Study of defect evolution by TEM with in situ ion irradiation and coordinated modeling

The paper describes a novel transmission electron microscopy (TEM) experiment with in situ ion irradiation designed to improve and validate a computer model. TEM thin foils of molybdenum were irradiated in situ by 1?MeV Kr ions up to ～0.045 displacements per atom (dpa) at 80°C at three dose rates ?5?×?10^?6, 5?×?10^?5, and 5?×?10^?4?dpa/s – at the Argonne IVEM-Tandem Facility. The low-dose experiments produced visible defect structure in dislocation loops, allowing accurate, quantitative measurements of defect number density and size distribution. Weak beam dark-field plane-view images were used to obtain defect density and size distribution as functions of foil thickness, dose, and dose rate. Diffraction contrast electron tomography was performed to image defect clusters through the foil thickness and measure their depth distribution. A spatially dependent cluster dynamic model was developed explicitly to model the damage by 1?MeV Kr ion irradiation in an Mo thin foil with temporal and spatial dependence of defect distribution. The set of quantitative data of visible defects was used to improve and validate the computer model. It was shown that the thin foil thickness is an important variable in determining the defect distribution. This additional spatial dimension allowed direct comparison between the model and experiments of defect structures. The defect loss to the surfaces in an irradiated thin foil was modeled successfully. TEM with in situ ion irradiation of Mo thin foils was also explicitly designed to compare with neutron irradiation data of the identical material that will be used to validate the model developed for thin foils.     

Effect of Pt on interdiffusion and mechanical properties of the γ and γ′ phases in the Ni–Pt–Al system

The effect of Pt on the growth kinetics of the γ′-[Ni(Pt)]₃Al ordered intermetallic phase and the γ-Ni(Pt, Al) solid solution diffusion rates of the species, hardness and elastic modulus was examined by employing the diffusion couple experimental technique. Experiments were conducted by using the β-Ni(Pt)Al phase and Ni(Pt) alloy couples, each of which had a fixed amount of Pt (5, 10 and 15 at. %) in both the end members so that the Pt content is more or less constant throughout the interdiffusion zone. The results suggest that the growth kinetics of both phases and the average effective interdiffusion coefficients of Ni and Al increase with the increase in Pt content. Nanoindentation studies across the compositional gradients show that the mechanical properties of the intermetallic phase in the superalloy are relatively insensitive to the presence of Pt but are more sensitive to the Ni/Al ratio. In contrast, the marked variation in the hardness of the γ phase were noted, increasing markedly with Al concentration in a given couple and also increasing with increasing Pt content. Possible causes for the observed variations are discussed.     

Spin-Hamiltonian parameters,defect model and defect structure for the tetragonal Mo5+ center in x-ray-irradiated α-ZnMoO4 crystals

ABSTRACT

The spin-Hamiltonian parameters (g factors g_i, hyperfine structure constants A_i (⁹⁵Mo⁵⁺) and A_i (⁹⁷Mo⁵⁺), i?=?// and ⊥) assigned to the tetragonal Mo⁵⁺ (4d¹) tetrahedral center in α-ZnMoO₄ crystal caused by a Mo⁶⁺(1) ion trapping an electron after x-ray irradiation are calculated from the high-order perturbation formulas resting on the two-mechanism model. The model takes account of both the effects of crystal-field (CF) mechanism concerning the CF excited states in the CF theory and that of the charge-transfer (CT) mechanism related to CT excited states. The calculated results are reasonably consistent with the experimental values, confirming this assignment (or defect model). The calculations also indicate that the effect of CT mechanism cannot be neglected. The defect structure (particularly, the angular distortion) and signs of constants A_i (⁹⁵Mo⁵⁺) and A_i (⁹⁷Mo⁵⁺) of this Mo⁵⁺ defect center are also decided from the calculations. The outcomes are discussed.     

一个非协调膜元的高精度分析

本文讨论一个四自由度三角形非协调膜元的整体超收敛性，外推和亏量校正。     

二维正方各向异性碲圆柱光子晶体完全禁带中缺陷模的FDTD计算分析和设计

用FDTD方法计算了二维正方晶胞各向异性碲圆柱光子晶体的点缺陷模.为了得到TE,TM模式在完全禁带中具有相同共振频率的缺陷模,对中心点缺陷半径Rd以及中心附近对称位置的点缺陷半径Rn做了一系列微调.计算表明,TM模对于Rn的变化不敏感,而TE模随着Rn的改变出现了明显的规则的移动趋势.通过计算分析,发现对应于f=0.4的背景(R=0.3568a),当Rd=0.55a,Rn=0.26a时在完全禁带中TE和TM的缺陷模具有相同的共振频率ω0=0.2466ωe(其中ωe=2πca,a为晶格常数) 关键词： 时域有限差分法 光子晶体 缺陷模 各向异性     

Defect of the five-thirds law using the Wiener-Hermite expansion

Application of the refined Wiener-Hermite expansion with moderate to high Reynolds numbers Re to homogeneous, isotropic turbulence is presented. The results show a defect to Kolmogorov's five-thirds law, increase in the absolute value of the exponent comparable with many theoretical predictions. Midrange spectra up to fluctuation Reynolds numbers of 10⁸ show little, if any, dependence of the defect on Re, as long as the initial spectra do not deviate too far from their equilibrium states. The renormalization scheme has also been proven to have no effect on the final shape of the spectrum.     

小尺度阻尼边界封闭空间声传递函数的有限元素法计算

如何求解阻尼边界封闭空间中声源点到接收点的低频声传递函数已成为目前小尺度封闭空间可听化技术研究的关键技术，能处理任意形状及复杂边界条件的有限元素法可作为求解该问题的适合方法，以室内声声有源Helmholtz方程及其相应边界方程为基础，本文推导出了用于小尺度阻尼边界封闭空间声传递函数的有限元素求解方法，并编制了相应的计算机程序，在算例中，首先通过与模态叠加法计算结果进行比较，验证了该方法的正确性。最后计算了某型车体内腔中任意两点间声传递函数。     

基于3G-ASCX的小型飞行器异常导航信号检测系统设计

传统方法在异常导航信号信噪比较低时对小型飞行器异常导航信号的检测效果不理想。设计并实现了一种基于3G-ASCX的小型飞行器异常导航信号检测系统,硬件设计时着重于ASCX传感器模块、异常导航信号检测模块、主控基站模块、3G/GPRS传输模块的研究,3G/GPRS传输模块的硬件设计中,通过功耗低体积小的CC1100完成异常导航信号的收发,传输过程中通过芯片STC12C5410AD完成电容的平衡转换,选取了MC3486进行电压的转换,最终实现异常信号数据的安全快速传输;软件设计中,系统软件流程设计及异常导航信号检测模块软件设计,最后进行仿真实验,实验结果证明,相比传统系统,所设计系统检测到的小型飞行器异常导航信号同实际测量的异常导航信号具有较高的匹配度,与实际值相比,误差小于1dB,适合推广使用。     

The structure of blocks

In this paper, we focus on the structure of p-blocks with defect group satisfying some special condition. These special conditions include: two elements of the defect group are conjugate to each other in defect D if and only if they are conjugate to each other in G; the number of conjugacy classes whose p-part is contained in P by conjugacy is not larger than ∣P∣     

Additivity of tunnel number for small knots

We show that for small knots , and that for small knots . Received: March 10, 1997.