中大量使用铜膜作为电信号通道,而且一般采用电镀工艺制成.铜膜的力学性能参数对于其热疲劳可靠性的研究非常重要.目前有关该材料的力学性能研究尚不充分,而且数据极为不统一.本文借助于纳米压痕法、声发射等实验手段对电镀铜薄膜的静态力学性能(包括弹性模量和屈服强度等)及疲劳性能进行了测试.结果发现,与大块铜材料相比,电镀铜薄膜的弹性模量低很多,但屈服强度与大块铜材料相当,甚至高出200％.同时,本文采用弯曲疲劳实验,以电阻变化为失效判据,对镀铜材料的疲劳性能进行了测试,获取了该材料不同失效判据下的疲劳寿命预测模型的系数.     

含冲击损伤复合材料层压板压缩破坏机制的声发射特性研究

复合材料层压板在压缩破坏过程中包含了丰富的声发射信息.为了研究含冲击损伤的复合材料层压板的压缩破坏机制,采用声发射观察层压板的压缩破坏过程,通过分析声发射信号的特征规律,表征了在压缩载荷下材料损伤的形式及其演化过程.结果表明:通过对声发射参数(撞击计数、能量、幅值、事件位置)和载荷曲线进行综合分析,发现损伤的发展过程经过了初始阶段、平稳扩展期和断裂阶段,冲击造成的分层区域最先出现屈曲并最早破坏;在损伤初始阶段和平稳扩展期间,损伤是一种渐进式的增长,层压板具有一定的承载能力;在断裂阶段损伤快速扩展,层压板的承载能力迅速下降,在出现纤维密集断裂的现象后整体破坏.     

船用金属材料声发射信号特性研究

利用声发射技术对6种船用金属材料拉伸试验过程中产生的声发射信号进行了详细研究。通过对材料从弹性、屈服、强化直至破坏过程中的声发射信号参数统计分析,总结了船用金属材料拉伸过程中声发射信号事件数量、幅度、频率随拉力变化的分布规律,为在船用金属材料与结构缺陷中进行声发射检测的设备参数的配置、传感器的选择和危险等级的划分提供了基础数据。     

利用岩石声发射凯塞效应测定岩体地应力

将砂岩在整个变形阶段的声发射信号特征可划分为加载初期、压密阶段、裂纹稳定扩展阶段、裂纹非稳定扩展阶段、砂岩破坏阶段5部分。利用岩样声发射信号的特征,确定出岩石的凯塞效应点与其裂纹稳定扩展阶段的起始点相对应,并进一步得出岩石凯塞效应点的上限为裂纹稳定扩展阶段的终点,裂纹非稳定扩展阶段的起始点。凯塞效应点受岩样两端面的平行度、压机加载速率等有关,岩样端面不平整,在加载初期会有强烈的声发射信号;压机加载速率过大,声发射信号可能显示不出来或被后续更强的声发射信号所掩盖。计算出深度为670m处巷道周围天然应力3个主应力的大小和方向,与在现场用应力解除法和水压致裂法测得的天然应力相比,其数值基本一致,但方向存在一定的偏差。     

等离子喷涂铁基涂层的疲劳磨损裂纹行为

采用等离子喷涂制备了铁基涂层,使用球盘式疲劳磨损试验机进行涂层的疲劳磨损试验,利用声发射技术在线判断涂层开裂,并通用透射电子显微镜（TEM）分析了试验前后涂层内部微观结构,研究了喷涂层疲劳磨损裂纹的扩展行为。结果表明：制备的涂层致密,结合状态良好,主要相为铁素体,同时存在大量的非晶-纳米晶相,利用声发射技术能够表征涂层的临界失效状态,其内部疲劳磨损裂纹主要以韧性穿晶断裂的形式扩展。     

应用声发射技术的钢筋与混凝土粘结滑移特性研究

为研究钢筋与混凝土间的粘结滑移特性,分别对不同粘结长度的钢筋混凝土试件进行了拉拔试验,同时对粘结长度相同而钢筋外形不同的试件进行了比较试验.利用声发射技术采集相应波形信号,并对采集信号进行了小波去噪和Gabor小波时频分析.结果显示,各试件受力全过程均可分为完全粘结、局部脱粘、非线性滑移及残余粘结四个阶段;不同粘结长度...     

