Optimized FIB silicon samples suitable for lattice parameters measurements by convergent beam electron diffraction

The aim of this paper is to check the effect of artefacts introduced by focused ion beam (FIB) milling on the strain measurement by convergent beam electron diffraction (CBED). We show that on optimized silicon FIB samples, the strain measurement can be performed with a sensitivity of about 2.5 × 10⁻⁴ which is very close to the theoretical one and we conclude that FIB preparation can be suitable for such measurements in microelectronic devices.

To achieve this, we first used CBED and electron energy loss spectroscopy (EELS) which provide a procedure permitting an exact knowledge of the sample geometry, i.e. the thickness of both amorphous and crystalline layers. This procedure was used in order to measure the FIB-amorphized sidewall layer. It was found that if the FIB preparation is optimized one can reduce this amorphous layer down to around 7 nm on each side. Secondly different preparation techniques (cleavage, Tripod™ and FIB) permit to check if the surface damaged layer introduced by FIB influences the strain state of the sample. Finally, it was found that the damaged layer does not introduce measurable strain in pure silicon but reduces appreciably the quality of the CBED patterns.     

自由空间量子通讯实验中纠缠源的研制

设计了适合自由空间量子通讯实验的纠缠源. 纠缠光子对的单模光纤搜集率约为每秒20000对,水平竖直方向的纠缠对比度大于95%,正负45°方向的纠缠对比度大于90%. 在本地得到了大于100个标准偏差的Bell 不等式破缺. 满足20 km量级的自由空间量子通讯试验要求. 关键词： 纠缠光子对 位相匹配 收集效率 贝尔不等式     

低温缓冲层对氧化锌薄膜质量的影响

利用金属有机化学气相沉积(MOCVD)法,在Si衬底上外延生长ZnO薄膜。为了改善氧化锌薄膜的质量,首先在Si衬底上生长低温ZnO缓冲层,然后再生长高质量的ZnO薄膜。通过XRD、SEM、光致发光(PL)光谱的实验研究,发现低温ZnO缓冲层可有效降低ZnO薄膜和Si衬底之间的晶格失配以及因热膨胀系数不同引起的晶格畸变。利用低温缓冲层生长的ZnO薄膜的(002)面衍射峰的强度要比直接在Si上生长的ZnO薄膜样品的高,并且衍射峰的半高宽也由0.21°减小到0.18°,同时有低温缓冲层的样品室温下的光致发光峰也有了明显的增高。这说明利用低温缓冲层生长的ZnO薄膜的结晶质量和光学性质都得到了明显改善。     

用于像移探测的位平面匹配改进算法

像移探测作为电子稳像的重要的步骤,直接影响稳像的精度和速度。针对传统位平面匹配算法的局限,对各阶位平面的探测效果进行了综合测试,并提出了一种改进方案,即对位平面4,5经过下采样后组成一个合成位平面来进行匹配。研究了匹配块大小变化对位平面算法的影响,比较了相邻帧和固定帧两种参考帧选取方法的优劣。实验表明,改进的位平面匹配算法提高了位平面算法的稳健性,在没有增加计算量的前提下,算法精度达到了与全搜索块匹配法相当的程度。     

Study on Interaction Between Two Parallel Plates with Iteration Method in Functional Theory

利用泛函分析理论中的迭代法,分别计算了平行平板双电层在高、中、低电位下的相互作用能,并以数值法所得结果为参照,在各电位下分别与Debye-Hückel线性近似法、Langmuir近似法所得的结果进行比较．结果表明,DH线性近似法和Langmuir近似法均只能分别局限于极低或极高电位,而泛函迭代法不但有简单的解析表达式,而且在各种电位下都能得到较满意的结果.     

地面铺设缆线的高空电磁脉冲响应研究

 利用时域多分辨分析方法,对地面铺设缆线屏蔽层感生电流的规律进行了研究。给出了屏蔽层感生电流与缆线距离地面的高度、缆线的长度、电磁脉冲的入射方向等的关系。结果表明：屏蔽层电流幅度随着缆线距离地面高度增高而增加;屏蔽层电流幅度、前沿、半高宽随着缆线长度增加而增加,直到分别达到各自的最大值;电磁脉冲正入射时,屏蔽层电流幅度沿缆线分布呈现中间大、两边小的规律;电磁脉冲斜入射时,屏蔽层电流相对电磁脉冲正入射时,幅度更高、前沿更快、半高宽更窄,幅度沿缆线的分布情况为从一端到另一端逐渐增大。     

针对平移和旋转的快速电子稳像方法

针对视频图像中存在的平移抖动和旋转抖动,提出了一种基于灰度投影和模板匹配的电子稳像方法。用网格法搜索图像中灰度特征明显的区域,结合分象限法提高系统的鲁棒性,在不同坐标系下分别投影,纠正平移和旋转偏差。给出了模板制作方法和配准步骤。实验证明,该方法具有较高的精度和很高的处理速度,能够实时去除由视频图像抖动引起的噪声。     

亚单分子层三聚氰胺的便携式拉曼检测

通过改进Lee和Meisel法,制备了两种银胶。以三聚氰胺分子为探针分子,银胶为SERS基底,使用便携式拉曼光谱仪进行拉曼测试。拉曼光谱表明银纳米粒子和三聚氰胺发生的吸附作用明显,三聚氰胺的四个较强振动峰有4～9cm-1的频移和强度比变化较大。由于SERS基底的表面增强作用,三聚氰胺的便携式拉曼光谱仪最小检测量达到了6×10-12g,实现了三聚氰胺的亚单分子层检测水平。该检测方法快捷、简便,如果结合奶粉或食品中三聚氰胺的固相萃取技术,将可以应用于三聚氰胺的现场、快速、半定量检测。     

Preparation and characterization of covalently bonded PVA/Laponite/HAPI nanocomposite multilayer freestanding films by layer‐by‐layer assembly

The layer‐by‐layer (LBL) assembly technique is an attractive method to make functional multilayer thin films and has been applied to fabricate a wide range of materials. LBL materials could improve optical transmittance and mechanical properties if the film components were covalently bonded. Covalently bonded nanocomposite multilayer films were prepared by employing hydrophilic aliphatic polyisocyanate (HAPI) as the reactive component, to react with Laponite and polyvinyl alcohol (PVA). FT‐IR spectra suggested that HAPI reacted with Laponite and PVA at ambient temperature rapidly. Ellipsometry measurement showed that the film thickness was in linear growth. The influences of HAPI on the optical, mechanical and thermal properties of the films were investigated by UV‐Vis spectroscopy, tensile stress measurement, DSC and TGA. The obtained results showed that the optical transmittance and mechanical strength were enhanced when the film components were covalently bonded by HAPI. © 2015 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2015 , 53, 545–551