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61.
62.
Here we present a simple yet effective gas chromatography-mass spectrometry (GC-MS) identification approach for the detection of heteroatom-containing compounds (HACCs) in petroleum fractions. The MS/AMDIS (Automated Mass Spectral Deconvolution and Identification System) program was used to identify parts per million (ppm) HACC concentrations in petroleum fractions in place of traditional techniques (extraction and standard injection). Polycyclic aromatic sulfur heterocycles (S-PAHs) were used as model compounds to confirm the validity of the AMDIS identifiers, which were compared with extracted results using the off-line X-calibur software. AMDIS was able to identify ppm concentrations of S-PAHs in oil condensate. There was good agreement between experimental and AMDIS identification results for S-PAHs in oil condensate. AMDIS was also used to detect nitrogen-containing compounds (NCCs) and alkylphenols in oil condensate. Our results confirmed the presence of 2-methylbenzothiazole, carbazole, and 2,4-ditertbutyl phenol. In a crude oil sample, AMDIS identification of m/z=191 biomarkers was consistent with empirical results. Therefore, AMDIS can help to reduce the number of experimental steps in identification protocols. 相似文献
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64.
磺酰脲类除草剂的三维药效团模型 总被引:3,自引:0,他引:3
磺酰脲类除草剂是七十年代末期[1,2]开发的一类超高效除草剂,杀草谱广,用量极低.它通过抑制植物体内乙酰乳酸合成酶(ALS,acetolactatesynthase)的活性[3],破坏支链氨基酸缬氨酸、亮氨酸和异亮氨酸的合成,造成杂草的死亡.本文从三维角度出发,利用先进的三维分子设计软件APEX(ActivityPredictionExpertSystem)-3D[4],建立破酸豚类除草剂药效团模型(biophoremodel),辅助设计、筛选活性化合物;再由药效团构造出模拟ALS酶活性位点(activesites)的空间结构,以该模拟结构为基点,以期设计出全新结构的ALS酶抑制剂的… 相似文献
65.
In order to bridge the gap between the supply and the demand of talent cultivation, the existing talent cultivation system of applied chemistry specialty is reformed and a new "113" talent cultivation system is guided by Outcome-Based Education (OBE) education. The advanced engineering education mode is adopted to provide students with an engineering education based on the background environment of the conceptual-design-implementation-operation (CDIO) process. The characteristic "three modernizations" education mechanism, namely, cooperative education, family training and personalized guidance, are implemented. By building a new system of "113" talents training, an engineering talent training environment is formed, which takes the family as a unit, the enterprise as the background, and the project as the carrier. The problem of separating the supply from the demand of talents training for applied chemistry specialty will be fundamentally solved. 相似文献
66.
In this paper, we deal with the critical problems in residue arithmetic. The reverse conversion from a Residue Number System (RNS) to positional notation is a main non-modular operation, and it constitutes a basis of other non-modular procedures used to implement various computational algorithms. We present a novel approach to the parallel reverse conversion from the residue code into a weighted number representation in the Mixed-Radix System (MRS). In our proposed method, the calculation of mixed-radix digits reduces to a parallel summation of the small word-length residues in the independent modular channels corresponding to the primary RNS moduli. The computational complexity of the developed method concerning both required modular addition operations and one-input lookup tables is estimated as , where k equals the number of used moduli. The time complexity is modular clock cycles. In pipeline mode, the throughput rate of the proposed algorithm is one reverse conversion in one modular clock cycle. 相似文献
67.
该文讨论一个新的离散特征值问题,导出了相应的离散的Hamilton系统的保谱族,并且证明了它们是Liouville可积系。通过谱问题的双非线性化,导出一个新的可积的辛映射 。
相似文献
68.
聚类分析在股票市场板块分析中的应用 总被引:7,自引:1,他引:7
本文将聚类分析应用于股票市场的研究,研究实例表明,聚类分析方法是股市板块分析中的一种有效、实用的方法 相似文献
69.
具有偏差变元的双曲型微分方程组解的振动性 总被引:65,自引:0,他引:65
本文获得了双曲型方程组在齐次Neumann,Dirichlet和Robin边值条件下,所有解振动的充分条件. 相似文献
70.
Hong-Wei Ge Feng Qian Yan-Chun Liang Wen-li Du Lu Wang 《Nonlinear Analysis: Real World Applications》2008,9(4):1345-1360
In this paper, we first present a learning algorithm for dynamic recurrent Elman neural networks based on a dissimilation particle swarm optimization. The proposed algorithm computes concurrently both the evolution of network structure, weights, initial inputs of the context units, and self-feedback coefficient of the modified Elman network. Thereafter, we introduce and discuss a novel control method based on the proposed algorithm. More specifically, a dynamic identifier is constructed to perform speed identification and a controller is designed to perform speed control for Ultrasonic Motors (USM). Numerical experiments show that the novel identifier and controller based on the proposed algorithm can both achieve higher convergence precision and speed than other state-of-the-art algorithms. In particular, our experiments show that the identifier can approximate the USM's nonlinear input–output mapping accurately. The effectiveness of the controller is verified using different kinds of speeds of constant, step, and sinusoidal types. Besides, a preliminary examination on a randomly perturbation also shows the robust characteristics of the two proposed models. 相似文献