全文获取类型
收费全文 | 3857篇 |
免费 | 329篇 |
国内免费 | 399篇 |
专业分类
化学 | 973篇 |
晶体学 | 14篇 |
力学 | 1071篇 |
综合类 | 78篇 |
数学 | 1189篇 |
物理学 | 1260篇 |
出版年
2024年 | 9篇 |
2023年 | 47篇 |
2022年 | 102篇 |
2021年 | 142篇 |
2020年 | 129篇 |
2019年 | 101篇 |
2018年 | 105篇 |
2017年 | 166篇 |
2016年 | 238篇 |
2015年 | 166篇 |
2014年 | 197篇 |
2013年 | 248篇 |
2012年 | 185篇 |
2011年 | 221篇 |
2010年 | 196篇 |
2009年 | 233篇 |
2008年 | 227篇 |
2007年 | 205篇 |
2006年 | 201篇 |
2005年 | 183篇 |
2004年 | 180篇 |
2003年 | 142篇 |
2002年 | 122篇 |
2001年 | 106篇 |
2000年 | 88篇 |
1999年 | 87篇 |
1998年 | 79篇 |
1997年 | 69篇 |
1996年 | 55篇 |
1995年 | 59篇 |
1994年 | 53篇 |
1993年 | 27篇 |
1992年 | 23篇 |
1991年 | 23篇 |
1990年 | 24篇 |
1989年 | 14篇 |
1988年 | 21篇 |
1987年 | 18篇 |
1986年 | 13篇 |
1985年 | 15篇 |
1984年 | 12篇 |
1982年 | 11篇 |
1981年 | 3篇 |
1980年 | 5篇 |
1979年 | 10篇 |
1978年 | 9篇 |
1977年 | 4篇 |
1976年 | 2篇 |
1974年 | 4篇 |
1973年 | 2篇 |
排序方式: 共有4585条查询结果,搜索用时 0 毫秒
51.
52.
在产品质量判定的抽样检验问题中,当目标指标需用破坏性试验才能得其值时,更为常用的是用非破坏性试验可得量值的协变指标量来预报它。但在产品抽样验收问题上,未能形成理论较为严密的方法,这是由于预报误差这个关键问题的处理尚未解决得好,即给不出抽样方案的功效计算的正确或是近似性较好的公式。本文通过建立合理的数学模型,把对目标指标的质量要求化为对协变指标量的统计要求,从而利用两者的回归关系,结合两种复杂的抽样方案,给出功效函数的计算公式和计算方法,并进行了分析。 相似文献
53.
54.
孔梯度陶瓷纤维复合膜管的制备及特性 总被引:1,自引:0,他引:1
陶瓷过滤管具有孔隙率高、耐腐蚀、耐高温、机械强度高、便于清洗、使用寿命长等优点,是高温烟尘处理用的高效过滤元件.本文研制了一种具有梯度孔结构堇青石陶瓷纤维复合膜过滤元件,该过滤元件是由多孔支撑体、过渡层和分离膜层组成.其中支撑体、过渡层和分离层的气孔率分别为35~40;、50~60;和60~70;.文中主要分析了孔梯度陶瓷纤维复合膜管的材料结构和抗热震性能,同时对复合膜管进行含尘气体过滤的冷态模拟试验.对于烟气中粒径大于或等于0.1μm的颗粒,复合膜管的截留率达到99.8;以上. 相似文献
55.
