稀土芦丁配合物的合成、表征及抗肿瘤活性研究

合成了稀土离子Tb3+的芦丁配合物,通过元素分析、核磁共振氢谱、摩尔电导、红外光谱、紫外光谱,确定了配合物的组成和结构,结果表明,配合物的组成为Na5TbLCl7·6H2O(L=C27H29O16),同时采用噻唑蓝还原法(MTT比色法)测定了配体及配合物对HepG2肝癌细胞株的抗肿瘤活性,实验结果表明,配合物对HepG...     

On the problematic rising ratio of cosmic-ray positrons at ultra-high energies

Summary The rising ratio of cosmic-ray positrons at ultra-high energies of interactions seems to have puzzled the theorists to a great extent. We have made here a somewhat successful attempt to interpret the behaviour of this ratio,R=e⁺/(e⁺+e⁻), by putting into use the main physical ideas from our two previous works. The importance and the implications of this observation have also been highlighted and emphasized in the proper background.

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Riassunto Il crescente rapporto dei positroni dei raggi cosmici ad energie ultra-alte di interazioni sembra aver non poco confuso i teorici. Qui si tenta con un certo successo di interpretare il comportamento di questo rapportoR=e⁺/(e⁺+e⁻) usando i principali concetti fisici dei nostri due precedenti lavori. L'importanza e le implicazioni di questa osservazione sono state sottolineate ed enfatizzate nell'appropriato contesto.

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Резюме Увеличивающиеся отношение позитронов космических лучей при ультравыс оких энергиях, по-видимому, представляет загадку для теоретиков. В этой статье мы предпринимает отчасти успешную попытку интерпретировать поведение этого отношенияR=e⁺/(e⁺+e⁻), используя основные физические идеи из наших двух предыдущих публикаций. Отмчаются важностя и приложения полученных результатов.

     

Surface Acoustic Wave Characterization of Equivalent Young's Moduli for Patterned Films北大核心CSCD

Based on the equivalent elasticity theory for layered materials, the micro-mechanics equivalent models for single and dual damascene structures were established. The equivalent elastic constant of the patterned structure was introduced, to establish the propagation model for the surface acoustic waves propagating in the layered structure of the patterned film/ substrate, and the theoretical dispersion curves of the surface acoustic waves were calculated with Green’s function and the matrix method. The finite element method was used to calculate 24 numerical examples of damascene structures with different volume ratios, and the results were compared with those of the strain energy method. The results show that, the average relative errors of the equivalent Young’s moduli of the 300 nm-thick dual damascene film and the 100 nm-thick single damascene film are 2.06% and 2.27%, respectively. The research verifies the correctness of the equivalent patterned structure model and the feasibility of the surface acoustic wave method to characterize the mechanical properties of patterned films, and provides a reference for the development of suitable chemico-mechanical polishing technologies for patterned films under low pressure. © 2023 Editorial Office of Applied Mathematics and Mechanics. All rights reserved.     

Exponential stabilization of nonlinear systems under saturated control involving impulse correction

This paper studies the problem of locally exponential stabilization (LES) of nonlinear systems under a class of hybrid control in the framework of actuator saturation, where the limitation of actuator saturation on both continuous state feedback control and impulsive control are fully considered. Based on impulsive control theory and differential inclusion approach, some sufficient conditions for LES are derived, where a novel set inclusion relation is proposed to handle the double saturation nonlinearities. Different from the existing results that each part of saturated hybrid control (SHC) is required to stabilize the system individually, our results relax the requirement by making full use of the correction effect of the impulse. Moreover, the maximum of estimation of domain of attraction is obtained by a convex optimal problem and corresponding algorithm. The result is applied to the robustness for a class of nonlinear systems. Finally, the validity of the results is shown by two examples and their simulations, where the synchronization problem of Chua’s oscillator is illustrated in the framework of actuator saturation.     

Secondary-school teachers’ noticing of aspects of mathematics teaching talk in the context of one-day workshops

In a research project with one-day teacher education workshops for secondary-school mathematics teachers, our study explores the potential of tool-supported discussions in helping them to notice important and critical aspects of mathematics teaching talk. Mathematical practices of naming and explaining in teaching talk, students’ content learning challenges, and noticing processes of identifying, interpreting and deciding are the components of our framework and the tools that guided the design and implementation of three workshops on linear equations, fractions and plane isometries. The data was collected during the discussions with the seven teachers and the teacher educator throughout these workshops. The coding of the discussions allowed us to see discourse moves that reveal the teachers’ noticing of: (i) challenges in the identification of mathematical naming, (ii) mathematical explaining that voices the students’ learning, (iii) classroom practice in relation to mathematical naming and explaining.     

活性艳蓝稀土染料的研制

本文以活性艳蓝和稀土为原料,制备了活性艳蓝稀土染料,并研究了稀土离子的种类、稀土盐的种类以及稀一等对染料性能的影响。用目视分光光度法测定了染料的上色率和固色率。     

Finite Element Based Micro-mechanical Modeling of Interphase in Filler Reinforced Elastomers

Characteristic properties of elastomers can be tailored by embedding them with filler particles. Along with enhancing the overall properties of the composite, filler particles also induce some inelastic effects. In this paper, a finite element computational model is used to study the effect of microstructure morphology in filled elastomers, on its macroscopic large deformation behavior. A multiphase material model that accounts for the hypothesis of shift in glass transition temperature in the vicinity of the filler particle is developed to simulate the interphase between the fillers and the matrix. It also accounts for the breakdown and re-aggregation of filler networks under cyclic loading. Examples at the microstructural level, demonstrating the dynamics of the interphase using the developed multiphase model have been successfully simulated. The obtained results are in good qualitative agreement with the Mullins effect. Therefore, computational experiments using this methodology enable the prediction of the experimentally observed softening behavior in filled elastomers based on its microstructure evolution.     

原子吸收光谱法测定冬枣叶茶中的8种金属元素

采用湿法对沾化冬枣叶茶样进行消化处理,利用火焰原子吸收光谱法测定了茶中K、Na、Ca、Mg、Fe、Mn、Cu、Zn的含量.结果表明,该法的加标回收率为95.2%～104.2%,RSD≤3.35%.该法操作简单,结果准确,为开发和利用冬枣叶茶提供了一定的科学依据.