Radiation damage by soft β-particles self-irradiation of β-tritiated polystyrene

The effect of self-irradiation of β-tritiated polystyrene under high vacuum at 25°C was studied, and simultaneous random chain scission and cross-linking were observed. Analyses of the gaseous products and the colored polymer residue showed that hydrogen was the only volatile product, while spectroscopic measurements indicated that the coloration was associated with the presence of main-chain double bonds.

G values for hydrogen formation GH₂, cross-linking, G _XL and chain scission, G _CS were obtained as follows: GH₂=0.031; G _CS=0.044; G _XL=0.061. Possible mechanisms of radiation damage are discussed.     

基于改进U-Net的量子点STM图像分割

为提升量子点图像分割精度,降低特征识别误差,提出一种基于改进U-Net的量子点图像分割方法.首先,在预处理阶段,设计了以色彩通道为权值的灰度化算法,以提升后续分割效果.其次,在STM图像分割部分,在原始U-Net结构上引入中间过渡层以均衡网络各层特征.而后,建立数据集,并通过实验对比不同分割算法的精确度、召回率、F-measure.最后,将分割算法应用于量子点的特征识别,并测试了不同分割方式对应用的影响.实验结果显示,改进灰度化方法保留细节信息丰富,明显提升了量子点分割精度;改进U-Net的平均精确率、召回率、F-measure相较原始网络分别提升了13.83%、2.16%、8.13%.同时,实验数据表明由于分割精度的提升,量子点数量、纵横比等特征参数的识别更加精确.     

光子扫描隧道显微镜的光电成像系统研究

本文论述了光子扫描隧道显微镜（ＰＳＴＭ）的显微成像机理、成像规律，针对具体的物理模型进行数值模拟计算，并得到了与实际探测相一致的场分布规律。采用自行研制的光子扫描隧道显微镜（ＰＳＴＭ）的显微实验系统对多种样品进行了表面显微成像研究，获得了关于样品表面三维立体图像信息，通过多种图像处理手段对原始图像进行后期处理，得到了更具视觉效果、更为逼真的样品表面图像。     

共焦激光扫描显微镜技术进展

共焦激光扫描显微镜已延伸到光学显微术领域，包括共焦荧光显微镜、共焦扫描光纤显微镜、彩色共焦激光显微镜、共焦光栅光学显微镜等。并很快成为半导体材料检测和生物医学诊断的重要工具。本文对国外该显微镜技术的特性和新的进展进行了综述。     

系列柱形薄壁腔靶制备工艺研究

为了从实验上深入研究超热电子产生规律，从而减少或抑制超热电子对惯性约束聚变（ＩＣＦ）的危害，我们制备了一系列薄壁腔靶，以供实验研究。本文详细地描述了柱形薄壁腔靶的制备工艺。利用ＮＧ－１０４型精密单向纵切车床，采用金刚石刀具车削，提高心轴质量，表表粗糙度可达０．１μｍ。采用电镀和磁控溅射二种方法镀膜，为了使腔靶壁厚均匀，在镀膜时，必须使心轴匀速旋转。利用磁控溅射在腔靶外表面再涂上１μｍ左右厚的二氧化硅，以提高超薄壁腔靶的强度和自立能力。在腐蚀心轴时，必须仔细控制酸的浓度，防止在腐蚀时因产生气泡太多，太快而使腔靶破裂。用Ｘ射线照相法和扫描电子显微镜测量腔靶的几何参数。制备系列柱形薄壁腔靶达到指标为：壁厚范围２～３０μｍ，壁厚均匀性小于１０％，表面粗糙度０．２～０．３μｍ。最后介绍了在“神光Ⅰ”上打靶结果。结果表明，实验值与理论值符合较好。     

基于扫描隧道显微镜的原子电子云结构

本文简要介绍了扫描隧道显微镜的基本工作原理，展示了一些扫描样品（石墨和铜）的电子云图，在简要介绍量子力学关于原子电子云结构基本理论的基础上，通过理论上的电子云结构与扫描结果的比较，在一定程度上验证了量子力学关于原子电子云结构理论的正确性．     

Influence of Interorbital Interference on Tunneling Process in STM

We present a theoretical study of the influence of intra-atomic interorbital interference on the formation of STM images of metal surfaces. The obtained results show that this kind of interference may modify significantly the tunneling current by the increase or decrease of the current contributions flowing through different orbitals of the surface atoms. STM simulations performed for aluminium and nickel surfaces indicate that the height of corrugation and the topographies of STM images of different surfaces depend considerably on this interference.     

Crystal structure and thermal behavior of two new organic monosulfates NH3(CH2)5NH3SO4 1.5H2O and NH3(CH2)9NH3SO4 H2O

The chemical preparation, the calorimetric studies and the crystal structure are given for two new organic sulfates NH₃(CH₂)₅NH₃SO₄ 1.5H₂O (DAP-S) and NH₃(CH₂)₉NH₃SO₄·H₂O (DAN-S). DAP-S is monoclinic P2₁/n with unit cell dimensions: a=11.9330(2) Å; b=10.9290(2) Å; c=17.5260(2) Å; β=101.873(1)°; V=2236.77(6) Å³; and Z=8. Its atomic arrangement is described as inorganic layers of units and water molecules separated by organic chains. DAN-S is monoclinic P2₁/c with unit cell parameters: a=5.768(2) Å; b=25.890(10) Å; c=11.177(5) Å; β=115.70(4)°; V=1504.0(11) Å³ and Z=4. Its structure exhibits infinite chains, parallel to the [100] direction where the organic cations are interconnected. In both structures a network of strong and weak hydrogen bonds connects the different components in the building of the crystal.     

Ripening of single-layer InGaAs islands on GaAs（001）

The present paper discusses our investigation of InGaAs surface morphology annealed for different lengths of time.After annealing for 15 min,the ripening of InGaAs islands is completed.The real space scanning tunneling microscopy(STM) images show the evolution of InGaAs surface morphology.A half-terrace diffusion theoretical model based on thermodynamic theory is proposed to estimate the annealing time for obtaining flat morphology.The annealing time calculated by the proposed theory is in agreement with the experimental results.     

激光点阵扫描法绝对定标太阳辐射计直射通道研究

利用可调谐激光器作为光源,以溯源于低温绝对辐射计的标准传递探测器作为激光束功率测量探测器,采用激光点阵扫描方法在太阳辐射计有效孔径光阑面形成均匀照度场,精确测量太阳辐射计870 nm无偏直射通道中心波长处绝对辐照度响应度。利用灯-单色仪系统扫描获得该通道相对光谱辐照度响应度,最终在实验室条件下获得该通道绝对光谱辐照度响应度,联合大气层外太阳照度谱数据通道内积分得到该通道大气层外响应常数V₀值,与NASA的GSFC中心的2009年定标结果差异仅为3.75%,定标不确定度达到2.06%,验证了这一新技术的原理可行性。