Sensitive determination of sulfonamides in environmental water by capillary electrophoresis coupled with both silvering detection window and in‐capillary optical fiber light‐emitting diode‐induced fluorescence detector

A new detector, silvering detection window and in‐capillary optical fiber light‐emitting diode‐induced fluorescence detector (SDW‐ICOF‐LED‐IFD), is introduced for capillary electrophoresis (CE). The strategy of the work was that half surface of the detection window was coated with silver mirror, which could reflect the undetected fluorescence to the photomultiplier tube to be detected, consequently enhancing the detection sensitivity. Sulfonamides (SAs) are important antibiotics that achieved great applications in many fields. However, they pose a serious threat on the environment and human health when they enter into the environment. The SDW‐ICOF‐LED‐IFD‐CE system was used to determine fluorescein isothiocyanate (FITC)‐labeled sulfadoxine (SDM), sulfaguanidine (SGD) and sulfamonomethoxine sodium (SMM‐Na) in environmental water. The detection results obtained by the SDW‐ICOF‐LED‐IFD‐CE system were compared to those acquired by the CE with in‐capillary optical fiber light‐emitting diode‐induced fluorescence detection (ICOF‐LED‐IFD‐CE). The limits of detection (LODs) of SDW‐ICOF‐LED‐IFD‐CE and ICOF‐LED‐IFD‐CE were 1.0–2.0 nM and 2.5–7.7 nM (S/N = 3), respectively. The intraday (n = 6) and interday (n = 6) precision of migration time and corresponding peak area for both types of CE were all less than 0.86% and 3.68%, respectively. The accuracy of the proposed method was judged by employing standard addition method, and recoveries obtained were in the range of 92.5–102.9%. The results indicated that the sensitivity of the SDW‐ICOF‐LED‐IFD‐CE system was improved, and that its reproducibility and accuracy were satisfactory. It was successfully applied to analyze SAs in environmental water.     

回转窑滚圈多轴疲劳寿命预测及与轴线偏移关系研究

结合轴线偏移情况开展回转窑滚圈多轴疲劳寿命研究,采用了Wang和Brown提出的多轴疲劳准则和雨流计数法及Miner准则进行累积损伤评估．回转窑运行轴线偏移会导致滚圈承受的支承载荷分布严重不均,因此引入载荷比来描述轴线偏移程度以进一步定量分析滚圈应力．采用有限元软件ANSYS进行了各载荷比下滚圈的接触应力分析,并根据滚动接触区域情况计算得到了切向摩擦应力．以某回转窑滚圈为分析对象,计算得到了随载荷比变化的疲劳寿命曲线,揭示了轴线偏移对滚圈疲劳寿命的影响规律．研究对减少滚圈疲劳失效有重要意义,同时也可作为轴线调整和优化调窑的理论依据．     

A weighted penalty finite element method for the analysis of power-law fluid flow problems

In this paper, a new finite element method for the flow analysis of the viscous incompressible power-law fluid is proposed by the use of penalty-hybrid/mixed finite element formulation and by the introduction of an alternative perturbation, which is weighted by viscosity, of the continuity equation. A numerical example is presented to exhibit the efficiency of the method.The Project Supported by the National Natural Science Foundation of China.     

染料敏化TiO2/WO3薄膜电池的光电变色

用光电化学方法研究了染料Ru(П) (4, 4′di COOEt 2, 2′bpy)2 (2, 2′bpy 4, 4′di CONH L tyrosineethylester) (PF6)2 (简写为Ru4)敏化TiO2 纳米结构电极的光电转换过程,同时,在导电玻璃上电沉积得到WO3 薄膜.结果表明,染料敏化的TiO2 多孔膜具有光电转换性能, WO3 薄膜具有良好的电致变色效应,将前者与电沉积得到的WO3 薄膜组成电池,在白光照射下可产生显著的颜色变化,有望用于自供电源的电色灵巧窗(Self poweredsmartwindow).     

Experimental study of the plasma window

The plasma window is an advanced apparatus that can work as the interface between a vacuum and a high pressure region. It can be used in many applications that need atmosphere-vacuum interface, such as a gas target, electron beam welding, synchrotron radiation and a spallation neutron source. A test bench of the plasma window is constructed in Peking University. A series of experiments and the corresponding parameter measurements have been presented in this article. The experiment result indicates the feasibility of such a facility acting as an interface between a vacuum and a high pressure region.     

Remaining Useful Life Prediction Model for Rolling Bearings Based on MFPE–MACNN

Aiming to resolve the problem of redundant information concerning rolling bearing degradation characteristics and to tackle the difficulty faced by convolutional deep learning models in learning feature information in complex time series, a prediction model for remaining useful life based on multiscale fusion permutation entropy (MFPE) and a multiscale convolutional attention neural network (MACNN) is proposed. The original signal of the rolling bearing was extracted and decomposed by resonance sparse decomposition to obtain the high-resonance and low-resonance components. The multiscale permutation entropy of the low-resonance component was calculated. Moreover, the locally linear-embedding algorithm was used for dimensionality reduction to remove redundant information. The multiscale convolution module was constructed to learn the feature information at different time scales. The attention module was used to fuse the feature information and input it into the remaining useful life prediction module for evaluation. The appropriate network structure and parameter configuration were determined, and a multiscale convolutional attention neural network was designed to determine the remaining useful life prediction model. The results show that the method demonstrates effectiveness and superiority in degrading the feature information representation and improving the remaining useful life prediction accuracy compared with other models.     

Modeling of the dynamic behavior of systems with rolling elements

Bearings, friction wheels, cams, etc. are widely employed elements in machine construction. The modeling of the dynamics of rolling friction plays therefore a crucial role in the simulation and optimization of such systems. This paper describes a recently developed transient-rolling-friction model with its application to different generic dynamical systems, to simulate the effects of rolling friction or traction on the dynamics of mechanical systems. The results, which are expressed in terms of the complex stiffness arising in the rolling-contact patches, show that the behavior depends on both the amplitude and the frequency of oscillation. For low amplitudes and frequencies, the behavior is quasi-linear. For increasing amplitudes and frequencies, however, strong non-linearities appear, leading to complex behavior.     

耐高压球形锗窗的研制

研制了耐高压的球形锗窗，测量了其光学和力学性能。     

连续CO2激光对红外窗口材料损伤研究

研究了连续ＣＯ２激光对几种红外窗口材料的表面损伤特性，研究表明，损伤机制在于杂质缺陷吸收造成的热冲击应力破坏。深入研究了杂质缺陷密度、焦斑与材料损伤阈值的关系，并建立了一个损伤模型。同时分析了热冲击应力破坏方式。     

A rolling window optimization method for large-scale WCDMA base stations planning problem

The large-scale base station planning problem for wideband code division multiple access (WCDMA) wireless networks is studied in this paper. A new rolling window optimization method is presented, where the global optimization problem is decomposed into small optimization sub-problems, which are defined on a series of successive rolling windows. Effective rolling strategies are designed in the rolling optimization method based on the prediction of the interference among the base stations in the WCDMA wireless network. We show that the proposed method has the property that the global objective is non-increasing in the successive optimization procedure. Simulations are carried out to analyze the performance of the proposed optimization method, which show the importance of the rolling strategy.