The traditional method for the determination of protein in food needs the operations of digestion, distillation, absorption, and titration; therefore, it is complicated and time-consuming and requires professional personnel. Is there a more convenient and faster detection method that can directly determine the ammonium ions in protein digestion solution to obtain the protein content of food and avoid the distillation–absorption–titration process? The feasibility of water ammonium ion test kits for food protein rapid detection was discussed here. After digestion, the protein in food transforms into ammonium ions in the digestion solution. Because of the variety of food, there are many different inorganic ions left in the food digestion solution, and at the same time, digestion agents are added in the digestion process and become potential interference factors in ammonium determination. Therefore, the detection accuracy of ammonium test kits needs to be evaluated first, including their anti-interference ability. The standard curve of ammonium was established by the test kit. When the ammonium concentration was 0.00–2.50 mg/L, the absorbance at 620 nm was linearly related to the ammonium concentration, the determination coefficient R2 was 0.9995, and the detection limit of this method was 0.01 mg/L. The influences of temperature, pH value, and reaction time on the test kit method were discussed. The precision was 0.90–3.33%; the repeatability was 1.71–4.86%; and the recovery rate of tap water, river water, and sea water was controlled within 90–103%. The anti-interference ability of the evaluated test kit was better than that of the national standard detection method. The test kit, combined with sample pretreatment and protein conversion formula, was used to detect protein in different types of food (milk powder, rice flour, wheat flour, soy, banana, milk, fish food, chicken food, and dog food). The results showed that there were no significant differences (ρ > 0.05) between the national method and the test kit method. The ammonium ion test kit method shortened the determination time and had higher sensitivity, showing its potential for the rapid determination of food protein. 相似文献
56.
57.
58.
Fabrication and characterization of rod-like nano-hydroxyapatite on MAO coating supported on Mg-Zn-Ca alloy 总被引:1,自引:0,他引:1
J.H. GaoS.K. Guan J. Chen L.G. WangS.J. Zhu J.H. HuZ.W. Ren 《Applied Surface Science》2011,257(6):2231-2237
The poor corrosion resistance of magnesium alloys is a dominant problem that limits their clinical application. In order to solve this challenge, micro-arc oxidation (MAO) was used to fabricate a porous coating on magnesium alloys and then electrochemical deposition (ED) was done to fabricate rod-like nano-hydroxyapatite (RNHA) on MAO coating. The cross-section morphology of the composite coatings and its corresponding energy dispersion spectroscopy (EDS) surficial scanning map of calcium revealed that HA rods were successfully deposited into the pores. The three dimensional morphology and scanning electron microscopy (SEM) image of the composite coatings showed that the distribution of the HA rods was dense and uniform. Atomic force microscope (AFM) observation of the composite coatings showed that the diameters of HA rods varied from 95 nm to 116 nm and the root mean square roughness (RMS) of the composite coatings was about 42 nm, which were favorable for cellular survival. The bonding strength between the HA film and MAO coating increased to 12.3 MPa, almost two times higher than that of the direct electrochemical deposition coating (6.3 MPa). Compared with that of the substrate, the corrosion potential of Mg-Zn-Ca alloy with composite coatings increased by 161 mV and its corrosion current density decreased from 3.36 × 10−4 A/cm2 to 2.40 × 10−7 A/cm2 which was due to the enhancement of bonding strength and the deposition of RNHA in the MAO pores. Immersion tests were carried out at 36.5 ± 0.5 °C in simulated body fluid (SBF). It was found that RNHA can induce the rapid precipitation of calcium orthophosphates in comparison with conventional HA coatings. Thus magnesium alloy coated with the composite coatings is a promising candidate as biodegradable bone implants. 相似文献
59.
描述一种微光像增强器综合测试系统的总体设计。设计采用了组合结构,使系统只用单一的光源就可以测试微光像增强器九项光量子类和几何类的参数,具有以往几台常规测试仪器功能的总和。系统对各参数测量的不确定度2~4%。 相似文献
60.
大功率窄脉冲半导体激光器主要光电性能参数为:输出峰值光功率、阈值电流、正向电压、上升时间、峰值波长、光谱半宽、半强度角.根据激光制导系统对大功率窄脉冲激光器参数的特殊测试要求,研制一种大功率窄脉冲激光器测试平台,将小型化大功率激励器功放模块、大范围可调DC-DC模块、信号源板、激光器座、光学准直镜集成在一个平台上,与峰值功率计、光谱仪、CCD摄像机等仪器配合,可测出大功率窄脉冲激光器的峰值功率、峰值波长及波长随温度变化的漂移特性、发光芯均匀性等参数.介绍了大功率窄脉冲激光器测试台的特点,并对测试结果作了论述. 相似文献