高效毛细管电泳法分析蓝色签字笔字迹色痕种类及相对形成时间

选用毛细管区带电泳分离模式,对13种市售蓝色签字笔样品字迹色痕进行了分析。当电压为15 kV、柱温为25 ℃时,以0.03 mol/L 四硼酸钠水溶液(外加10%(体积分数)的甲醇)为缓冲液,所有样品都可以得到良好的区分;依据紫外区检测结果,样品可以分为三大类、五小类;依据可见区检测结果,样品可以分为四类;两种分析结果相结合有助于增大不同样品之间的区分度;选择3种样品进行暗处保存老化制样,根据字迹中色料成分相对含量的变化,对字迹的相对形成时间进行了初步探讨。研究还发现纸张类型对于上述研究结果无影响。     

Photosensitive Materials for Integrated Optic Applications

Abstract

This article presents results of device fabrication using UV processing of materials and integrated optic components produced by flame hydrolysis deposition and hybrid sol-gel technology. Photosensitive materials were employed in the fabrication of channel waveguides and channel photo-imprinted waveguides incorporating Bragg gratings through single and double-step exposure.     

新型书写方式—化学书写术

应用化学原理发明了化学书写术，它比现行的书写方式具有突出的优点。     

Monolithically integrated photonic-crystal devices with photodiodes

In this paper, we demonstrate the monolithic integration of a conventional waveguide, a photonic crystal demultiplexer, a photonic crystal taper coupler, photonic crystal waveguides, and photodiodes in InGaAsP-based material to form a planar nano-optics system. Photonic crystal demultiplexers consist of hexagonally arranged air holes. Finite-difference time-domain method is implemented to investigate the performance of the demultiplexer. The system is fabricated using e-beam lithography and conventional photolithography. The input light at wavelengths of 1530 and 1550 nm can be separated using the demultiplexing system. These can then be detected by photodiodes that exhibit a wide-bandwidth performance of 22 GHz.     

在线协同写作的人类动力学分析

对人类在线行为模式的探讨是近年来人类动力学研究的热点.基于维基百科数据,文章针对一类重要且普遍的在线行为--在线协同写作,进行时间统计特性分析和内容更新统计分析.实证显示在线协同写作时间间隔分布呈多尺度特征,1 min到30 min和30 min到24 h两个时间段上时间间隔分别服从指数为1.62和1.16的幂律分布,而大于24 h的时间间隔服从形如F(τ)∝τ^{－b－alog(τ)}的累积分布.分析表明 关键词： 在线协同写作 人类动力学 多尺度特征 维基百科     

Embedded dots inside glass for optical film using UV laser of ultrafast laser pulse

Microstructures are usually fabricated on the surface of optical sheets to improve the optical characteristics. In this study, a new fabrication process with UV (ultraviolet) laser direct writing method is developed to embed microstructures inside the glass. Then the optical properties of glass such as reflection and refraction indexes can be modified. Single- and multi-layer microstructures are designed and embedded inside glass substrate to modify the optical characteristics. Both luminance and uniformity can be controlled with the embedded microstructures. Thus, the glass with inside pattern can be used as a light guide plate to increase optical performance. First, an optical commercial software, FRED, is applied to design the microstructure configuration. Then, UV laser direct writing with output power 2.5-2.6 W, repetition rate 30 kHz, wave length: 355 nm, and pulse duration 15 ns is used to fabricate the microstructures inside the glass. The effect of dot pattern in the glass such as the dot pitch, the layer gap, and the number of layer on the optical performance is discussed. Machining capacity of UV laser ranges from micron to submicrometer; hence with this ultrafast laser pulse, objectives of various dimensions such as dot, line width, and layers can be easily embedded in the glass by one simple process. In addition, the embedded microstructures can be made with less contamination. Finally, the optical performance of the glasses with various configurations is measured using a Spectra Colorometer (Photo Research PR650) and compared with the simulated results.     

Fabrication of fluorinated polyimide optical waveguides by micropen direct writing technology

A novel and cheap direct writing method based on the micropen has been developed to fabricate fluorinated polyimide stripe optical waveguides on Si/SiO₂ wafers. The overall design, starting material, micropen direct writing system and fabrication processes of the stripe optical waveguides are presented. The effects of the key direct writing parameters, such as the tip-to-substrate distance, extrusive gas pressure, writing speed and viscosity of the polyamic acid, on the dimension and morphology of the stripe optical waveguides are discussed in detail. After deposition by the micropen system and baking process, the fluorinated polyimide stripe optical waveguides with good morphology and surface quality can be fabricated using the optimal parameters. The propagation losses at the wavelength of 1.55 μm are in the range of 1.4-3.5 dB cm⁻¹ as characterized by different length combinations of the strip optical waveguides.     

极坐标激光直写法制作圆对称连续衍射元件掩模的能量表征方法研究

采用激光直写法制作连续衍射光学元件,具有过程简单、周期短、成本低等优点。介绍了极坐标激光直写法制作圆对称连续衍射元件的原理。通过实验,研究了衍射微结构深度与激光功率、曝光位置半径与激光功率的关系。实验结果显示,在相同曝光位置半径条件下,微结构深度与激光功率呈正比;在相同微结构深度条件下,曝光位置半径与激光功率呈正比。分析总结出了极坐标激光直写法制作圆对称连续衍射元件的能量表征方法,并采用该方法成功制作了圆对称连续衍射聚光透镜掩模。     

3D Laser Micro‐ and Nanoprinting: Challenges for Chemistry

3D printing is a powerful emerging technology for the tailored fabrication of advanced functional materials. This Review summarizes the state‐of‐the art with regard to 3D laser micro‐ and nanoprinting and explores the chemical challenges limiting its full exploitation: from the development of advanced functional materials for applications in cell biology and electronics to the chemical barriers that need to be overcome to enable fast writing velocities with resolution below the diffraction limit. We further explore chemical means to enable direct laser writing of multiple materials in one resist by highly wavelength selective (λ‐orthogonal) photochemical processes. Finally, chemical processes to construct adaptive 3D written structures that are able to respond to external stimuli, such as light, heat, pH value, or specific molecules, are highlighted, and advanced concepts for degradable scaffolds are explored.     

Melt Electrospinning

Melt electrospinning is relatively under‐investigated compared to solution electrospinning but provides opportunities in numerous areas, in which solvent accumulation or toxicity are a concern. These applications are diverse, and provide a broad set of challenges to researchers involved in electrospinning. In this context, melt electrospinning provides an alternative approach that bypasses some challenges to solution electronspinning, while bringing new issues to the forefront, such as the thermal stability of polymers. This Focus Review describes the literature on melt electrospinning, as well as highlighting areas where both melt and solution are combined, and potentially merge together in the future.