2D-C/SiC拉伸损伤的声发射信号聚类分析

对2D-C/SiC复合材料进行常温拉伸试验,利用声发射(AE)仪在线监测其损伤过程.应用K-均值聚类算法对AE信号进行模式识别,结合扫描电镜观察,发现2IC/SiC复合材料拉伸过程的损伤模式包括基体开裂、界面层脱粘、层间剥离、纤维断裂以及纤维束断裂等,并得到了各种损伤模式AE信号参数的中心值.通过对不同损伤模式AE累积事件数和累积能量随时间变化的统计分析,描述了2DC/SiC复合材料拉伸损伤演化过程.     

PM2.5 in China: Measurements,sources, visibility and health effects,and mitigation

Concern over the health effects of fine particles in the ambient environment led the U.S. Environmental Protection Agency to develop the first standard for PM_2.5 (particulate matter less than 2.5 μm) in 1997. The Particle Technology Laboratory at the University of Minnesota has helped to establish the PM_2.5 standard by developing many instruments and samplers to perform atmospheric measurements. In this paper, we review various aspects of PM_2.5, including its measurement, source apportionment, visibility and health effects, and mitigation. We focus on PM_2.5 studies in China and where appropriate, compare them with those obtained in the U.S. Based on accurate PM_2.5 sampling, chemical analysis, and source apportionment models, the major PM_2.5 sources in China have been identified to be coal combustion, motor vehicle emissions, and industrial sources. Atmospheric visibility has been found to correlate well with PM_2.5 concentration. Sulfate, ammonium, and nitrate carried by PM_2.5, commonly found in coal burning and vehicle emissions, are the dominant contributors to regional haze in China. Short-term exposure to PM_2.5 is strongly associated with the increased risk of morbidity and mortality from cardiovascular and respiratory diseases in China. The strategy for PM_2.5 mitigation must be based on reducing the pollutants from the two primary sources of coal-fired power plants and vehicle emissions. Although conventional Particulate Emission Control Devices (PECD) such as electrostatic precipitators in Chinese coal-fired power plants are generally effective for large particles, most of them may not have high collection efficiency of PM_2.5. Baghouse filtration is gradually incorporated into the PECD to increase the PM_2.5 collection efficiency. By adopting stringent vehicle emissions standard such as Euro 5 and 6, the emissions from vehicles can be gradually reduced over the years. An integrative approach, from collaboration among academia, government, and industries, can effectively manage and mitigate the PM_2.5 pollution in China.     

Nonideal effects behind reflected shock waves in a high-pressure shock tube

Abstract. Shock tubes often experience temperature and pressure nonuniformities behind the reflected shock wave that cannot be neglected in chemical kinetics experiments. Because of increased viscous effects, smaller tube diameters, and nonideal shock formation, the reflected-shock nonidealities tend to be greater in higher-pressure shock tubes. Since the increase in test temperature () is the most significant parameter for chemical kinetics, experiments were performed to characterize in the Stanford High Pressure Shock Tube using infrared emission from a known amount of CO in argon. From the measured change in vibrationally equilibrated CO emission with time, the corresponding ddt (or for a known time interval) of the mixture was inferred assuming an isentropic relationship between post-shock temperature and pressure changes. For a range of representative conditions in argon (24–530 atm, 1275–1900 K), the test temperature 2 cm from the endwall increased 3–8 K after 100 s and 15–40 K after 500 s, depending on the initial conditions. Separate pressure measurements using a shielded piezoelectric transducer confirmed the isentropic assumption. An analytical model of the reflected-shock gas dynamics was also developed, and the calculated 's agree well with those obtained from experiment. The analytical model was used to estimate the effects of temperature and pressure nonuniformities on typical chemical kinetics measurements. When the kinetics are fast (s), the temperature increase is typically negligible, although some correction is suggested for kinetics experiments lasting longer than 500 s. The temperature increase, however, has a negligible impact on the measured laser absorption profiles of OH (306 nm) and CH (216 nm), validating the use of a constant absorption coefficient. Infrared emission experiments are more sensitive to temperature and density changes, so nonuniformities should be taken into account when interpreting ir-emission data. Received 25 April 2000 / Accepted 8 September 2000     

New Strong MM FIR Emissions in CH2=CF2 Pumped by a Pulsed CO2 Laser

By pumping with a suitable pulsed CO₂ laser we have produced several strong MM laser lines in 1,1 difluoroethene. All the emissions are easily identified because the emission spectroscopy is simplified in pulsed optical pumping.