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New results on the phase diagram of KNbO 3 determined, from 10 to 650 K up to 30 GPa, with Raman scattering are given. On increasing pressure the Curie temperature T c was found to shift down regularly from 700 K, at atmospheric pressure, to 20 K at ~25 GPa. Up to 20 GPa, the pressure dependence of T c follows a classical regime described by the Ising model where the dipolar interaction follow a i 2 /v law, where i is the off-center displacement and v the unit cell volume. This behaviour found also for the ice VII-VIII is very likely encountered in a number of (anti)ferroelectric-paraelectric transformations involving positional disorder. 相似文献
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从统计计算的角度出发,提出多台设备老炼试验可靠性评估方法,并模拟计算了可靠度置信下限的覆盖率、分位点及标准差.结果表明此方法具有可行性和实用性. 相似文献
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Lan-lan Fang Qian Tao Ming-fang Li Ling-wen Liao Dong Chen Yan-xia Chen 《化学物理学报(中文版)》2010,23(5):543-548
Four methods, including voltammetric measurement of double layer capacitance, surface oxides reduction, under potential deposition of Cu and carbon monoxide (CO) stripping have been applied to evaluate the real surface area of a polycrystalline Pd (pc-Pd) electrode. The results reveal that the second and third methods lead to consistent results with deviations below 5%. And from the determined double layer capacitance and CO stripping charge, it is deduced that the double layer capacity unit area is 23.1±0.4 μF/cm2 and the saturated CO adlayer should be ca. 0.66 ML in order to ensure that the real surface area as determined isconsistent with the other two techniques. The applicability as well as the attentions when applying these techniques for the determination of the real surface area of pc-Pd electrodes have been discussed. 相似文献
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"自动回流消化仪"消化-AFS法测定油中的砷 总被引:2,自引:0,他引:2
本文报道了“自动回流消化仪”消化,原子荧光光度法测定的油中的砷。“自动回流消化仪”消化油既防止了砷元素的损失,又能使油容易消化,同时在试剂用量、劳动强度、消化速度等方面都有较好的效果。原子荧光光度法,采用新的仪器和原理,提出了方法的灵敏度。该法回收率为91.8%-104.7%,相对标准偏差0.51%,与传统湿法消化法比较无显著性差异(t0.05)。 相似文献